贝派度酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.073110323085423084043083073089563090480.37
210.143091213092213091710.03
单位质量响应值RSD%判断
30689.9730490.240.47数据可信
供试品溶液-24032601批-pH6.6
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min187468-8746828.51431.075.1428.5131.075.14
2100318-10031832.70332.70
395845-9584531.24531.24
492446-9244630.13730.14
595507-9550731.13431.13
6100283-10028332.69132.69
10min1218929-21892971.36972.561.6971.4272.621.70
2220189-22018971.78071.83
3226120-22612073.71373.77
4218833-21883371.33871.39
5224138-22413873.06773.12
6227339-22733974.11174.17
15min1257995-25799584.10484.611.2784.2784.781.27
2254204-25420482.86883.04
3263139-26313985.78185.96
4258576-25857684.29484.46
5261633-26163385.29085.46
6261723-26172385.31985.50
20min1278790-27879090.88391.171.1791.1991.481.17
2273715-27371589.22989.54
3283252-28325292.33892.66
4280795-28079591.53791.85
5281353-28135391.71992.03
6280083-28008391.30591.62
30min1300512-30051297.96498.120.9098.4298.590.89
2296959-29695996.80697.27
3303266-30326698.86299.33
4304674-30467499.32199.78
5300199-30019997.86298.33
6300397-30039797.92798.40
45min1311127-311127101.425101.531.28102.05102.161.27
2309961-309961101.045101.67
3312115-312115101.747102.38
4318925-318925103.967104.59
5308511-308511100.572101.20
6308050-308050100.422101.06
60min1312433-312433101.850101.971.45102.64102.771.43
2312298-312298101.806102.60
3312582-312582101.899102.71
4321357-321357104.760105.56
5308860-308860100.686101.49
6309291-309291100.826101.63
极限1312675-312675101.929101.871.30102.89102.841.29
2312166-312166101.763102.72
3312620-312620101.911102.89
4319875-319875104.276105.25
5308377-308377100.528101.50
6309335-309335100.841101.81
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