盐酸达泊西汀片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DSZJ-4057-240226对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数2000
标示量(mg)60供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.852051902052472050562051682049972051320.05
215.812048732051112049920.09
单位质量响应值RSD%判断
12942.0812965.970.14数据可信
供试品溶液-250401批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min126967-2696715.61311.3029.3915.6111.3029.40
223309-2330913.49513.50
321119-2111912.22712.23
419903-1990311.52311.52
511402-114026.6016.60
614413-144138.3458.34
10min183055-8305548.08647.276.0948.1747.336.11
283892-8389248.57148.65
383211-8321148.17748.24
487617-8761750.72850.79
578845-7884545.64945.69
673248-7324842.40842.45
15min1106690-10669061.77060.943.2862.1261.263.29
2103291-10329159.80260.15
3107270-10727062.10662.44
4108252-10825262.67563.02
5106890-10689061.88662.18
699100-9910057.37657.66
20min1115442-11544266.83865.751.5367.5366.421.55
2114131-11413166.07966.76
3112738-11273865.27265.95
4113845-11384565.91366.61
5114676-11467666.39467.03
6110554-11055464.00864.61
30min1118373-11837368.53567.972.6969.6069.002.68
2115887-11588767.09568.14
3117544-11754468.05569.10
4119010-11901068.90369.96
5121412-12141270.29471.30
6112130-11213064.92065.88
45min1122100-12210070.69269.132.1572.1470.542.13
2114770-11477066.44967.87
3121090-12109070.10871.53
4120371-12037169.69171.13
5119237-11923769.03570.43
6118877-11887768.82670.14
60min1125085-12508572.42172.081.4474.2673.871.46
2125444-12544472.62874.41
3123319-12331971.39873.21
4126101-12610173.00974.84
5125612-12561272.72674.50
6121414-12141470.29571.99
极限1130232-13023275.40176.152.3177.6478.342.30
2131313-13131376.02678.22
3131251-13125175.99178.20
4135346-13534678.36180.60
5134225-13422577.71279.89
6126792-12679273.40975.50
盐酸达泊西汀片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DSZJ-4057-240226对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数2000
标示量(mg)60供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.852048182048232046982042792045782046390.12
215.812057312056442056880.03
单位质量响应值RSD%判断
12910.9813009.990.55数据可信
供试品溶液-250402批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1713-7130.4134.9091.540.414.9091.57
220801-2080112.03712.04
37292-72924.2204.22
413556-135567.8457.84
57649-76494.4264.43
6745-7450.4310.43
10min177515-7751544.85746.706.4244.8646.736.44
282504-8250447.74447.81
388678-8867851.31751.34
479216-7921645.84245.89
582729-8272947.87447.90
673578-7357842.57942.58
15min1101605-10160558.79860.342.4259.0560.622.46
2106711-10671161.75362.08
3106892-10689261.85762.17
4104688-10468860.58260.88
5104771-10477160.63060.92
6100904-10090458.39258.63
20min1110035-11003563.67665.021.7264.2565.641.73
2111747-11174764.66765.34
3115125-11512566.62267.27
4111071-11107164.27664.91
5114192-11419266.08266.71
6111983-11198364.80365.37
30min1115341-11534166.74767.430.9767.6868.420.98
2118034-11803468.30569.34
3116099-11609967.18568.21
4115301-11530166.72467.72
5117378-11737867.92668.92
6117025-11702567.72168.64
45min1118842-11884268.77369.371.4970.0870.731.46
2121286-12128670.18771.60
3120032-12003269.46170.86
4120218-12021869.56970.93
5116987-11698767.69969.07
6121931-12193170.56071.86
60min1122720-12272071.01771.150.8772.7072.890.84
2121568-12156870.35072.15
3124422-12442272.00273.78
4121982-12198270.59072.34
5123452-12345271.44073.19
6123578-12357871.51373.20
极限1131197-13119775.92275.411.3778.0077.541.29
2128322-12832274.25976.45
3127864-12786473.99476.18
4130692-13069275.63077.77
5131633-13163376.17578.32
6132120-13212076.45778.55
点击查看处理图标(人工保存)
　
原始图谱下载图谱(吕婷婷 于 2025-05-27 15:56:59 完成)
生成报告数据部分(等待生成报告)
Current page cost:55 ms