枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.272322342324862319912323032323332322690.08
217.232318462317902318180.02
单位质量响应值RSD%判断
13449.2813454.320.03数据可信
长期12月-供试品溶液-pH2.0
批号样品(片)A1A2A平均溶出量(%)平均(%)RSD%置信区间
20240301211269448269105269276101.36101.851.56100.19%～103.52%
2273260273651273456102.93
3269779270224270002101.63
4270667270923270795101.93
526351826400426376199.28
6276554275943276248103.98
20240302211267040266723266882100.46102.291.23100.97%～103.61%
2268284269006268645101.12
3272516272389272452102.56
4273121273294273208102.84
5273485273371273428102.92
6276057275696275876103.84
2024030321126292526268726280698.92100.151.0199.10%～101.21%
2267185267709267447100.67
3267651267501267576100.72
426297926319526308799.03
5269315269673269494101.44
6265915266167266041100.14
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.274659314661784657804657044651984657580.08
217.234661054675844668440.23
单位质量响应值RSD%判断
26969.2027094.830.33数据可信
长期12月-供试品溶液-pH2.0
批号样品(片)A1A2A平均溶出量(%)平均(%)RSD%置信区间
2024030121153302153288353295299.8398.850.7798.06%～99.64%
253294253171653232999.71
352387852384352386098.13
452445452490552468098.28
552443452499852471698.29
652663952893452778698.86
2024030221152609352683552646498.6198.201.6496.51%～99.88%
251667951661551664796.78
352259352214852237097.85
452634452584752609698.55
551511751486351499096.47
6538804538894538849100.93
2024030321152863252832452847898.9998.401.4796.89%～99.92%
252884152855052869699.03
353108453106953107699.48
452772952720452746698.80
551014350973750994095.52
652607152669352638298.60
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.279405819392309411539410309402359404460.09
217.239383789382699383240.01
单位质量响应值RSD%判断
54455.4754458.730.01数据可信
长期12月-供试品溶液-pH2.0
批号样品(片)A1A2A平均溶出量(%)平均(%)RSD%置信区间
2024030121110583581058926105864298.4398.012.3895.57%～100.45%
210637351063938106383698.92
3109628310940321095158101.83
410419601041616104178896.87
510441391042711104342597.02
610210661022113102159094.99
2024030221110584971058882105869098.4499.720.6999.00%～100.45%
2107800110782671078134100.25
310749321075033107498299.95
4107594910775431076746100.12
5107703910766171076828100.12
610697411069772106975699.47
2024030321110539331054246105409098.0198.640.8997.73%～99.56%
210617881061175106148298.70
3107882810779151078372100.27
410538631054017105394098.00
510627961062417106260698.80
610554091054393105490198.09
点击查看处理图标(人工保存)
　
原始图谱下载图谱(谢鑫慧 于 2025-06-17 19:24:54 完成)
生成报告数据部分(等待生成报告)
Current page cost:71 ms