托伐普坦口崩片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101242-202302对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数2000
标示量(mg)7.5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.482010592010312008952007682010802009670.07
216.552018312017982018140.02
单位质量响应值RSD%判断
12194.6012194.200.01数据可信
供试品溶液-2025050921批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min119725-197259.6969.653.279.709.653.26
220738-2073810.19310.19
319889-198899.7769.78
419188-191889.4329.43
519214-192149.4449.44
619012-190129.3459.35
10min139202-3920219.26919.152.4619.2919.172.46
240501-4050119.90819.92
339048-3904819.19419.21
437976-3797618.66718.68
539143-3914319.24019.26
637899-3789918.62918.64
15min155717-5571727.38727.071.7327.4427.111.74
255935-5593527.49427.54
355185-5518527.12527.17
453603-5360326.34826.39
555736-5573627.39627.44
654211-5421126.64726.69
20min168983-6898333.90833.781.5334.0033.871.53
269876-6987634.34734.44
368758-6875833.79733.89
466976-6697632.92133.01
569575-6957534.19934.29
668186-6818633.51633.61
30min190542-9054244.50544.271.2244.6644.421.23
291232-9123244.84445.00
390115-9011544.29544.44
488127-8812743.31843.46
590723-9072344.59444.74
689593-8959344.03844.19
45min1114964-11496456.50955.711.1956.7355.941.18
2113607-11360755.84256.07
3114004-11400456.03756.26
4112097-11209755.10055.32
5114022-11402256.04656.27
6111390-11139054.75254.97
60min1132925-13292565.33864.460.8865.6664.780.88
2131565-13156564.66964.99
3131044-13104464.41364.73
4129493-12949363.65163.96
5131375-13137564.57664.89
6130487-13048764.13964.45
90min1156113-15611376.73575.520.9777.1675.950.97
2154029-15402975.71176.14
3153762-15376275.58076.00
4151855-15185574.64275.06
5153743-15374375.57076.00
6152376-15237674.89875.32
120min1170862-17086283.98582.640.9784.5483.190.96
2168314-16831482.73383.29
3167628-16762882.39582.95
4166325-16632581.75582.30
5168797-16879782.97083.52
6166861-16686182.01882.56
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
极限1179579-17957988.27086.541.6388.9787.231.63
2177546-17754687.27087.96
3176169-17616986.59487.28
4170940-17094084.02384.70
5176312-17631286.66487.35
6175811-17581186.41887.10
托伐普坦口崩片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101242-202302对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数2000
标示量(mg)7.5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.482028812027272025122024372026742026460.09
216.552060132056692058410.12
单位质量响应值RSD%判断
12296.4812437.520.81数据可信
供试品溶液-2025050921批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min119008-190089.2139.311.539.219.311.56
219715-197159.5569.56
319052-190529.2349.23
419289-192899.3499.35
519310-193109.3599.36
618904-189049.1639.16
10min136936-3693617.90318.602.3417.9218.622.33
238233-3823318.53118.55
338719-3871918.76718.78
439703-3970319.24419.26
538491-3849118.65618.67
638210-3821018.52018.54
15min153021-5302125.69926.271.7725.7426.321.77
253965-5396526.15626.20
354050-5405026.19826.24
455902-5590227.09527.14
553835-5383526.09326.14
654458-5445826.39526.44
20min166836-6683632.39532.851.3132.4832.941.30
267258-6725832.59932.69
367679-6767932.80432.89
469429-6942933.65233.74
567767-6776732.84632.94
667739-6773932.83332.92
30min187392-8739242.35842.961.0542.5043.101.05
289007-8900743.14143.29
387741-8774142.52742.67
489872-8987243.56043.71
588584-8858442.93643.08
689148-8914843.20943.35
45min1110162-11016253.39554.180.8653.6154.390.86
2111144-11114453.87154.09
3112043-11204354.30654.52
4112699-11269954.62454.85
5112492-11249254.52454.74
6112101-11210154.33554.55
60min1128176-12817662.12662.540.6662.4362.850.66
2129355-12935562.69763.00
3129092-12909262.57062.88
4129815-12981562.92063.23
5127848-12784861.96762.27
6129910-12991062.96663.27
90min1151109-15110973.24174.291.5273.6574.701.52
2152960-15296074.13974.55
3152406-15240673.87074.28
4153519-15351974.41074.83
5151905-15190573.62774.04
6157697-15769776.43576.85
120min1165475-16547580.20580.870.9380.7381.410.93
2166744-16674480.82081.35
3166315-16631580.61281.15
4166997-16699780.94281.48
5165790-16579080.35780.89
6169798-16979882.30082.84
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
极限1177094-17709485.83685.330.6486.5086.000.64
2176893-17689385.73986.41
3175264-17526484.94985.62
4176094-17609485.35186.03
5174221-17422184.44485.11
6176747-17674785.66886.34
托伐普坦口崩片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101242-202302对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数2000
标示量(mg)7.5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.482043042042662038882036132039652040070.15
216.552054902055532055220.03
单位质量响应值RSD%判断
12379.0712418.250.23数据可信
供试品溶液-2025051021批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min119393-193939.3759.303.579.389.303.58
218545-185458.9658.97
318248-182488.8228.82
419492-194929.4239.42
519892-198929.6179.62
619850-198509.5969.60
10min138026-3802618.38319.045.9618.4019.065.96
237705-3770518.22818.24
338391-3839118.56018.57
443716-4371621.13421.15
538022-3802218.38118.40
640481-4048119.57019.59
15min154777-5477726.48126.473.1626.5326.513.17
252973-5297325.60925.65
354265-5426526.23426.28
454884-5488426.53326.58
553630-5363025.92725.97
657956-5795628.01828.07
20min168691-6869133.20832.962.4033.3033.052.40
266079-6607931.94532.03
368325-6832533.03133.12
469780-6978033.73433.83
566358-6635832.08032.17
669826-6982633.75733.85
30min189505-8950543.27043.222.0743.4243.362.07
286493-8649341.81441.96
390146-9014643.58043.72
491152-9115244.06744.22
587960-8796042.52342.67
691111-9111144.04744.20
45min1113467-11346754.85554.421.8955.0754.631.89
2109866-10986653.11453.32
3112806-11280654.53554.75
4115150-11515055.66855.89
5110154-11015453.25353.47
6113916-11391655.07255.30
60min1130829-13082963.24863.051.8063.5663.361.81
2127008-12700861.40161.70
3131388-13138863.51863.83
4132882-13288264.24164.56
5128142-12814261.94962.25
6132278-13227863.94964.27
90min1153529-15352974.22274.151.6174.6474.571.61
2149260-14926072.15872.56
3155429-15542975.14175.55
4155873-15587375.35575.78
5151939-15193973.45373.86
6154309-15430974.59975.02
120min1170032-17003282.20081.251.7882.7481.791.78
2162952-16295278.77879.30
3169573-16957381.97882.52
4171056-17105682.69583.25
5166357-16635780.42480.95
6168438-16843881.43081.98
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
极限1175894-17589485.03485.401.4685.7186.071.46
2172275-17227583.28583.94
3178214-17821486.15686.83
4179927-17992786.98487.67
5176522-17652285.33886.00
6177039-17703985.58886.27
点击查看处理图标(人工保存)
　
原始图谱下载图谱(吕婷婷 于 2025-06-16 15:44:45 完成)
生成报告数据部分(等待生成报告)
Current page cost:66 ms