他克莫司颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号D230603FK对照品来源自制对照品使用方法直接使用
对照品含量(%)97.04对照品水分(%)0对照品稀释倍数17500
标示量(mg)1供试品稀释倍数1.4系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.031571771573171572441572741573091572640.04
214.081566981562051564520.23
单位质量响应值RSD%判断
11209.1211111.650.62数据可信
供试品溶液-2025032622批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min152123-5212332.63230.3210.2332.6330.3210.23
253102-5310233.24533.24
349154-4915430.77330.77
450787-5078731.79531.80
545542-4554228.51228.51
639902-3990224.98124.98
10min184775-8477553.07452.807.3153.4453.147.32
293341-9334158.43758.81
384946-8494653.18153.52
486273-8627354.01254.36
582392-8239251.58251.90
674306-7430646.52046.80
15min1104389-10438965.35361.476.7566.3162.406.77
2106521-10652166.68867.71
396109-9610960.17061.10
498305-9830561.54462.50
595632-9563259.87160.76
688164-8816455.19555.99
20min1110830-11083069.38666.327.0471.0667.927.05
2115076-11507672.04473.80
3105757-10575766.21067.81
4108757-10875768.08869.73
5100959-10095963.20664.76
694207-9420758.97960.39
30min1120250-12025075.28374.077.6677.7376.417.64
2132688-13268883.07085.63
3119863-11986375.04177.38
4117596-11759673.62276.02
5114709-11470971.81474.07
6104741-10474165.57467.64
45min1133767-13376783.74581.475.9087.0384.645.95
2138699-13869986.83390.32
3130994-13099482.00985.18
4133705-13370583.70786.92
5127160-12716079.60982.66
6116515-11651572.94575.74
60min1135379-13537984.75582.866.0888.9786.936.09
2142216-14221689.03593.48
3137662-13766286.18490.27
4129223-12922380.90185.04
5130466-13046681.67985.62
6119126-11912674.57978.18
90min1149765-14976593.76187.647.8898.9292.647.81
2152737-15273795.622101.06
3140265-14026587.81492.85
4140291-14029187.83092.87
5134871-13487184.43789.28
6122026-12202676.39580.83
极限1144102-14410290.21687.036.8296.4293.006.82
2152139-15213995.247101.75
3140971-14097188.25694.27
4139644-13964487.42593.44
5132541-13254182.97888.76
6124722-12472278.08383.36
他克莫司颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号D230603FK对照品来源自制对照品使用方法直接使用
对照品含量(%)97.04对照品水分(%)0对照品稀释倍数17500
标示量(mg)1供试品稀释倍数1.4系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.031590771584561588411590531589441588740.16
214.081581271586781584020.25
单位质量响应值RSD%判断
11323.8811250.140.47数据可信
供试品溶液-2025032622批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min160564-6056437.49133.588.6837.4933.588.68
259636-5963636.91636.92
350187-5018731.06731.07
451703-5170332.00632.01
553412-5341233.06333.06
649990-4999030.94530.95
10min192913-9291357.51659.393.2957.9359.763.27
299469-9946961.57461.98
391439-9143956.60356.95
496317-9631759.62359.98
596970-9697060.02760.39
698522-9852260.98861.33
15min198352-9835260.88266.645.3961.9467.675.30
2111395-11139568.95670.05
3106022-10602265.63066.60
4112507-11250769.64570.66
5104447-10444764.65565.69
6113196-11319670.07171.09
20min1110215-11021568.22671.773.9669.9673.543.94
2121662-12166275.31277.17
3110640-11064068.48970.19
4117868-11786872.96374.76
5116569-11656972.15973.91
6118694-11869473.47575.27
30min1132623-13262382.09780.873.0284.5983.442.99
2132939-13293982.29384.99
3123131-12313176.22178.69
4133863-13386382.86585.47
5129824-12982480.36482.92
6131462-13146281.37883.99
45min1137804-13780485.30486.733.4388.7190.203.39
2142324-14232488.10291.71
3132908-13290882.27485.58
4147265-14726591.16194.68
5141126-14112687.36190.81
6139192-13919286.16389.68
60min1140790-14079087.15388.142.2891.5092.572.24
2144573-14457389.49494.09
3138819-13881985.93390.16
4138932-13893286.00390.54
5145413-14541390.01494.43
6145744-14574490.21994.70
90min1139963-13996386.64190.612.4591.9696.022.42
2149668-14966892.64898.23
3144770-14477089.61694.80
4147735-14773591.45296.94
5147067-14706791.03896.46
6149065-14906592.27597.76
极限1141818-14181887.78990.142.6694.0796.562.64
2149563-14956392.58399.20
3140342-14034286.87593.05
4145129-14512989.83996.35
5147725-14772591.44697.88
6149117-14911792.30798.81
点击查看处理图标(人工保存)
　
原始图谱下载图谱(谢超君 于 2025-04-12 15:04:10 完成)
生成报告数据部分下载报告(谢超君 于 2025-04-12 15:04:29 完成)
Current page cost:76 ms