氢氯噻嗪坎地沙坦酯片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100309-202205对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.7对照品水分(%)0对照品稀释倍数1000
标示量(mg)12.5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
112.014652204654094649704652744649784651700.05
212.064645664642154643900.06
单位质量响应值RSD%判断
38731.8938506.630.42数据可信
加速6月-供试品溶液-2024082321批-氢氯噻嗪-pH4.5
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1302095-30209556.15367.9011.9156.1567.9011.91
2427438-42743879.45179.45
3384517-38451771.47371.47
4365508-36550867.94067.94
5333115-33311561.91961.92
6378979-37897970.44470.44
10min1475877-47587788.45592.253.9988.5592.364.00
2511059-51105994.99495.13
3505259-50525993.91694.04
4507707-50770794.37194.48
5466493-46649386.71186.81
6511265-51126595.03395.15
15min1517450-51745096.18297.531.9296.4297.801.93
2528655-52865598.26598.56
3534662-53466299.38299.66
4533594-53359499.18399.45
5508611-50861194.53994.79
6525337-52533797.64897.92
20min1530673-53067398.64098.641.0999.0499.071.10
2533243-53324399.11899.57
3538019-538019100.006100.45
4533829-53382999.22799.66
5521826-52182696.99697.40
6526556-52655697.87598.31
30min1535822-53582299.59799.080.93100.1699.670.92
2534247-53424799.30599.92
3539801-539801100.337100.94
4533268-53326899.12399.72
5529233-52923398.37398.94
6525863-52586397.74698.35
45min1535242-53524299.49099.010.93100.2299.770.93
2533971-53397199.253100.04
3539495-539495100.280101.06
4532858-53285899.04699.81
5528823-52882398.29699.03
6525535-52553597.68598.45
60min1529292-52929298.38498.760.9099.2899.690.91
2533808-53380899.223100.17
3538871-538871100.164101.11
4532117-53211798.90999.84
5528845-52884598.30199.20
6525026-52502697.59198.52
极限1534516-53451699.35599.150.68100.42100.240.68
2534401-53440199.333100.45
3537799-53779999.965101.07
4534065-53406599.271100.37
5532705-53270599.018100.08
6526871-52687197.93499.02
氢氯噻嗪坎地沙坦酯片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100685-201903对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.521531951537361536571535051533691534920.15
216.491538711535711537210.14
单位质量响应值RSD%判断
9291.289322.070.24数据可信
加速6月-供试品溶液-2024082321批-坎地沙坦酯-pH4.5
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
10min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
15min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
20min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
30min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
45min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
60min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
极限1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
氢氯噻嗪坎地沙坦酯片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100309-202205对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.7对照品水分(%)0对照品稀释倍数1000
标示量(mg)12.5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
112.014625654626194626124626484629564626800.04
212.064611024610074610540.02
单位质量响应值RSD%判断
38524.5638230.020.55数据可信
加速6月-供试品溶液-2024082321批-氢氯噻嗪-pH4.5
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1390752-39075273.09167.608.1973.0967.608.19
2346103-34610364.73964.74
3311790-31179058.32158.32
4358262-35826267.01367.01
5375159-37515970.17470.17
6386214-38621472.24272.24
10min1511325-51132595.64493.893.3395.7794.003.33
2491518-49151891.93992.05
3474172-47417288.69488.79
4511854-51185495.74395.85
5502793-50279394.04894.16
6519957-51995797.25897.38
15min1540136-540136101.03399.691.45101.3199.961.45
2527785-52778598.72398.98
3521142-52114297.48097.73
4540253-540253101.055101.33
5530957-53095799.31699.59
6537434-537434100.528100.81
20min1544972-544972101.937100.511.20102.39100.941.21
2537550-537550100.549100.97
3527269-52726998.62699.03
4543232-543232101.612102.05
5533731-53373199.835100.27
6537341-537341100.510100.96
30min1544453-544453101.840100.481.22102.46101.081.22
2538578-538578100.741101.33
3527348-52734898.64199.21
4543419-543419101.647102.26
5532656-53265699.634100.24
6536499-536499100.353100.97
45min1545459-545459102.029100.341.29102.82101.111.30
2537513-537513100.542101.30
3526587-52658798.49999.23
4542368-542368101.450102.23
5531633-53163399.442100.21
6535182-535182100.106100.89
60min1542725-542725101.51799.961.33102.48100.901.34
2536062-536062100.271101.20
3524691-52469198.14499.04
4540973-540973101.189102.14
5528037-52803798.77099.71
6533839-53383999.855100.81
极限1542625-542625101.49899.781.33102.63100.891.33
2534672-534672100.011101.11
3523182-52318297.86298.93
4539282-539282100.873101.99
5528627-52862798.88099.98
6532291-53229199.565100.68
氢氯噻嗪坎地沙坦酯片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100685-201903对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.521535731535841536841535491538191536420.08
216.491531941533081532510.06
单位质量响应值RSD%判断
9300.369293.570.06数据可信
加速6月-供试品溶液-2024082321批-坎地沙坦酯-pH4.5
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
10min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
15min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
20min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
30min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
45min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
60min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
极限1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
氢氯噻嗪坎地沙坦酯片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100309-202205对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.7对照品水分(%)0对照品稀释倍数1000
