玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.139830498210982469814798202982220.06
211.179828298149982160.10
单位质量响应值RSD%判断
8824.988792.840.26数据可信
供试品溶液-2025051721批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min179398-7939880.93482.231.6580.9382.231.65
282552-8255284.14984.15
379067-7906780.59780.60
481021-8102182.58882.59
581613-8161383.19283.19
680360-8036081.91581.91
10min189251-8925190.97892.671.4791.4393.131.47
292675-9267594.46894.94
391132-9113292.89593.34
492030-9203093.81094.27
589606-8960691.34091.80
690790-9079092.54693.00
15min193007-9300794.80695.160.7095.7696.130.71
294141-9414195.96296.95
393139-9313994.94195.90
494210-9421096.03397.01
592773-9277394.56895.54
692833-9283394.62995.60
20min195022-9502296.86096.291.5398.3497.801.52
295591-9559197.44098.97
392954-9295494.75296.24
495907-9590797.76299.28
592402-9240294.19095.68
694928-9492896.76598.26
30min192528-9252894.31895.691.0996.3497.721.09
295140-9514096.98199.05
393000-9300094.79996.82
494860-9486096.69598.75
593744-9374495.55897.58
693957-9395795.77597.81
45min193983-9398395.80195.321.4098.3597.891.38
295200-9520097.04299.65
391425-9142593.19495.74
494231-9423196.05498.65
592805-9280594.60097.15
693426-9342695.23397.80
60min190761-9076192.51794.211.8895.5997.311.85
295304-9530497.148100.29
392124-9212493.90696.97
493522-9352295.33198.46
590871-9087192.62995.70
691970-9197093.74996.84
极限190882-9088292.64093.161.5696.2396.781.54
293387-9338795.19498.88
390180-9018091.92595.51
491674-9167493.44897.10
589653-8965391.38794.98
692548-9254894.33897.95
玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.139828198466981999824198158982690.13
211.179790798173980400.20
单位质量响应值RSD%判断
8829.208777.080.42数据可信
供试品溶液-2025051721批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min152844-5284453.90258.194.5053.9058.194.50
256288-5628857.41557.41
356748-5674857.88457.88
457193-5719358.33858.34
560474-6047461.68561.68
658731-5873159.90759.91
10min169415-6941570.80575.713.4371.1076.043.44
274903-7490376.40376.72
373747-7374775.22375.54
476037-7603777.55977.88
574820-7482076.31876.66
676443-7644377.97378.31
15min179551-7955181.14485.232.6681.8485.972.67
283956-8395685.63786.38
382874-8287484.53385.27
484006-8400685.68886.44
584961-8496186.66287.43
685976-8597687.69788.46
20min187044-8704488.78790.561.2089.9391.781.21
289064-8906490.84792.07
388767-8876790.54491.75
490300-9030092.10893.34
589069-8906990.85292.10
688443-8844390.21491.47
30min189351-8935191.14093.541.5892.7895.261.59
292753-9275394.61096.33
390855-9085592.67494.39
493414-9341495.28497.03
591704-9170493.54095.29
692119-9211993.96395.72
45min190842-9084292.66193.671.3794.8095.911.36
293249-9324995.11697.37
390810-9081092.62894.85
493587-9358795.46197.73
591093-9109392.91795.19
691428-9142893.25895.53
60min192929-9292994.78994.150.9997.4596.910.95
291925-9192593.76596.54
392184-9218494.03096.77
493800-9380095.67898.48
591328-9132893.15695.95
691653-9165393.48896.28
极限191988-9198893.83094.361.4597.0197.641.43
292647-9264794.50297.80
391407-9140793.23796.50
495051-9505196.954100.29
592426-9242694.27697.58
691521-9152193.35396.67
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