诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.943927647392773639285053931023392900939287840.04
29.953922416392091339216640.03
单位质量响应值RSD%判断
395249.90394137.090.20数据可信
供试品溶液-24032501批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1435650-43565019.78815.9518.0419.7915.9518.05
2307752-30775213.97913.98
3314221-31422114.27314.27
4324451-32445114.73714.74
5428569-42856919.46719.47
6296642-29664213.47413.47
10min1906742-90674241.18736.027.4441.2236.057.45
2777250-77725035.30535.33
3765627-76562734.77734.80
4759018-75901834.47734.50
5803291-80329136.48836.52
6746363-74636333.90233.92
15min11256231-125623157.06151.855.4357.1651.945.44
21153864-115386452.41252.49
31128316-112831651.25151.33
41083723-108372349.22649.31
51133354-113335451.48051.57
61093536-109353649.67149.75
20min11500963-150096368.17862.714.5668.3762.884.56
21398497-139849763.52363.69
31338736-133873660.80960.98
41352151-135215161.41861.58
51352520-135252061.43561.61
61340733-134073360.90061.06
30min11772910-177291080.53077.643.6680.8477.913.66
21734095-173409578.76779.04
31622763-162276373.71073.98
41775535-177553580.65080.92
51692456-169245676.87677.16
61657294-165729475.27975.54
45min11962083-196208389.12385.752.9189.5786.162.92
21917059-191705987.07887.48
31802008-180200881.85282.24
41903556-190355686.46586.87
51887216-188721685.72286.13
61854819-185481984.25184.64
60min11988687-198868790.33189.471.9290.9290.021.92
21964579-196457989.23689.79
31905113-190511386.53587.06
41981638-198163890.01190.56
52017614-201761491.64592.20
61960328-196032889.04389.57
极限11994329-199432990.58891.271.1391.3391.971.12
21983105-198310590.07890.78
31992572-199257290.50891.18
42016869-201686991.61292.31
52040026-204002692.66393.37
62028934-202893492.16092.84
诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.943919446391801939182673916673391335339171520.06
29.953926915393049139287030.07
单位质量响应值RSD%判断
394079.68394844.520.14数据可信
供试品溶液-24032502批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1326640-32664014.84614.557.6414.8514.547.63
2285369-28536912.97012.97
3350291-35029115.92015.92
4296350-29635013.46913.47
5326799-32679914.85314.85
6334765-33476515.21515.21
10min1711332-71133232.33033.136.4432.3533.156.44
2710187-71018732.27732.30
3773604-77360435.16035.19
4651738-65173829.62129.64
5766311-76631134.82834.85
6760315-76031534.55634.58
15min11052861-105286147.85248.011.7347.9348.081.73
21035495-103549547.06247.14
31077369-107736948.96649.05
41049070-104907047.67947.75
51043182-104318247.41247.49
61079610-107961049.06749.15
20min11250307-125030756.82658.251.8456.9858.401.84
21269338-126933857.69057.84
31308454-130845459.46859.64
41263696-126369657.43457.59
51298540-129854059.01859.18
61299014-129901459.03959.20
30min11610195-161019573.18272.271.3273.4472.521.32
21556579-155657970.74571.00
31583938-158393871.98972.25
41580128-158012871.81672.06
51611108-161110873.22473.48
61598367-159836772.64572.91
45min11811298-181129882.32282.291.3982.7082.671.39
21796876-179687681.66782.03
31831439-183143983.23883.62
41780083-178008380.90381.27
51847623-184762383.97384.36
61796391-179639181.64582.03
60min11826129-182612982.99684.521.4483.5185.031.43
21853666-185366684.24884.75
31845157-184515783.86184.39
41854044-185404484.26584.77
51903349-190334986.50687.03
61874933-187493385.21485.73
极限11891738-189173885.97885.741.0686.6386.391.06
21900168-190016886.36187.01
31870883-187088385.03085.69
41855111-185511184.31384.96
51909229-190922986.77387.44
61891463-189146385.96686.63
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