标示量(mg)12.5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
112.014608384613634617954617124613804614180.09
212.064588734589544589140.02
单位质量响应值RSD%判断
38419.4838052.570.68数据可信
加速6月-供试品溶液-2024082521批-氢氯噻嗪-pH4.5
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1348914-34891465.50659.028.3765.5159.028.37
2299258-29925856.18456.18
3289100-28910054.27754.28
4288971-28897154.25254.25
5318531-31853159.80259.80
6341452-34145264.10564.11
10min1496975-49697593.30487.344.2093.4187.444.20
2442436-44243683.06483.16
3462365-46236586.80686.90
4448563-44856384.21584.31
5466598-46659887.60187.70
6474444-47444489.07489.18
15min1534321-534321100.31597.951.81100.5898.191.81
2515974-51597496.87197.10
3526023-52602398.75798.99
4510069-51006995.76295.99
5528950-52895099.30799.55
6515024-51502496.69296.95
20min1538759-538759101.148100.870.95101.58101.280.94
2538586-538586101.116101.51
3542770-542770101.902102.30
4536513-536513100.727101.12
5539342-539342101.258101.67
6527816-52781699.09499.51
30min1541395-541395101.643101.611.04102.24102.181.03
2542910-542910101.928102.49
3547523-547523102.794103.36
4541319-541319101.629102.19
5543363-543363102.013102.59
6530714-53071499.638100.22
45min1540817-540817101.535101.471.12102.30102.211.11
2542325-542325101.818102.55
3547094-547094102.713103.45
4541308-541308101.627102.35
5542176-542176101.790102.54
6529047-52904799.325100.07
60min1540093-540093101.399101.271.15102.34102.181.14
2541304-541304101.626102.53
3545976-545976102.503103.42
4539795-539795101.343102.24
5541526-541526101.668102.59
6527649-52764999.06399.98
极限1540525-540525101.480101.181.14102.59102.261.13
2543133-543133101.970103.04
3545118-545118102.342103.43
4538168-538168101.038102.10
5538894-538894101.174102.26
6527654-52765499.064100.14
氢氯噻嗪坎地沙坦酯片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100685-201903对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.521534551535141537621538261535931536300.11
216.491529301527461528380.09
单位质量响应值RSD%判断
9299.649268.530.24数据可信
加速6月-供试品溶液-2024082521批-坎地沙坦酯-pH4.5
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
10min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
15min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
20min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
30min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
45min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
60min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
极限1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
氢氯噻嗪坎地沙坦酯片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100309-202205对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.7对照品水分(%)0对照品稀释倍数1000
标示量(mg)12.5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
112.014585004585404591284595474601054591640.15
212.064568874572924570900.07
单位质量响应值RSD%判断
38231.8137901.330.62数据可信
加速6月-供试品溶液-2024082521批-氢氯噻嗪-pH4.5
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1297730-29773056.14557.687.1956.1557.687.19
2269005-26900550.72950.73
3300991-30099156.76056.76
4328827-32882762.01062.01
5313400-31340059.10059.10
6325382-32538261.36061.36
10min1450610-45061084.97586.265.5085.0786.355.50
2413914-41391478.05578.14
3451168-45116885.08185.18
4485053-48505391.47191.57
5473408-47340889.27589.37
6470284-47028488.68588.79
15min1507726-50772695.74697.342.3695.9897.582.37
2495339-49533993.41093.62
3522390-52239098.51298.75
4525253-52525399.05199.31
5520332-52033298.12398.37
6525949-52594999.18399.43
20min1521454-52145498.335100.641.2698.73101.041.27
2530937-530937100.123100.49
3535955-535955101.070101.47
4539363-539363101.712102.13
5535605-535605101.004101.41
6538900-538900101.625102.04
30min1530627-530627100.065101.560.78100.62102.130.79
2538053-538053101.465102.00
3538684-538684101.584102.15
4541733-541733102.159102.75
5540182-540182101.867102.45
6542032-542032102.216102.80
45min1530963-530963100.128101.480.72100.85102.220.73
2537277-537277101.319102.03
3538852-538852101.616102.35
4541207-541207102.060102.82
5538934-538934101.631102.38
6541440-541440102.104102.86
60min1530392-530392100.021101.310.68100.91102.210.69
2536526-536526101.177102.05
3537315-537315101.326102.23
4539728-539728101.781102.71
5539626-539626101.762102.68
6539677-539677101.771102.70
极限1529129-52912999.782101.020.68100.84102.100.69
2536433-536433101.160102.20
3536571-536571101.186102.26
4536916-536916101.251102.35
5535001-535001100.890101.98
6540147-540147101.860102.96
氢氯噻嗪坎地沙坦酯片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100685-201903对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.521531821532481530031533991536211532910.16
216.491523961529081526520.24
单位质量响应值RSD%判断
9279.129257.250.17数据可信
加速6月-供试品溶液-2024082521批-坎地沙坦酯-pH4.5
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
10min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
15min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
20min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
30min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
45min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
60min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
极限1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
点击查看处理图标(自动生成)
 
原始图谱下载图谱(谢鑫慧 于 2025-03-26 14:28:34 完成)
生成报告数据部分(等待生成报告)
Current page cost:1.747 s