枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.279355009351359349019342689335199346650.09
217.239325449323479324460.02
单位质量响应值RSD%判断
54120.7354117.590.01数据可信
长期12月-供试品溶液-2024051911批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1973187-97318791.05391.631.8891.0591.631.88
2993239-99323992.92992.93
3946680-94668088.57388.57
4979982-97998291.68891.69
5998017-99801793.37693.38
6985111-98511192.16892.17
10min11020884-102088495.51596.281.5995.6796.441.59
21044731-104473197.74697.90
31001409-100140993.69393.84
41031561-103156196.51496.67
51044796-104479697.75397.91
61031070-103107096.46896.62
15min11036108-103610896.94098.201.4297.2598.511.42
21069965-1069965100.107100.43
31031140-103114096.47596.78
41054489-105448998.65998.97
51060575-106057599.22999.55
61044956-104495697.76798.08
20min11043866-104386697.66599.171.2798.1499.641.27
21079131-1079131100.965101.45
31051338-105133898.36598.83
41064289-106428999.576100.05
51069907-1069907100.102100.59
61051034-105103498.33698.81
30min11048485-104848598.09899.661.2998.73100.301.29
21086825-1086825101.685102.34
31063792-106379299.530100.16
41068137-106813799.936100.58
51070576-1070576100.165100.82
61053144-105314498.53499.17
45min11047061-104706197.96499.761.3398.76100.571.33
21088846-1088846101.874102.70
31062903-106290399.447100.24
41070798-1070798100.185101.00
51070406-1070406100.149100.97
61057535-105753598.94499.75
极限11046031-104603197.86899.641.2998.83100.611.29
21086982-1086982101.699102.69
31061901-106190199.353100.31
41067417-106741799.869100.85
51069573-1069573100.071101.06
61057785-105778598.96899.94
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.279312639311739312389309899308609311050.02
217.239340369353049346700.10
单位质量响应值RSD%判断
53914.5954246.660.44数据可信
长期12月-供试品溶液-2024052011批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1966396-96639690.48391.820.7690.4891.820.76
2982115-98211591.95491.95
3985875-98587592.30692.31
4980772-98077291.82991.83
5986679-98667992.38292.38
6982415-98241591.98291.98
10min11022675-102267595.75297.001.3395.9097.161.33
21027308-102730896.18696.34
31032110-103211096.63596.79
41061679-106167999.40499.56
51038484-103848497.23297.39
61033858-103385896.79996.95
15min11053107-105310798.60198.821.2698.9199.131.26
21044037-104403797.75298.07
31045476-104547697.88798.20
41080769-1080769101.191101.51
51055596-105559698.83499.15
61053450-105345098.63398.95
20min11066542-106654299.85999.741.21100.33100.221.21
21055551-105555198.83099.31
31051955-105195598.49398.97
41088679-1088679101.932102.42
51065809-106580999.790100.27
61062928-106292899.521100.00
30min11077248-1077248100.862100.471.28101.50101.121.27
21063724-106372499.595100.24
31053409-105340998.62999.27
41093841-1093841102.415103.07
51075277-1075277100.677101.32
61075187-1075187100.669101.31
45min11075038-1075038100.655100.581.35101.46101.391.35
21066161-106616199.823100.63
31052487-105248798.54399.35
41096259-1096259102.641103.47
51076661-1076661100.807101.62
61078753-1078753101.002101.82
极限11073323-1073323100.494100.271.35101.47101.251.35
21063252-106325299.551100.52
31049250-104925098.24099.21
41093056-1093056102.342103.34
51071324-1071324100.307101.29
61075288-1075288100.678101.66
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.279321819313669325519318149311239318070.07
217.239345129342229343670.03
单位质量响应值RSD%判断
53955.2454229.080.36数据可信
长期12月-供试品溶液-2024052111批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1998185-99818593.43992.031.3293.4492.031.32
2976959-97695991.45291.45
3981282-98128291.85691.86
4996978-99697893.32693.33
5981514-98151491.87891.88
6963825-96382590.22290.22
10min11020134-102013495.49396.440.8295.6596.600.82
21029057-102905796.32996.48
31033178-103317896.71496.87
41044225-104422597.74897.90
51031451-103145196.55396.71
61023613-102361395.81995.97
15min11026349-102634996.07597.981.1596.3998.301.15
21046405-104640597.95398.27
31050208-105020898.30998.62
41061742-106174299.38899.71
51053384-105338498.60698.92
61042393-104239397.57797.89
20min11032195-103219596.62298.681.1497.1099.161.13
21055025-105502598.75999.24
31054430-105443098.70499.18
41065361-106536199.727100.21
51064285-106428599.626100.10
61053806-105380698.64599.12
30min11040159-104015997.36899.171.0198.0099.811.01
21058274-105827499.06499.70
31060762-106076299.29699.94
41071626-1071626100.313100.96
51066255-106625599.811100.46
61059403-105940399.16999.81
45min11050284-105028498.31699.490.7899.11100.290.78
21061863-106186399.400100.21
31062862-106286299.493100.30
41074004-1074004100.536101.35
51068863-1068863100.055100.87
61058853-105885399.11899.92
极限11056118-105611898.86299.330.5599.82100.310.55
21058383-105838399.074100.05
31060686-106068699.289100.26
41070714-1070714100.228101.21
51065173-106517399.709100.69
61055897-105589798.84199.81
点击查看处理图标(人工保存)
　
原始图谱下载图谱(谢鑫慧 于 2025-06-17 19:27:54 完成)
生成报告数据部分(等待生成报告)
Current page cost:61 ms