多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数5000
标示量(mg)2供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.083306232746328043276233001328750.45
210.053314332879330110.57
单位质量响应值RSD%判断
3261.413284.680.51数据可信
供试品溶液-25041502批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min124090-2409066.03767.248.8966.0467.248.89
226125-2612571.61571.62
327965-2796576.65976.66
424030-2403065.87265.87
522990-2299063.02163.02
621964-2196460.20960.21
10min132520-3252089.14587.313.6189.2687.423.62
232428-3242888.89389.01
333294-3329491.26791.39
431345-3134585.92486.03
531510-3151086.37786.48
630016-3001682.28182.38
15min134348-3434894.15693.641.0494.4193.891.05
234261-3426193.91894.19
334427-3442794.37394.65
433716-3371692.42492.68
534490-3449094.54694.79
633710-3371092.40792.64
20min134682-3468295.07295.280.5595.4995.690.54
234678-3467895.06195.48
334815-3481595.43695.87
434464-3446494.47494.88
534991-3499195.91996.33
634908-3490895.69196.08
30min136497-36497100.04797.621.47100.6298.191.45
235146-3514696.34496.93
335252-3525296.63497.23
435220-3522096.54797.11
535679-3567997.80598.37
635875-3587598.34298.89
45min135724-3572497.92897.740.7698.6798.480.75
235148-3514896.34997.09
335661-3566197.75698.51
435758-3575898.02198.75
535685-3568597.82198.55
635958-3595898.57099.28
60min136054-3605498.83398.670.8699.7499.570.85
235510-3551097.34298.25
336316-3631699.551100.47
435947-3594798.54099.43
535822-3582298.19799.09
636313-3631399.543100.42
极限136411-3641199.81199.610.39100.88100.680.39
236108-3610898.981100.05
336456-3645699.935101.02
436469-3646999.970101.02
536234-3623499.326100.38
636357-3635799.663100.71
多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数5000
标示量(mg)2供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.083262332863326993304432691327840.52
210.053287132974329220.23
单位质量响应值RSD%判断
3252.383275.820.51数据可信
供试品溶液-25041901批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min120920-2092057.50460.248.2457.5060.248.24
223440-2344064.43164.43
324247-2424766.64966.65
419237-1923752.87852.88
521408-2140858.84558.85
622244-2224461.14361.14
10min130560-3056084.00283.003.3484.1083.103.34
230215-3021583.05483.16
331596-3159686.85086.96
428628-2862878.69178.78
529596-2959681.35281.45
630586-3058684.07384.18
15min133159-3315991.14690.601.7891.3890.841.79
233141-3314191.09791.34
333533-3353392.17492.43
431850-3185087.54887.77
532856-3285690.31390.55
633218-3321891.30891.55
20min134489-3448994.80293.971.2095.1994.361.20
234153-3415393.87894.28
334332-3433294.37094.78
433390-3339091.78192.15
534286-3428694.24494.63
634460-3446094.72295.12
30min135281-3528196.97996.330.8897.5296.880.88
234900-3490095.93296.49
335142-3514296.59797.16
434504-3450494.84395.36
535338-3533897.13697.68
635104-3510496.49297.04
45min135296-3529697.02097.540.8197.7398.250.81
235661-3566198.02398.74
335486-3548697.54298.27
435016-3501696.25096.93
535750-3575098.26898.97
635701-3570198.13398.85
60min135802-3580298.41197.810.9299.2898.680.92
235250-3525096.89497.77
335840-3584098.51599.41
435184-3518496.71297.55
535477-3547797.51898.38
635948-3594898.81299.69
极限136115-3611599.27198.820.97100.3099.850.97
235793-3579398.38699.43
336333-3633399.871100.93
435355-3535597.18298.18
536160-3616099.395100.42
635944-3594498.80199.84
多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数5000
标示量(mg)2供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.083352033380331363346933170333350.53
210.053271832793327560.17
单位质量响应值RSD%判断
3307.043259.301.03数据可信
供试品溶液-25041902批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min127320-2732074.66368.398.7774.6668.398.77
226540-2654072.53172.53
325441-2544169.52869.53
423425-2342564.01864.02
525978-2597870.99571.00
621444-2144458.60458.60
10min132191-3219187.97587.001.6988.1087.111.70
232559-3255988.98089.10
331764-3176486.80886.92
431522-3152286.14686.25
531951-3195187.31987.44
631017-3101784.76684.86
15min133162-3316290.62892.121.0290.9092.381.02
234133-3413393.28293.55
333750-3375092.23592.50
433730-3373092.18192.43
533962-3396292.81593.08
633509-3350991.57791.82
20min133823-3382392.43594.201.0492.8694.621.02
234545-3454594.40894.83
334351-3435193.87894.29
434842-3484295.22095.62
534573-3457394.48494.90
634689-3468994.80195.19
30min134183-3418393.41995.591.2593.9996.161.24
234990-3499095.62496.21
335021-3502195.70996.28
435457-3545796.90097.46
535264-3526496.37396.95
634954-3495495.52696.08
45min134594-3459494.54296.571.0895.2797.301.07
235444-3544496.86597.61
335335-3533596.56797.30
435612-3561297.32498.05
535430-3543096.82797.56
635608-3560897.31398.02
60min134909-3490995.40397.220.9996.2998.110.98
235655-3565597.44198.34
335645-3564597.41498.31
435662-3566297.46198.35
535618-3561897.34098.24
635957-3595798.26799.14
极限134603-3460394.56697.761.6495.6198.811.62
235830-3583097.92098.98
336099-3609998.65599.71
435895-3589598.09799.15
536055-3605598.53599.59
636142-3614298.77299.81
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