洛索洛芬钠细粒剂项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100638-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)87.5对照品水分(%)0对照品稀释倍数200
标示量(mg)60供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.811146725115500011565471151657115366611527190.33
213.761163455115137811574160.74
单位质量响应值RSD%判断
83469.8884114.530.55数据可信
加速3月-供试品溶液-2025020621批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11244495-124449597.46999.411.4697.4799.421.46
21275321-127532199.88399.88
31260548-126054898.72698.73
41299748-1299748101.796101.80
51272784-127278499.68499.68
61263128-126312898.92898.93
10min11270479-127047999.504101.091.3099.67101.261.30
21296082-1296082101.509101.68
31282940-1282940100.480100.64
41320355-1320355103.410103.58
51289209-1289209100.971101.14
61285639-1285639100.691100.86
15min11266090-126609099.160100.871.1699.49101.201.16
21293372-1293372101.297101.63
31288154-1288154100.888101.22
41311647-1311647102.728103.07
51281751-1281751100.387100.72
61286502-1286502100.759101.09
30min11260311-126031198.707100.641.2999.20101.141.29
21284709-1284709100.618101.12
31284010-1284010100.564101.06
41312360-1312360102.784103.30
51286564-1286564100.764101.27
61282086-1282086100.413100.91
极限11260381-126038198.713100.471.3699.37101.141.35
21283981-1283981100.561101.23
31285431-1285431100.675101.34
41312301-1312301102.779103.46
51282959-1282959100.481101.15
61271686-127168699.598100.27
洛索洛芬钠细粒剂项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100638-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)87.5对照品水分(%)0对照品稀释倍数200
标示量(mg)60供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.811153011115321511517461151543115142011521870.08
213.761149815115448511521500.29
单位质量响应值RSD%判断
83431.3583731.830.26数据可信
加速3月-供试品溶液-2025020721批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11257163-125716398.70899.691.1698.7199.691.16
21247822-124782297.97497.97
31286915-1286915101.044101.04
41279563-1279563100.467100.47
51276204-1276204100.203100.20
61270712-127071299.77299.77
10min11273722-1273722100.008100.731.25100.17100.901.25
21258384-125838498.80498.97
31292447-1292447101.478101.65
41283201-1283201100.752100.92
51305060-1305060102.469102.64
61284794-1284794100.877101.04
15min11270859-127085999.783100.691.40100.11101.021.40
21253307-125330798.40598.73
31297523-1297523101.877102.21
41293003-1293003101.522101.86
51299194-1299194102.008102.35
61280289-1280289100.524100.86
30min11268687-126868799.613100.731.58100.11101.231.58
21255589-125558998.58499.08
31303644-1303644102.357102.86
41282205-1282205100.674101.18
51308449-1308449102.735103.24
61278893-1278893100.414100.92
极限11264846-126484699.311100.631.4199.97101.301.41
21256221-125622198.63499.29
31301418-1301418102.183102.86
41288838-1288838101.195101.87
51297651-1297651101.887102.57
61280688-1280688100.555101.22
洛索洛芬钠细粒剂项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100638-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)87.5对照品水分(%)0对照品稀释倍数200
标示量(mg)60供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.811153322115658311530831152129116392611558090.42
213.761154338114975611520470.29
单位质量响应值RSD%判断
83693.6383724.350.03数据可信
加速3月-供试品溶液-2025020821批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11308044-1308044102.546101.620.66102.55101.620.66
21299918-1299918101.909101.91
31286792-1286792100.880100.88
41302099-1302099102.080102.08
51291578-1291578101.255101.26
61288642-1288642101.025101.03
10min11325572-1325572103.920102.670.97104.09102.840.97
21310218-1310218102.717102.89
31291930-1291930101.283101.45
41321704-1321704103.617103.79
51308081-1308081102.549102.72
61300349-1300349101.943102.11
15min11327705-1327705104.088102.671.28104.43103.011.28
21315383-1315383103.122103.46
31288950-1288950101.049101.39
41328563-1328563104.155104.50
51298545-1298545101.802102.14
61298245-1298245101.778102.12
30min11321130-1321130103.572102.330.91104.09102.840.91
21305521-1305521102.348102.86
31289180-1289180101.067101.57
41316438-1316438103.204103.72
51300885-1300885101.985102.49
61298713-1298713101.815102.32
极限11313396-1313396102.966102.070.84103.66102.760.84
21303916-1303916102.223102.91
31282549-1282549100.547101.22
41310289-1310289102.722103.41
51303175-1303175102.164102.84
61298652-1298652101.810102.49
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