多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数5000
标示量(mg)2供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.086517565095652506509065354651930.18
2 10.056495165365651580.45
单位质量响应值RSD%判断
6467.566483.380.18数据可信
供试品溶液-25041501批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min153404-5340473.99473.057.3773.9973.047.37
255461-5546176.84476.84
354523-5452375.54575.54
454350-5435075.30575.30
553644-5364474.32774.33
644937-4493762.26362.26
10min164575-6457589.47289.252.4189.6089.372.41
266406-6640692.00992.14
364924-6492489.95690.08
465079-6507990.17090.30
563675-6367588.22588.35
661820-6182085.65585.76
15min166909-6690992.70693.250.8292.9893.520.82
268405-6840594.77995.06
367210-6721093.12393.40
467116-6711692.99393.27
567120-6712092.99893.27
667061-6706192.91793.16
20min168257-6825794.57494.980.7295.0095.400.71
268983-6898395.58096.02
369091-6909195.72996.16
467990-6799094.20494.63
568102-6810294.35994.78
668878-6887895.43495.84
30min168987-6898795.58596.730.9896.1797.310.98
270298-7029897.40298.00
370056-7005697.06697.66
469478-6947896.26696.85
569265-6926595.97096.55
670785-7078598.07698.64
45min170134-7013497.17497.680.5597.9298.420.55
270891-7089198.22398.98
370849-7084998.16598.92
470230-7023097.30798.06
570082-7008297.10297.85
670796-7079698.09298.82
60min170773-7077398.06098.410.5198.9799.320.51
271317-7131798.81499.74
371530-7153099.109100.02
470587-7058797.80298.71
570843-7084398.15799.06
671090-7109098.49999.39
极限171729-7172999.38499.500.62100.45100.580.62
271799-7179999.481100.57
372495-72495100.446101.53
471874-7187499.585100.66
571111-7111198.52899.60
671877-7187799.589100.64
多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数5000
标示量(mg)2供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.086504265150651106521264988651000.14
2 10.056591065767658380.16
单位质量响应值RSD%判断
6458.336551.041.01数据可信
供试品溶液-25041801批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min144888-4488861.91864.524.0961.9264.524.09
247568-4756865.61565.62
346651-4665164.35064.35
446010-4601063.46663.47
545373-4537362.58762.59
650167-5016769.20069.20
10min160499-6049983.45285.631.5483.5685.741.54
262840-6284086.68186.79
362320-6232085.96486.07
461619-6161984.99785.10
562032-6203285.56785.67
663170-6317087.13787.25
15min166130-6613091.22092.140.8891.4692.390.88
267409-6740992.98493.24
367594-6759493.23993.49
466410-6641091.60691.85
566766-6676692.09792.34
666470-6647091.68991.95
20min167602-6760293.25094.200.8993.6494.600.89
269058-6905895.25895.67
368680-6868094.73795.14
468458-6845894.43194.83
568410-6841094.36594.77
667538-6753893.16293.58
30min169088-6908895.30095.720.8395.8596.280.83
269761-6976196.22896.80
369766-6976696.23596.80
469915-6991596.44197.00
569438-6943895.78396.34
668394-6839494.34394.91
45min169402-6940295.73396.500.8596.4497.220.84
270231-7023196.87797.60
370292-7029296.96197.68
470628-7062897.42498.14
570114-7011496.71597.43
669073-6907395.27996.01
60min170121-7012196.72597.300.7297.5998.180.72
270491-7049197.23598.12
371082-7108298.05098.94
471093-7109398.06698.95
570590-7059097.37298.25
669841-6984196.33997.22
极限170421-7042197.13998.180.8898.1799.230.88
271390-7139098.47599.53
371390-7139098.47599.52
471945-7194599.241100.28
571516-7151698.64999.69
670408-7040897.12198.17
多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数5000
标示量(mg)2供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.086530065658653916575465814655830.35
2 10.056618266290662360.12
单位质量响应值RSD%判断
6506.256590.650.92数据可信
供试品溶液-25041802批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min139906-3990654.67864.1713.2354.6864.1713.23
252872-5287272.44472.44
350793-5079369.59569.59
450553-5055369.26669.27
548659-4865966.67166.67
638206-3820652.34952.35
10min159395-5939581.38185.224.6081.4785.324.61
265041-6504189.11789.24
363716-6371687.30287.42
463348-6334886.79786.91
563797-6379787.41387.52
657869-5786979.29079.38
15min164955-6495588.99990.942.3989.2391.192.40
268231-6823193.48893.76
367010-6701091.81592.08
467406-6740692.35892.62
566594-6659491.24591.50
664021-6402187.72087.94
20min167734-6773492.80793.251.5893.1893.651.59
269435-6943595.13895.56
368669-6866994.08894.50
468259-6825993.52693.94
568020-6802093.19993.61
666235-6623590.75391.12
30min169712-6971295.51794.951.1696.0595.511.17
270295-7029596.31696.90
369683-6968395.47796.05
469085-6908594.65895.23
569044-6904494.60295.17
667973-6797393.13493.65
45min170694-7069496.86396.150.8497.5596.870.85
270884-7088497.12397.87
370332-7033296.36797.10
469831-6983195.68096.41
570009-7000995.92496.65
669305-6930594.95995.63
60min170734-7073496.91796.650.5197.7797.530.50
271060-7106097.36498.27
370339-7033996.37697.27
470091-7009196.03696.92
570310-7031096.33697.22
670709-7070996.88397.71
极限171456-7145697.90797.270.7598.9298.300.75
271687-7168798.22399.29
371181-7118197.53098.58
470422-7042296.49097.54
570684-7068496.84997.89
670506-7050696.60597.60
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