非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.651918528191794519180041914469191290419163700.14
29.821954375195366819540220.03
单位质量响应值RSD%判断
198587.56198983.910.15数据可信
供试品溶液-20200718批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11819469-181946982.37683.163.7082.3883.163.70
21902396-190239686.13186.13
31795134-179513481.27581.27
41730138-173013878.33278.33
51898083-189808385.93685.94
61875964-187596484.93484.93
10min12119513-211951395.96195.291.1196.1495.471.11
22114999-211499995.75695.95
32092592-209259294.74294.92
42078635-207863594.11094.28
52138284-213828496.81197.00
62084111-208411194.35894.55
15min12135681-213568196.69395.571.1097.0995.961.10
22115463-211546395.77796.18
32099400-209940095.05095.44
42090446-209044694.64595.03
52139123-213912396.84997.25
62084586-208458694.37994.78
20min12123265-212326596.13195.471.0096.7496.081.00
22115467-211546795.77896.39
32099333-209933395.04795.65
42090071-209007194.62895.22
52138990-213899096.84397.46
62084837-208483794.39195.00
30min12127182-212718296.30895.281.1497.1396.101.15
22112386-211238695.63896.47
32092451-209245194.73695.55
42081240-208124094.22895.03
52135190-213519096.67197.51
62078601-207860194.10994.93
45min12109665-210966595.51594.990.9996.5596.020.99
22107650-210765095.42496.47
32087958-208795894.53295.56
42081819-208181994.25495.27
52128218-212821896.35597.41
62073144-207314493.86194.89
极限12105711-210571195.33694.821.0796.5996.061.07
22104007-210400795.25996.51
32084021-208402194.35495.59
42076509-207650994.01495.24
52127817-212781796.33797.60
62067303-206730393.59794.83
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.651900203190146019008751902687190042319011300.06
29.821903173190373919034560.03
单位质量响应值RSD%判断
197008.29193834.621.15数据可信
供试品溶液-20200718批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11161801-116180153.50967.9828.6053.5167.9828.60
21562730-156273071.97571.98
3798874-79887436.79436.79
41590259-159025973.24373.24
51877931-187793186.49386.49
61864908-186490885.89385.89
10min11990952-199095291.69893.563.2991.8293.713.33
22084800-208480096.02096.18
31918090-191809088.34288.42
42031882-203188293.58393.75
52079277-207927795.76695.96
62082789-208278995.92896.12
15min12110784-211078497.21796.271.6597.5496.631.61
22101215-210121596.77697.15
32129151-212915198.06398.34
42028656-202865693.43593.81
52084689-208468996.01596.42
62086540-208654096.10096.50
20min12116541-211654197.48296.471.5698.0297.041.52
22097291-209729196.59697.18
32140220-214022098.57399.07
42044397-204439794.15994.74
52085818-208581896.06796.69
62082748-208274895.92696.54
30min12119017-211901797.59696.371.6398.3597.161.58
22092800-209280096.38997.19
32139726-213972698.55099.27
42042604-204260494.07794.86
52084128-208412895.98996.82
62076373-207637395.63296.46
45min12112682-211268297.30596.151.6398.2897.161.58
22089323-208932396.22997.25
32135773-213577398.36899.30
42037927-203792793.86294.86
52076671-207667195.64696.69
62073890-207389095.51896.56
极限12109730-210973097.16996.021.7198.3697.241.66
22086569-208656996.10297.33
32134693-213469398.31899.47
42030575-203057593.52394.73
52075638-207563895.59896.86
62071787-207178795.42196.68
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.651941566194173619408121938605193830119402040.09
29.821998559199658319975710.07
单位质量响应值RSD%判断
201057.41203418.640.83数据可信
供试品溶液-20200721批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11967623-196762387.56680.8619.7587.5780.8619.75
21088287-108828748.43348.43
32000186-200018689.01589.02
41896486-189648684.40084.40
51970884-197088487.71187.71
61978427-197842788.04788.05
10min12117348-211734894.22993.603.9494.4293.783.97
21941508-194150886.40486.51
32177302-217730296.89897.10
42113831-211383194.07394.26
52121826-212182694.42994.62
62147216-214721695.55995.75
15min12123406-212340694.49995.181.1794.9095.571.17
22142950-214295095.36995.67
32178098-217809896.93397.35
42114743-211474394.11494.51
52117667-211766794.24494.65
62155672-215567295.93596.34
20min12119076-211907694.30695.021.2194.9295.621.19
22154689-215468995.89196.40
32175178-217517896.80397.43
42111249-211124993.95894.56
52113284-211328494.04994.66
62137101-213710195.10995.73
30min12120426-212042694.36695.161.2895.1995.961.27
22151850-215185095.76596.49
32174661-217466196.78097.62
42110400-211040093.92094.73
52112575-211257594.01794.84
62159164-215916496.09096.92
45min12117005-211700594.21495.031.1495.2596.051.13
22151552-215155295.75296.69
32169803-216980396.56497.62
42118484-211848494.28095.30
52108125-210812593.81994.85
62147373-214737395.56696.61
极限12116222-211622294.17994.831.3295.4296.061.31
22148029-214802995.59596.75
32164765-216476596.34097.61
42103143-210314393.59794.83
52099104-209910493.41894.66
62153279-215327995.82997.09
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.651959148196129819584401956920195454019580690.13
29.821954696195407419543850.03
单位质量响应值RSD%判断
202908.70199020.881.37数据可信
供试品溶液-20200721批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12062993-206299392.39869.7933.2592.4069.7933.26
22039800-203980091.35991.36
31153603-115360351.66851.67
41980366-198036688.69788.70
51124889-112488950.38250.38
6987541-98754144.23044.23
10min12187110-218711097.95792.455.3798.1692.605.42
22151338-215133896.35496.56
31961328-196132887.84487.96
42138269-213826995.76995.97
52028206-202820690.84090.95
61918204-191820485.91386.01
15min12187458-218745897.97294.962.1898.4095.322.23
22146903-214690396.15696.57
32090783-209078393.64293.95
42136731-213673195.70096.11
52100764-210076494.08994.40
62058022-205802292.17592.46
20min12181735-218173597.71695.071.8098.3695.641.86
22146785-214678596.15196.78
32093013-209301393.74294.26
42132269-213226995.50096.12
52101167-210116794.10794.63
62080884-208088493.19993.69
30min12197512-219751298.42395.271.9299.2896.061.96
22146522-214652296.13996.98
32092164-209216493.70494.43
42130354-213035495.41596.25
52102338-210233894.16094.89
62094260-209426093.79894.50
45min12175194-217519497.42395.051.8198.5096.051.87
22160867-216086796.78197.84
32087853-208785393.51194.45
42125845-212584595.21396.26
52096213-209621393.88694.83
62087644-208764493.50294.41
极限12192093-219209398.18094.832.0099.4796.042.05
22133530-213353095.55796.83
32078044-207804493.07294.21
42120685-212068594.98296.24
52093553-209355393.76694.92
62086395-208639593.44694.56
点击查看处理图标(人工保存)
　
原始图谱下载图谱(吕婷婷 于 2025-06-24 15:59:48 完成)
生成报告数据部分(等待生成报告)
Current page cost:74 ms