坎地沙坦酯氢氯噻嗪片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100309-201404对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.7对照品水分(%)0对照品稀释倍数1000
标示量(mg)12.5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.574376674382154379824388354386984382790.12
211.604382244386484384360.07
单位质量响应值RSD%判断
37880.6437796.210.16数据可信
供试品溶液-24032701批-pH6.8(内含0.35%吐温20)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1298946-29894656.71463.8020.7456.7163.8020.75
2425833-42583380.78680.79
3337494-33749464.02764.03
4230848-23084843.79543.79
5327421-32742162.11662.12
6397127-39712775.34075.34
10min1423309-42330980.30784.038.5680.4084.148.57
2483617-48361791.74891.88
3439911-43991183.45683.56
4380152-38015272.11972.19
5455926-45592686.49586.60
6474760-47476090.06890.19
15min1451462-45146285.64889.414.1485.8889.664.16
2492913-49291393.51293.80
3472310-47231089.60389.85
4444997-44499784.42184.61
5477287-47728790.54790.79
6488865-48886592.74493.02
20min1465263-46526388.26691.822.5288.6492.222.55
2496775-49677594.24494.69
3485867-48586792.17592.57
4473558-47355889.84090.17
5489173-48917392.80293.20
6493470-49347093.61794.05
30min1478194-47819490.71993.971.8791.2494.521.88
2501430-50143095.12795.73
3500891-50089195.02595.57
4495431-49543193.98994.47
5493058-49305893.53994.09
6502953-50295395.41696.00
45min1489258-48925892.81895.701.6693.4996.401.66
2505868-50586895.96996.73
3511236-51123696.98897.69
4508771-50877196.52097.16
5500880-50088095.02395.73
6510658-51065896.87897.62
60min1495796-49579694.05996.561.6394.8897.421.62
2506477-50647796.08597.00
3517536-51753698.18399.05
4514460-51446097.59998.40
5504461-50446195.70296.57
6515032-51503297.70898.61
极限1530814-530814100.702101.880.57101.68102.900.59
2537900-537900102.046103.13
3538463-538463102.153103.19
4538578-538578102.175103.14
5538461-538461102.153103.18
6537839-537839102.035103.10
坎地沙坦酯氢氯噻嗪片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100309-201404对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.7对照品水分(%)0对照品稀释倍数1000
标示量(mg)12.5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.574389284390944392834390324391214390920.03
211.604379234380724379980.03
单位质量响应值RSD%判断
37950.9137758.450.36数据可信
供试品溶液-24032702批-pH6.8(内含0.35%吐温20)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1289573-28957354.91250.9812.0954.9150.9812.09
2276036-27603652.34552.35
3292675-29267555.50055.50
4236665-23666544.87944.88
5297804-29780456.47356.47
6220304-22030441.77741.78
10min1440831-44083183.59678.954.6383.6979.034.64
2423884-42388480.38280.47
3427532-42753281.07481.17
4390375-39037574.02774.10
5418789-41878979.41679.51
6396465-39646575.18275.25
15min1457550-45755086.76684.853.0387.0085.073.04
2448138-44813884.98185.20
3459919-45991987.21587.44
4434208-43420882.34082.54
5457170-45717086.69486.92
6427803-42780381.12581.32
20min1465818-46581888.33487.402.4788.7187.752.48
2467174-46717488.59188.95
3469852-46985289.09989.47
4454893-45489386.26286.60
5467265-46726588.60888.98
6440238-44023883.48383.81
30min1479127-47912790.85890.412.1091.3890.912.11
2478010-47801090.64691.16
3483541-48354191.69592.22
4479294-47929490.88991.37
5483581-48358191.70292.22
6456963-45696386.65587.12
45min1492293-49229393.35493.482.0394.0394.142.04
2496795-49679594.20894.87
3498818-49881894.59295.27
4497192-49719294.28394.91
5499473-49947394.71695.39
6473189-47318989.73290.35
60min1502777-50277795.34295.462.1196.1796.272.11
2510138-51013896.73897.56
3507733-50773396.28297.11
4505264-50526495.81496.60
5511645-51164597.02497.85
6482811-48281191.55692.32
极限1520733-52073398.747100.681.4999.74101.651.49
2538750-538750102.164103.14
3537527-537527101.932102.92
4529632-529632100.435101.38
5536544-536544101.746102.74
6522516-52251699.086100.00
点击查看处理图标(自动生成)
　
原始图谱下载图谱(谢超君 于 2024-04-01 19:03:18 完成)
生成报告数据部分(等待生成报告)
Current page cost:62 ms