类型试验信息(多次测定用,隔开)图谱读取备注
项目代号:已存用户保存
项目名称:已存用户保存
试验名称可缺:待存默认值
时间点可缺:待存默认值
图谱类型:已存HPLC用户保存
样品类型:已存自制品,自制品,自制品用户保存
批号:已存20250401批,20250401批,20250401批用户保存
规格可缺:待存40mg规格,40mg规格,40mg规格图谱读取
介质名称:已存shui(内含0.2%SDS),pH4.5(内含0.5%SDS),pH1.0(内含0.5%SDS)用户保存
方法名称可缺:已存用户保存
转速可缺:已存用户保存
组成图标非布司他片溶出曲线测定HPLC图谱
自制品-20250401批批()-shui(内含0.2%SDS)-桨法-50转
注1:成分名称多个峰按出峰顺序【,】(半角逗号)隔开;
注2:试验批号和介质名称都一样的填一个;有任何不一致的需要【,】(半角逗号)隔开填写波数个;
注3:特别注意:批号和规格必须存在;
编号5355
项目名称非布司他片
选择方法
峰的筛选AUTO
根据对照品保留时间的0.95~1.05进行筛选;
对照品图谱务必只出主成分峰;
测定类型溶出
成分(个数)
成分名称
进样针数1针　2针
双波长
溶出度
图谱类型
制剂单位
谢超君2025-04-30 16:46:20进行了保存!
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既往测定情况概览
编号 试验名称 介质体积 取样体积 补液体积 R批号 R来源 R使用方法 R含量(%) R水分(%) R稀释 R标示量(mg) T稀释 操作
5356 900 1.5 1.5 101278-202104 中检院 直接使用 100.0 0 250 40 1 使用
5355 900 1.5 1.5 101278-202104 中检院 直接使用 100.0 0 250 40 1 本法
5302 900 1.5 1.5 101278-202104 中检院 直接使用 100.0 0 250 40 1 使用
5301 900 1.5 1.5 101278-202104 中检院 直接使用 100.0 0 250 40 1 使用
5288 900 1.5 1.5 101278-202104 中检院 直接使用 100.0 0 500 20 1 使用
5287 900 1.5 1.5 101278-202104 中检院 直接使用 100.0 0 500 20 1 使用
84 稳定性考察 1000,1000 2,2 2,20 S2561,x1252 中检院,中检院 直接使用,直接使用 100,100 0,0 1000,1000 10,25 1,1 使用
注意:::正在使用与其他方法的参数!恢复
【 非布司他 】信息
介质体积(ml)取样体积(ml)补液体积(ml)
对照品批号对照品来源对照品使用方法
对照品含量(%)对照品水分(%)对照品稀释倍数
标示量(mg)供试品稀释倍数系数
称样量1(mg)称样量2(mg)
谢超君2025-04-30 16:46:29进行了保存!
类型波数成分响应值RSD%
审阅状态N
审阅权限孙文新,谢鑫慧,王丹,姜进硙,邵涛明
供试品测定波数:::3次
供试品测定片数:::6片
供试品取样点数:::5min,10min,15min,20min,30min,45min,60min,极限;
对照品的峰个数:::1个峰
图谱最多峰个数:::1个峰
对照品保留时间:::4.044
对照品　峰面积:::3934157
待处理PDF文件:::查阅
筛选规则为:::自动
图谱张数为:::168
2025-04-30 16:46:34谢超君进行了保存!
序号文件名溶液名称保留时间峰面积
1zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-rj无峰无面积1NA1
2zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-dz1-14.06939298881MA1
3zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-dz1-24.07039276921MA1
4zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-dz1-34.07039280571MA1
5zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-dz1-44.07139280931MA1
6zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-dz1-54.07139248441MA1
7zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p1-5min3.9464881891MA1
8zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p2-5min3.9314265831MA1
9zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p3-5min3.9249783001MA1
10zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p4-5min3.9302443701MA1
11zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p5-5min3.92411521471MA1
12zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p6-5min3.9275435651MA1
13zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p1-10min3.92511840541MA1
14zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p2-10min3.92411758471MA1
15zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p3-10min3.92121233091MA1
16zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p4-10min3.9208235201MA1
17zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p5-10min3.92222050021MA1
18zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p6-10min3.92313939911MA1
19zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p1-15min3.92413380391MA1
20zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p2-15min3.92616233111MA1
21zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p3-15min3.92124619121MA1
22zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p4-15min3.92411277651MA1
23zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p5-15min3.92122501631MA1
24zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p6-15min3.92317360781MA1
25zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p1-20min3.92514056921MA1
26zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p2-20min3.92317391321MA1
27zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p3-20min3.92124583481MA1
28zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p4-20min3.92413179451MA1
29zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p5-20min3.92321746491MA1
30zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p6-20min3.92417818301MA1
31zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p1-30min3.92514081301MA1
32zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p2-30min3.92417272051MA1
33zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p3-30min3.92323440291MA1
34zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p4-30min3.92514727211MA1
35zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p5-30min3.92319662691MA1
36zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p6-30min3.92417258681MA1
37zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p1-45min3.92514056901MA1
38zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p2-45min3.91616754371MA1
39zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p3-45min3.92421296581MA1
40zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p4-45min3.92415236261MA1
41zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p5-45min3.92517938991MA1
42zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p6-45min3.92316943121MA1
43zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p1-60min3.92513921971MA1
44zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p2-60min3.92516167921MA1
45zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p3-60min3.92220019461MA1
46zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p4-60min3.92515390161MA1
47zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p5-60min3.92416952211MA1
48zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p6-60min3.92415711961MA1
49zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p1-jxzs3.92613936651MA1
50zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p2-jxzs3.92415765361MA1
51zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p3-jxzs3.92419154141MA1
52zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p4-jxzs3.91915125831MA1
53zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p5-jxzs3.92416354881MA1
54zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-p6-jxzs3.92515641501MA1
55zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-dz2-13.96839885011MA1
56zzp-40mg-20250401p-rcqx-shui+0.2sdsjz-dz2-23.99939864041MA1
57zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-rj无峰无面积1NA1
58zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-dz1-14.04339266441MA1
59zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-dz1-24.04939215891MA1
60zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-dz1-34.06639328871MA1
61zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-dz1-44.07539301131MA1
62zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-dz1-54.08039274571MA1
63zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p1-5min3.8847220541MA1
64zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p2-5min3.8656945431MA1
65zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p3-5min3.8654927931MA1
66zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p4-5min3.86311638331MA1
67zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p5-5min3.8645153241MA1
68zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p6-5min3.8637172481MA1
69zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p1-10min3.86215381441MA1
70zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p2-10min3.86316482021MA1
71zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p3-10min3.86314009771MA1
72zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p4-10min3.86223354561MA1
73zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p5-10min3.86413083661MA1
74zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p6-10min3.86318178031MA1
75zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p1-15min3.86223579321MA1
76zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p2-15min3.86324595451MA1
77zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p3-15min3.86422993751MA1
78zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p4-15min3.86428706181MA1
79zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p5-15min3.86321119381MA1
80zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p6-15min3.86326455191MA1
81zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p1-20min3.86128568991MA1
82zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p2-20min3.86328930601MA1
83zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p3-20min3.86227872251MA1
84zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p4-20min3.86231223421MA1
85zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p5-20min3.86426468561MA1
86zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p6-20min3.86330345191MA1
87zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p1-30min3.86233053111MA1
88zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p2-30min3.86432869771MA1
89zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p3-30min3.86232654401MA1
90zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p4-30min3.86133672631MA1
91zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p5-30min3.86232262741MA1
92zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p6-30min3.86233525361MA1
93zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p1-45min3.86235880941MA1
94zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p2-45min3.86335561061MA1
95zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p3-45min3.86335739331MA1
96zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p4-45min3.86335871771MA1
97zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p5-45min3.86335843071MA1
98zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p6-45min3.86336061221MA1
99zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p1-60min3.86337446481MA1
100zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p2-60min3.86437072811MA1
101zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p3-60min3.86437274461MA1
102zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p4-60min3.86437165371MA1
103zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p5-60min3.86237497421MA1
104zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p6-60min3.86237471871MA1
105zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p1-jxzs3.86338666871MA1
106zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p2-jxzs3.86438256211MA1
107zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p3-jxzs3.86438560931MA1
108zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p4-jxzs3.86438306741MA1
109zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p5-jxzs3.86438855341MA1
110zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-p6-jxzs3.86338543291MA1
111zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-dz2-13.96139509221MA1
112zzp-40mg-20250401p-rcqx-pH4.5+0.5sdsjz-dz2-24.00339476571MA1
113zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-rj无峰无面积1NA1
114zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-dz1-14.04739204771MA1
115zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-dz1-24.06039241081MA1
116zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-dz1-34.07139260861MA1
117zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-dz1-44.07939261681MA1
118zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-dz1-54.08439290381MA1
119zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p1-5min3.92511719481MA1
120zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p2-5min3.9037945161MA1
121zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p3-5min3.9034772651MA1
122zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p4-5min3.89610663881MA1
123zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p5-5min3.9035758241MA1
124zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p6-5min3.9058824331MA1
125zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p1-10min3.90523091131MA1
126zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p2-10min3.90319700661MA1
127zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p3-10min3.90416551991MA1
128zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p4-10min3.90422495771MA1
129zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p5-10min3.90417669731MA1
130zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p6-10min3.90421192751MA1
131zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p1-15min3.90526935291MA1
132zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p2-15min3.90525851581MA1
133zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p3-15min3.90523398321MA1
134zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p4-15min3.90627030881MA1
135zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p5-15min3.90524901831MA1
136zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p6-15min3.90526371991MA1
137zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p1-20min3.90629218551MA1
138zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p2-20min3.90628645181MA1
139zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p3-20min3.90527247961MA1
140zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p4-20min3.90629260831MA1
141zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p5-20min3.90727887511MA1
142zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p6-20min3.90728876641MA1
143zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p1-30min3.90731869351MA1
144zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p2-30min3.90731811611MA1
145zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p3-30min3.90731324861MA1
146zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p4-30min3.90732053071MA1
147zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p5-30min3.90731443101MA1
148zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p6-30min3.90831609691MA1
149zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p1-45min3.90834180811MA1
150zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p2-45min3.90734264301MA1
151zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p3-45min3.90834355591MA1
152zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p4-45min3.90834506921MA1
153zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p5-45min3.90834304311MA1
154zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p6-45min3.90834028841MA1
155zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p1-60min3.90835616411MA1
156zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p2-60min3.90935787031MA1
157zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p3-60min3.90935997811MA1
158zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p4-60min3.90935908181MA1
159zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p5-60min3.90935895111MA1
160zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p6-60min3.90835471161MA1
161zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p1-jxzs3.90836958411MA1
162zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p2-jxzs3.90837221341MA1
163zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p3-jxzs3.90837523981MA1
164zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p4-jxzs3.90837248311MA1
165zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p5-jxzs3.90837467121MA1
166zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-p6-jxzs3.91036870631MA1
167zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-dz2-13.97239214951MA1
168zzp-40mg-20250401p-rcqx-pH1.0+0.5sdsjz-dz2-24.01939191691MA1
计算
Current page cost:305 ms