非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.651916270191518819109711913607191416819140410.11
29.821936481193685319366670.02
单位质量响应值RSD%判断
198346.22197216.600.41数据可信
供试品溶液-20200722批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11028797-102879746.81668.0934.1846.8268.0934.18
21905042-190504286.68986.69
31934394-193439488.02588.02
41931223-193122387.88187.88
51413227-141322764.30964.31
6765686-76568634.84334.84
10min11989455-198945590.53094.833.9390.6394.983.97
22108024-210802495.92696.12
32128849-212884996.87497.07
42138030-213803097.29197.49
52166219-216621998.57498.72
61973105-197310589.78689.86
15min12110732-211073296.04997.491.6696.3597.851.64
22109005-210900595.97196.38
32133736-213373697.09697.51
42133919-213391997.10497.52
52201766-2201766100.192100.55
62164736-216473698.50798.78
20min12120969-212096996.51597.491.7097.0398.061.67
22101264-210126495.61896.24
32129001-212900196.88197.51
42130058-213005896.92997.56
52197924-2197924100.017100.60
62174585-217458598.95599.45
30min12124585-212458596.68097.361.7197.4198.161.67
22098035-209803595.47196.30
32121634-212163496.54597.39
42124939-212493996.69697.54
52194112-219411299.843100.65
62174020-217402098.92999.64
45min12115137-211513796.25097.963.3297.2098.973.28
22093896-209389695.28396.33
32116695-211669596.32197.38
42133425-213342597.08298.14
52289147-2289147104.168105.20
62168085-216808598.65999.59
极限12111968-211196896.10597.092.0397.2798.322.00
22088978-208897895.05996.31
32112034-211203496.10897.38
42118987-211898796.42597.70
52206981-2206981100.429101.69
62162711-216271198.41499.57
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.651900418190555519024461904117190241819029910.11
29.821966985196931619681500.09
单位质量响应值RSD%判断
197201.14200422.611.15数据可信
供试品溶液-20200722批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12013214-201321491.14279.7325.5691.1479.7325.56
21968479-196847989.11789.12
31936460-193646087.66787.67
4847748-84774838.37938.38
51864057-186405784.38984.39
61936718-193671887.67987.68
10min12145292-214529297.12195.962.9297.3296.132.95
22157652-215765297.68197.88
32168207-216820798.15998.35
42005589-200558990.79790.88
52092339-209233994.72494.91
62148213-214821397.25497.45
15min12149594-214959497.31696.891.0597.7397.281.04
22159192-215919297.75198.17
32131059-213105996.47796.89
42154358-215435897.53297.82
52098698-209869895.01295.41
62147614-214761497.22797.64
20min12145227-214522797.11896.791.1397.7597.391.11
22154863-215486397.55598.19
32127052-212705296.29696.92
42160581-216058197.81498.32
52094670-209467094.83095.44
62144905-214490597.10497.73
30min12143257-214325797.02996.711.2897.8897.531.27
22165484-216548498.03698.88
32121189-212118996.03096.87
42153026-215302697.47298.19
52088865-208886594.56795.39
62145100-214510097.11397.96
45min12135208-213520896.66596.561.1397.7397.591.11
22145153-214515397.11598.18
32147665-214766597.22998.28
42151255-215125597.39198.33
52086276-208627694.45095.48
62131623-213162396.50397.56
极限12135625-213562596.68496.131.1697.9697.381.14
22141117-214111796.93298.22
32110280-211028095.53696.81
42145023-214502397.10998.26
52080018-208001894.16695.41
62127805-212780596.33097.60
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.653962504395877439490133943575394145739510650.24
29.824103042410451141037760.03
单位质量响应值RSD%判断
409436.79417899.801.45数据可信
供试品溶液-20200712批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13350191-335019172.89658.6418.5972.9058.6418.59
22383481-238348151.86251.86
32749538-274953859.82759.83
41894748-189474841.22841.23
52850014-285001462.01362.01
62940818-294081863.98963.99
10min14126586-412658689.79088.473.5189.9588.603.52
24006390-400639087.17487.29
34153018-415301890.36590.50
43820674-382067483.13383.23
54228810-422881092.01492.15
64061320-406132088.37088.51
15min14284857-428485793.23492.180.8793.6092.510.90
24227438-422743891.98492.29
34252722-425272292.53492.87
44182155-418215590.99991.28
54259854-425985492.68993.03
64212909-421290991.66892.01
20min14336744-433674494.36393.331.2294.9393.861.23
24242016-424201692.30192.81
34260158-426015892.69693.24
44245923-424592392.38692.86
54281853-428185393.16893.72
64368074-436807495.04495.59
30min14305933-430593393.69293.170.2994.4793.910.31
24274857-427485793.01693.73
34276799-427679993.05893.80
44282789-428278993.18993.87
54272719-427271992.96993.72
64278713-427871393.10093.85
45min14300906-430090693.58392.900.4294.5793.840.42
24260381-426038192.70193.63
34262406-426240692.74593.70
44279700-427970093.12194.01
54255980-425598092.60593.57
64257326-425732692.63493.59
极限14280829-428082993.14692.690.2994.3493.840.32
24246591-424659192.40193.53
34256632-425663292.61993.78
44254563-425456392.57493.67
54253435-425343592.55093.72
64267379-426737992.85394.02
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.653958886396082639515033949430394422039529730.18
29.824056157405663940563980.01
单位质量响应值RSD%判断
409634.51413075.150.60数据可信
供试品溶液-20200712批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13199697-319969770.00762.8012.6970.0162.8012.69
22969450-296945064.96964.97
32958280-295828064.72564.73
42166688-216668847.40647.41
52854474-285447462.45462.45
63073697-307369767.25067.25
10min14144082-414408290.67091.052.4990.8391.192.51
24184803-418480391.56191.70
34247128-424712892.92493.07
43963387-396338786.71686.82
54200155-420015591.89692.04
64230156-423015692.55392.70
15min14167942-416794291.19292.900.9691.5593.240.95
24243398-424339892.84393.19
34283585-428358593.72294.07
44265560-426556093.32793.63
54255927-425592793.11793.46
64260314-426031493.21393.57
20min14214042-421404292.20093.030.5892.7693.580.57
24237914-423791492.72393.28
34278477-427847793.61094.17
44277006-427700693.57894.08
54246328-424632892.90793.46
64256892-425689293.13893.70
30min14156357-415635790.93892.741.0491.7093.501.03
24231604-423160492.58593.34
34271982-427198293.46894.23
44278576-427857693.61294.33
54243520-424352092.84593.60
64250559-425055992.99993.77
45min14142197-414219790.62892.401.0491.6093.361.02
24219587-421958792.32293.29
34265572-426557293.32894.30
44256083-425608393.12094.04
54229701-422970192.54393.51
64226275-422627592.46893.44
极限14136036-413603690.49492.220.9891.6693.390.96
24215767-421576792.23893.41
34242991-424299192.83494.02
44245891-424589192.89794.03
54214594-421459492.21293.38
64234899-423489992.65793.84
点击查看处理图标(人工保存)
　
原始图谱下载图谱(吕婷婷 于 2025-06-24 16:06:44 完成)
生成报告数据部分(等待生成报告)
Current page cost:85 ms