布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.662649225264953026474162639926265083426473860.17
2 10.732646382264522826458050.04
单位质量响应值RSD%判断
248347.65246580.150.51数据可信
供试品溶液-240920336批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1513872-51387218.67118.072.4718.6718.072.48
2503918-50391818.30918.31
3500838-50083818.19718.20
4494971-49497117.98417.98
5493122-49312217.91717.92
6477330-47733017.34317.34
10min1552336-55233620.06819.913.2720.1019.943.26
2515531-51553118.73118.76
3562913-56291320.45220.48
4559124-55912420.31520.34
5558301-55830120.28520.31
6539582-53958219.60519.63
15min1581444-58144421.12620.623.9821.1920.693.97
2526208-52620819.11919.18
3582558-58255821.16621.23
4578438-57843821.01621.08
5556345-55634520.21420.28
6580639-58063921.09621.16
20min1566476-56647620.58219.804.1720.6819.904.15
2534100-53410019.40519.50
3566747-56674720.59220.69
4555087-55508720.16820.27
5540545-54054519.64019.74
6507541-50754118.44118.54
30min1558503-55850320.29219.284.1620.4319.414.13
2535390-53539019.45219.58
3522756-52275618.99319.13
4495290-49529017.99518.13
5524691-52469119.06419.19
6547444-54744419.89020.02
45min1564540-56454020.51118.936.6120.6819.106.56
2511587-51158718.58818.75
3532596-53259619.35119.52
4547403-54740319.88920.05
5468892-46889217.03617.20
6501351-50135118.21618.38
60min1492646-49264617.89918.315.7718.1018.515.73
2493575-49357517.93318.12
3550711-55071120.00920.21
4526066-52606619.11419.31
5470006-47000617.07717.27
6491129-49112917.84418.04
极限1430065-43006515.62618.809.8615.8619.039.72
2505602-50560218.37018.59
3504198-50419818.31918.55
4559611-55961120.33220.56
5572565-57256520.80321.02
6532699-53269919.35519.58
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.662643387264492526420552641395264067326424870.07
2 10.732646363264829726473300.06
单位质量响应值RSD%判断
247888.09246722.270.34数据可信
供试品溶液-240920336批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1482706-48270617.54916.414.4317.5516.414.42
2463854-46385416.86416.86
3455271-45527116.55216.55
4431057-43105715.67215.67
5443444-44344416.12216.12
6432308-43230815.71715.72
10min1515681-51568118.74818.862.2918.7818.882.28
2522897-52289719.01019.04
3536583-53658319.50819.54
4523107-52310719.01819.04
5501661-50166118.23818.27
6512071-51207118.61718.64
15min1517512-51751218.81518.332.1318.8818.392.14
2509051-50905118.50718.57
3509662-50966218.52918.59
4503604-50360418.30918.37
5498997-49899718.14218.20
6486400-48640017.68417.74
20min1491742-49174217.87817.781.0117.9717.870.99
2481331-48133117.49917.59
3487336-48733617.71817.81
4488203-48820317.74917.84
5489847-48984717.80917.90
6496058-49605818.03518.12
30min1476594-47659417.32716.925.1617.4517.045.12
2467420-46742016.99417.11
3424724-42472415.44115.56
4476185-47618517.31217.43
5453314-45331416.48116.60
6494216-49421617.96818.08
45min1459896-45989616.72016.766.8016.8716.906.75
2462512-46251216.81516.96
3401540-40154014.59814.74
4492641-49264117.91118.06
5473226-47322617.20517.35
6475373-47537317.28317.43
60min1486029-48602917.67016.618.6717.8516.788.60
2456800-45680016.60716.78
3392829-39282914.28214.45
4505177-50517718.36618.54
5464888-46488816.90217.07
6434728-43472815.80515.98
极限1506124-50612418.40116.4110.4718.6116.6210.37
2466220-46622016.95017.15
3380849-38084913.84614.04
4480309-48030917.46217.67
5467356-46735616.99117.19
6408140-40814014.83815.04
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.662651357264667026523912651205265086926504980.09
2 10.732647172264942326482980.07
单位质量响应值RSD%判断
248639.59246812.490.53数据可信
