类型试验信息(多次测定用,隔开)图谱读取备注
项目代号:已存用户保存
项目名称:已存用户保存
试验名称可缺:待存默认值
时间点可缺:待存默认值
图谱类型:已存HPLC用户保存
样品类型:已存自制品,自制品,自制品用户保存
批号:已存2024102121批,2024102221批,2024102221批用户保存
规格可缺:待存60mg规格,60mg规格,60mg规格图谱读取
介质名称:已存pH6.8(内含3%SDS),pH6.8(内含3%SDS),pH6.8(内含3%SDS)用户保存
方法名称可缺:已存用户保存
转速可缺:已存用户保存
组成图标奥利司他胶囊溶出曲线测定HPLC图谱
自制品-2024102121批批()-pH6.8(内含3%SDS)-桨法-75转
注1:成分名称多个峰按出峰顺序【,】(半角逗号)隔开;
注2:试验批号和介质名称都一样的填一个;有任何不一致的需要【,】(半角逗号)隔开填写波数个;
注3:特别注意:批号和规格必须存在;
编号4887
项目名称奥利司他胶囊
选择方法
峰的筛选AUTO
根据对照品保留时间的0.95~1.05进行筛选;
对照品图谱务必只出主成分峰;
测定类型溶出
成分(个数)
成分名称
进样针数1针　2针
双波长
溶出度
图谱类型
制剂单位
谢超君2025-03-24 15:34:12进行了保存!
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既往测定情况概览
编号 试验名称 介质体积 取样体积 补液体积 R批号 R来源 R使用方法 R含量(%) R水分(%) R稀释 R标示量(mg) T稀释 操作
7941 900 1.5 0 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
7940 900 1.5 0 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
7937 使用
7818 900 1.5 1.5 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
7817 900 1.5 1.5 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
6250 900 1.5 1.5 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
6249 900 1.5 1.5 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
6248 900 1.5 1.5 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
6058 900 10 10 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
6057 900 10 10 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
6044 900 10 10 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
6025 900 1.5 1.5 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
6024 900 1.5 1.5 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
6003 900 1.5 1.5 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
6002 900 1.5 1.5 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
6001 900 1.5 1.5 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
5929 900 10 10 520027-202102 中检所 直接使用 99.5 0 200 120 2 使用
5928 使用
5927 900 10 10 520027-202102 中检所 直接使用 99.5 0 200 120 2 使用
5914 900 1.5 1.5 520027-202102 中检所 直接使用 99.5 0 200 60 1 使用
注意:::正在使用与其他方法的参数!恢复
【 奥利司他 】信息
介质体积(ml)取样体积(ml)补液体积(ml)
对照品批号对照品来源对照品使用方法
对照品含量(%)对照品水分(%)对照品稀释倍数
标示量(mg)供试品稀释倍数系数
称样量1(mg)称样量2(mg)
谢超君2025-03-24 15:34:21进行了保存!
类型波数成分响应值RSD%
审阅状态N
审阅权限孙文新,谢鑫慧,王丹,姜进硙,邵涛明
供试品测定波数:::3次
供试品测定片数:::6片
供试品取样点数:::5min,10min,15min,20min,30min,45min,60min,极限;
对照品的峰个数:::1个峰
图谱最多峰个数:::1个峰
对照品保留时间:::2.261
对照品　峰面积:::444522
待处理PDF文件:::查阅
筛选规则为:::自动
图谱张数为:::168
2025-03-24 15:34:24谢超君进行了保存!
序号文件名溶液名称保留时间峰面积
1zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-rj无峰无面积1NA1
2zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-dz1-12.2644490071MA1
3zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-dz1-22.2644433611MA1
4zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-dz1-32.2644447581MA1
5zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-dz1-42.2644443201MA1
6zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-dz1-52.2644440451MA1
7zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-5min-P12.292585031MA1
8zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-5min-P22.292544691MA1
9zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-5min-P32.294567881MA1
10zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-5min-P42.293581581MA1
11zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-5min-P52.293591501MA1
12zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-5min-P62.293488831MA1
13zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-10min-P12.2921562771MA1
14zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-10min-P22.2921610251MA1
15zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-10min-P32.2921593351MA1
16zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-10min-P42.2931623121MA1
17zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-10min-P52.2931581771MA1
18zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-10min-P62.2921412231MA1
19zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-15min-P12.2912278501MA1
20zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-15min-P22.2922369381MA1
21zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-15min-P32.2922372211MA1
22zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-15min-P42.2922376921MA1
23zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-15min-P52.2922328791MA1
24zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-15min-P62.2922183291MA1
25zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-20min-P12.2912783671MA1
26zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-20min-P22.2922901321MA1
27zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-20min-P32.2922936841MA1
28zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-20min-P42.2922919681MA1
29zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-20min-P52.2922883931MA1
30zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-20min-P62.2932746951MA1
31zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-30min-P12.2923454321MA1
32zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-30min-P22.2933545501MA1
33zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-30min-P32.2933649091MA1
34zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-30min-P42.2943599371MA1
35zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-30min-P52.2933580331MA1
36zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-30min-P62.2943473661MA1
37zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-45min-P12.2933965201MA1
38zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-45min-P22.2934027781MA1
39zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-45min-P32.2944161081MA1
40zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-45min-P42.2944084021MA1
41zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-45min-P52.2944096921MA1
42zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-45min-P62.2944034351MA1
43zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-60min-P12.2944236871MA1
44zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-60min-P22.2954244151MA1
45zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-60min-P32.2944371131MA1
46zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-60min-P42.2954293131MA1
47zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-60min-P52.2954321181MA1
48zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-60min-P62.2954282971MA1
49zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-jxzs-P12.2944437531MA1
50zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-jxzs-P22.2954398241MA1
51zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-jxzs-P32.2964495891MA1
52zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-jxzs-P42.2964405041MA1
53zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-jxzs-P52.2964439651MA1
54zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-jxzs-P62.2964421561MA1
55zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-dz2-12.2674469761MA1
56zzp-2024102121p-60mg-rcqx-pH6.8+3sdsjz-2-dz2-22.2684468491MA1
57zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-rj无峰无面积1NA1
58zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-dz1-12.2674440321MA1
59zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-dz1-22.2674445531MA1
60zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-dz1-32.2684443511MA1
61zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-dz1-42.2684440011MA1
62zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-dz1-52.2684446981MA1
63zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-5min-P12.297521421MA1
64zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-5min-P22.297678661MA1
65zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-5min-P32.298587251MA1
66zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-5min-P42.297552081MA1
67zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-5min-P52.297442401MA1
68zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-5min-P62.297632571MA1
69zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-10min-P12.2971506341MA1
70zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-10min-P22.2961665961MA1
71zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-10min-P32.2961617571MA1
72zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-10min-P42.2961581541MA1
73zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-10min-P52.2961386391MA1
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75zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-15min-P12.2972230451MA1
76zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-15min-P22.2962362231MA1
77zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-15min-P32.2952347571MA1
78zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-15min-P42.2962352381MA1
79zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-15min-P52.2962077901MA1
80zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-15min-P62.2952312091MA1
81zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-20min-P12.2952749641MA1
82zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-20min-P22.2952857141MA1
83zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-20min-P32.2962870481MA1
84zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-20min-P42.2962890701MA1
85zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-20min-P52.2962579141MA1
86zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-20min-P62.2952832471MA1
87zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-30min-P12.2943378231MA1
88zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-30min-P22.2933515161MA1
89zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-30min-P32.2953500591MA1
90zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-30min-P42.2953547161MA1
91zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-30min-P52.2943250161MA1
92zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-30min-P62.2953522981MA1
93zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-45min-P12.2943885901MA1
94zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-45min-P22.2944000591MA1
95zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-45min-P32.2943973771MA1
96zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-45min-P42.2954057971MA1
97zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-45min-P52.2943774591MA1
98zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-45min-P62.2944047651MA1
99zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-60min-P12.2964162501MA1
100zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-60min-P22.2944261081MA1
101zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-60min-P32.2944213331MA1
102zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-60min-P42.2944278131MA1
103zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-60min-P52.2954043851MA1
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105zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-jxzs-P12.2954362911MA1
106zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-jxzs-P22.2954455101MA1
107zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-jxzs-P32.2954395671MA1
108zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-jxzs-P42.2964449071MA1
109zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-jxzs-P52.2954276661MA1
110zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-jxzs-P62.2954425591MA1
111zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-dz2-12.2684439521MA1
112zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-1-dz2-22.2674440061MA1
113zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-rj无峰无面积1NA1
114zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-dz1-12.2684439021MA1
115zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-dz1-22.2674442251MA1
116zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-dz1-32.2684440601MA1
117zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-dz1-42.2684435681MA1
118zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-dz1-52.2684443101MA1
119zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-5min-P12.296577811MA1
120zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-5min-P22.292672181MA1
121zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-5min-P32.286573341MA1
122zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-5min-P42.278558461MA1
123zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-5min-P52.268548901MA1
124zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-5min-P62.264372821MA1
125zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-10min-P12.2621511291MA1
126zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-10min-P22.2601713681MA1
127zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-10min-P32.2621574491MA1
128zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-10min-P42.2631487891MA1
129zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-10min-P52.2621535251MA1
130zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-10min-P62.2621265161MA1
131zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-15min-P12.2612224761MA1
132zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-15min-P22.2602428631MA1
133zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-15min-P32.2582261091MA1
134zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-15min-P42.2572207821MA1
135zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-15min-P52.2572234341MA1
136zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-15min-P62.2552007641MA1
137zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-20min-P12.2532720331MA1
138zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-20min-P22.2522907461MA1
139zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-20min-P32.2512757671MA1
140zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-20min-P42.2492710101MA1
141zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-20min-P52.2482745651MA1
142zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-20min-P62.2462578821MA1
143zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-30min-P12.2443342071MA1
144zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-30min-P22.2423498511MA1
145zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-30min-P32.2413450091MA1
146zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-30min-P42.2403369761MA1
147zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-30min-P52.2393396181MA1
148zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-30min-P62.2383342901MA1
149zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-45min-P12.2363816211MA1
150zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-45min-P22.2363940481MA1
151zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-45min-P32.2353890021MA1
152zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-45min-P42.2343881561MA1
153zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-45min-P52.2333886051MA1
154zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-45min-P62.2333968271MA1
155zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-60min-P12.2324058681MA1
156zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-60min-P22.2314175791MA1
157zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-60min-P32.2304146411MA1
158zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-60min-P42.2304136921MA1
159zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-60min-P52.2294161251MA1
160zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-60min-P62.2284251391MA1
161zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-jxzs-P12.2274244831MA1
162zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-jxzs-P22.2274345451MA1
163zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-jxzs-P32.2254353031MA1
164zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-jxzs-P42.2244336861MA1
165zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-jxzs-P52.2244366651MA1
166zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-jxzs-P62.2234447921MA1
167zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-dz2-12.2004432801MA1
168zzp-2024102221p-60mg-rcqx-pH6.8+3sdsjz-2-dz2-22.2044427071MA1
计算
Current page cost:128 ms