诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.953930265393251739320173934358393280739323930.04
29.943930517392911439298160.03
单位质量响应值RSD%判断
395215.38395353.720.03数据可信
供试品溶液-24032501批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1658359-65835914.93016.187.9814.9316.187.97
2712888-71288816.16616.17
3786021-78602117.82517.82
4770358-77035817.47017.47
5645431-64543114.63714.64
6708762-70876216.07316.07
10min11570982-157098235.62636.094.6335.6536.114.63
21597399-159739936.22536.25
31659109-165910937.62437.65
41682533-168253338.15538.18
51478310-147831033.52433.55
61559771-155977135.37135.40
15min12296724-229672452.08452.532.3852.1752.622.39
22298778-229877852.13052.22
32362682-236268253.57953.67
42403583-240358354.50754.60
52275175-227517551.59551.68
62261162-226116251.27751.36
20min12834343-283434364.27564.412.1064.4564.592.11
22811877-281187763.76663.94
32908818-290881865.96466.15
42914542-291454266.09466.28
52765441-276544162.71362.88
62806653-280665363.64763.82
30min13441186-344118678.03778.871.4378.3279.151.43
23409222-340922277.31277.59
33537099-353709980.21280.50
43529434-352943480.03880.33
53474645-347464578.79679.07
63475707-347570778.82079.10
45min13774514-377451485.59687.421.9886.0087.841.98
23746856-374685684.96985.38
33915804-391580488.80089.23
43863437-386343787.61288.04
53911530-391153088.70389.11
63917740-391774088.84489.25
60min13888866-388886688.18990.672.1188.7491.222.10
23900647-390064788.45689.01
34065232-406523292.18992.76
44000099-400009990.71291.28
54059152-405915292.05192.60
64074712-407471292.40492.96
极限14249013-424901396.35697.040.4397.0597.750.44
24291732-429173297.32598.02
34290364-429036497.29498.02
44269853-426985396.82997.55
54274641-427464196.93797.64
64298765-429876597.48598.20
诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.953934192393662339375253936891393828139367020.04
29.943940918394017539405460.02
单位质量响应值RSD%判断
395648.44396433.200.15数据可信
供试品溶液-24032502批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1943842-94384221.36319.206.1921.3619.206.18
2820579-82057918.57318.57
3850878-85087819.25919.26
4862292-86229219.51719.52
5797312-79731218.04618.05
6815801-81580118.46518.46
10min12086223-208622347.22044.303.4247.2644.343.43
21901556-190155643.04043.07
31927660-192766043.63143.66
41917001-191700143.39043.42
51964419-196441944.46344.49
61947348-194734844.07644.11
15min12922507-292250766.14862.992.7266.2663.102.72
22723711-272371161.64961.75
32733490-273349061.87061.97
42729747-272974761.78561.89
52791972-279197263.19463.30
62796278-279627863.29163.40
20min13500363-350036379.22776.082.4479.4576.292.44
23306303-330630374.83575.04
33318013-331801375.10075.31
43271253-327125374.04274.25
53391564-339156476.76576.97
63379694-337969476.49676.71
30min14155373-415537394.05390.462.0994.4190.802.10
23928430-392843088.91689.25
33962936-396293689.69790.03
43934588-393458889.05689.39
53999620-399962090.52890.87
64000127-400012790.53990.88
45min14395531-439553199.48997.191.48100.0097.681.48
24197630-419763095.00995.49
34278859-427885996.84897.33
44306015-430601597.46397.94
54293049-429304997.16997.66
64292079-429207997.14797.64
60min14422124-4422124100.09198.591.33100.7799.241.33
24270156-427015696.65197.29
34314376-431437697.65298.30
44403620-440362099.672100.31
54383471-438347199.21699.87
64340964-434096498.25498.90
极限14488802-4488802101.60099.281.88102.45100.091.88
24256301-425630196.33797.14
34351780-435178098.49899.31
44437593-4437593100.441101.25
54427747-4427747100.218101.03
64354752-435475298.56699.38
点击查看处理图标(自动生成)
　
原始图谱下载图谱(姜进硙 于 2024-04-07 20:17:52 完成)
生成报告数据部分(等待生成报告)
Current page cost:58 ms