供试品溶液-240920336批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13020518-3020518109.629104.892.38109.63104.892.38
22831614-2831614102.772102.77
32893940-2893940105.034105.03
42892746-2892746104.991104.99
52847626-2847626103.354103.35
62854027-2854027103.586103.59
10min13045478-3045478110.534106.402.03110.72106.582.03
22882630-2882630104.624104.80
32931842-2931842106.410106.59
42933714-2933714106.478106.65
52901159-2901159105.296105.47
62894404-2894404105.051105.22
15min13047349-3047349110.602106.572.03110.97106.922.03
22881695-2881695104.590104.94
32942845-2942845106.809107.16
42937619-2937619106.620106.97
52912659-2912659105.714106.06
62895043-2895043105.074105.42
20min13043433-3043433110.460106.631.90111.01107.171.90
22883569-2883569104.658105.18
32934739-2934739106.515107.05
42941073-2941073106.745107.28
52919906-2919906105.977106.50
62905456-2905456105.452105.98
30min13036436-3036436110.206106.491.92110.94107.201.92
22870453-2870453104.182104.88
32942087-2942087106.782107.49
42930292-2930292106.354107.06
52924407-2924407106.140106.84
62901042-2901042105.292105.99
45min13031021-3031021110.010106.261.86110.93107.151.86
22872791-2872791104.267105.13
32926695-2926695106.223107.11
42922809-2922809106.082106.97
52914698-2914698105.788106.67
62898505-2898505105.200106.07
60min13021138-3021138109.651106.051.82110.75107.111.82
22865619-2865619104.007105.05
32921999-2921999106.053107.12
42920019-2920019105.981107.04
52912658-2912658105.714106.77
62890303-2890303104.902105.95
极限13019281-3019281109.584105.851.90110.87107.091.90
22852831-2852831103.542104.76
32914174-2914174105.769107.01
42912411-2912411105.705106.94
52908940-2908940105.579106.81
62891166-2891166104.934106.16
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.662648658264776026405332651429264360926463980.17
2 10.732646284263493726406100.31
单位质量响应值RSD%判断
248254.97246095.990.62数据可信
供试品溶液-240920336批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12917396-2917396106.122103.091.95106.12103.091.95
22865567-2865567104.237104.24
32857141-2857141103.930103.93
42782364-2782364101.210101.21
52802671-2802671101.949101.95
62778974-2778974101.087101.09
10min12939259-2939259106.917104.451.72107.09104.621.72
22909727-2909727105.843106.02
32884496-2884496104.925105.10
42817828-2817828102.500102.67
52858014-2858014103.962104.13
62818778-2818778102.535102.70
15min12954049-2954049107.455104.291.83107.81104.641.83
22893063-2893063105.237105.59
32876768-2876768104.644104.99
42828531-2828531102.890103.23
52812693-2812693102.314102.66
62837720-2837720103.224103.56
20min12927843-2927843106.502104.541.28107.04105.061.29
22902996-2902996105.598106.12
32882304-2882304104.846105.37
42838009-2838009103.234103.75
52854230-2854230103.825104.34
62838471-2838471103.251103.76
30min12924420-2924420106.378104.661.09107.09105.361.10
22899108-2899108105.457106.16
32878907-2878907104.722105.42
42836768-2836768103.189103.87
52870156-2870156104.404105.09
62854604-2854604103.838104.52
45min12903169-2903169105.605104.490.81106.49105.360.81
22897762-2897762105.408106.29
32867100-2867100104.293105.16
42852618-2852618103.766104.62
52866644-2866644104.276105.14
62847635-2847635103.585104.44
60min12902842-2902842105.593104.370.84106.66105.410.84
22885581-2885581104.965106.02
32875598-2875598104.602105.65
42839136-2839136103.275104.30
52864208-2864208104.187105.22
62847335-2847335103.574104.60
极限12895825-2895825105.338104.180.84106.58105.400.85
22885006-2885006104.944106.17
32872860-2872860104.502105.72
42835533-2835533103.144104.34
52849319-2849319103.646104.85
62846161-2846161103.531104.73
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