玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 11.211008511006171008481009441006271007770.15
2 11.201004231010261007240.43
单位质量响应值RSD%判断
8989.928993.210.03数据可信
加速3月-供试品溶液-SF1批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min175462-7546275.35966.6310.9875.3666.6310.98
259299-5929959.21859.22
362297-6229762.21262.21
469836-6983669.74169.74
10min168328-6832868.23575.3413.4668.6575.7113.38
268281-6828168.18868.52
389833-8983389.71090.06
475316-7531675.21375.60
15min176484-7648476.38080.933.7977.1881.723.75
282492-8249282.37983.09
383095-8309582.98283.83
482074-8207481.96282.77
20min195103-9510394.97388.505.6796.2089.745.60
283314-8331483.20084.37
386500-8650086.38287.69
489550-8955089.42890.69
30min189720-8972089.59891.182.1491.3592.912.13
290595-9059590.47192.10
394142-9414294.01495.80
490770-9077090.64692.40
45min191191-9119191.06792.591.7993.3194.831.81
291460-9146091.33593.47
394578-9457894.44996.76
493633-9363393.50595.77
60min195606-9560695.47695.750.7798.2398.500.81
295438-9543895.30897.95
396970-9697096.83899.67
495491-9549195.36198.14
极限195144-9514495.01495.520.4298.3098.800.39
296058-9605895.92799.09
395865-9586595.73499.10
495541-9554195.41198.72
玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 11.211013161011841015061013571012841013290.12
2 11.201006491008841007660.17
单位质量响应值RSD%判断
9039.168996.960.34数据可信
加速3月-供试品溶液-SF1批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min185515-8551585.14886.742.5685.1586.742.56
290378-9037889.99089.99
386671-8667186.29986.30
485890-8589085.52185.52
10min192070-9207091.67590.841.8292.1591.321.81
292529-9252992.13292.63
391479-9147991.08691.57
488835-8883588.45488.93
15min193792-9379293.38991.792.3494.3792.782.32
294246-9424693.84194.85
390753-9075390.36391.35
489956-8995689.57090.54
20min191648-9164891.25591.381.2992.7692.881.28
292978-9297892.57994.11
390203-9020389.81691.30
492262-9226291.86693.33
30min192500-9250092.10391.031.1694.1193.041.16
292152-9215291.75693.80
390354-9035489.96691.95
490692-9069290.30392.28
45min192806-9280692.40890.512.2594.9393.022.23
292512-9251292.11594.67
389339-8933988.95591.44
488936-8893688.55491.03
60min191100-9110090.70989.272.5593.7492.282.52
292094-9209491.69994.77
387931-8793187.55490.53
487500-8750087.12490.09
极限191936-9193691.54191.020.9995.0894.531.02
292396-9239691.99995.58
390835-9083590.44593.91
490482-9048290.09493.55
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