布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.113172505317071131694243171050317354231714460.06
213.123173500317550131745000.05
单位质量响应值RSD%判断
241910.45241958.840.02数据可信
供试品溶液-25050801批-pH5.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12190921-219092181.42178.602.2081.4278.602.20
22152288-215228879.98579.99
32097993-209799377.96877.97
42082148-208214877.37977.38
52073047-207304777.04077.04
62093597-209359777.80477.80
10min12247984-224798483.54285.262.4683.6885.392.46
22364987-236498787.89088.02
32218176-221817682.43482.56
42274681-227468184.53484.66
52322789-232278986.32286.45
62336437-233643786.82986.96
15min12446795-244679590.93090.740.7591.2191.020.75
22457759-245775991.33891.62
32438766-243876690.63290.90
42415371-241537189.76290.03
52428158-242815890.23790.51
62463697-246369791.55891.83
20min12386409-238640988.68691.661.6689.1192.091.65
22484044-248404492.31492.75
32490272-249027292.54692.96
42469747-246974791.78392.20
52470008-247000891.79392.22
62498716-249871692.86093.29
30min12510267-251026793.28992.680.8593.8693.260.85
22493059-249305992.64993.24
32468876-246887691.75192.32
42470218-247021891.80192.37
52500245-250024592.91693.49
62520678-252067893.67694.26
45min12479079-247907992.13092.770.8692.8693.500.86
22494569-249456992.70593.45
32471236-247123691.83892.56
42496843-249684392.79093.52
52504550-250455093.07693.81
62531915-253191594.09394.83
60min12448913-244891391.00992.291.0691.8993.181.06
22479262-247926292.13793.03
32513989-251398993.42794.31
42471490-247149091.84892.73
52471241-247124191.83992.72
62515221-251522193.47394.37
极限12450689-245068991.07592.270.9592.1193.310.94
22456183-245618391.27992.33
32495199-249519992.72993.76
42506468-250646893.14894.18
52490641-249064192.56093.60
62497992-249799292.83393.88
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.113169978317389631718033172066316974031714970.06
213.123168580316598531672820.06
单位质量响应值RSD%判断
241914.34241408.690.15数据可信
供试品溶液-25051201批-pH5.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12102249-210224978.21472.915.4778.2172.915.46
22023201-202320175.27375.27
31980433-198043373.68273.68
41960684-196068472.94772.95
51902170-190217070.77070.77
61788940-178894066.55766.56
10min12392504-239250489.01384.106.1089.1484.226.10
22318043-231804386.24386.37
32312360-231236086.03186.15
42296123-229612385.42785.55
52247962-224796283.63583.75
61995739-199573974.25174.36
15min12542234-254223494.58490.045.0194.8690.305.02
22454715-245471591.32891.60
32478208-247820892.20292.47
42458588-245858891.47291.74
52394814-239481489.09989.36
62192341-219234181.56681.80
20min12606140-260614096.96193.842.8997.4094.262.91
22530415-253041594.14494.57
32556844-255684495.12795.55
42550631-255063194.89695.31
52497621-249762192.92493.33
62392414-239241489.01089.38
30min12651484-265148498.64894.914.1299.2595.484.12
22580591-258059196.01196.59
32606337-260633796.96997.55
42589454-258945496.34196.92
52524826-252482693.93694.50
62353825-235382587.57488.09
45min12702829-2702829100.55996.513.12101.3297.243.13
22619113-261911397.44498.18
32638411-263841198.16298.90
42603326-260332696.85797.59
52518919-251891993.71694.43
62481978-248197892.34293.01
60min12682469-268246999.80195.644.23100.7396.534.23
22588523-258852396.30697.21
32629192-262919297.81998.72
42598319-259831996.67097.57
52559752-255975295.23696.11
62365872-236587288.02288.84
极限12704468-2704468100.62096.273.97101.7297.323.97
22594428-259442896.52697.59
32641767-264176798.28799.35
42621141-262114197.51998.58
52560777-256077795.27496.31
62402671-240267189.39190.36
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