非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.653875171387863938791333881352387392438776440.08
29.823951488395667539540820.10
单位质量响应值RSD%判断
401828.39402656.010.15数据可信
供试品溶液-20200709批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11703112-170311238.10656.6725.2838.1156.6725.28
23165080-316508070.81770.82
33022082-302208267.61867.62
42780886-278088662.22162.22
51756082-175608239.29239.29
62768916-276891661.95361.95
10min13898170-389817087.22090.404.5187.3090.524.54
24210258-421025894.20394.36
34184970-418497093.63793.79
44162239-416223993.12893.27
53755843-375584384.03584.12
64029779-402977990.16590.30
15min14223960-422396094.50994.071.4394.7994.391.45
24222943-422294394.48794.85
34244836-424483694.97795.33
44217270-421727094.36094.70
54083631-408363191.37091.64
64232045-423204594.69095.03
20min14337196-433719697.04395.621.1697.5396.161.15
24277489-427748995.70796.28
34320726-432072696.67597.24
44267311-426731195.47996.03
54216365-421636594.33994.82
64223395-422339594.49795.05
30min14351113-435111397.35495.331.2398.0696.081.22
24249666-424966695.08595.87
34284225-428422595.85896.64
44251392-425139295.12395.89
54202435-420243594.02894.71
64225824-422582494.55195.31
45min14343078-434307897.17595.211.1098.1096.171.08
24246186-424618695.00796.01
34262550-426255095.37396.37
44233144-423314494.71595.69
54238613-423861394.83795.73
64207948-420794894.15195.12
极限14332820-433282096.94595.081.0698.0896.251.04
24234061-423406194.73595.95
34264714-426471495.42196.63
44224282-422428294.51795.71
54209778-420977894.19295.30
64229868-422986894.64295.82
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.653969839396767239687483966717396740939680770.04
29.823982037397848339802600.07
单位质量响应值RSD%判断
411199.69405321.791.02数据可信
供试品溶液-20200709批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12594508-259450857.19858.9422.7457.2058.9422.74
23130475-313047569.01469.01
32581096-258109656.90356.90
41549371-154937134.15734.16
53158214-315821469.62669.63
63028124-302812466.75866.76
10min14184231-418423192.24590.083.5892.3790.213.60
24106010-410601090.52190.67
33910738-391073886.21686.34
43897112-389711285.91585.99
54207537-420753792.75992.91
64209754-420975492.80892.96
15min14239610-423961093.46693.080.8993.8093.410.91
24250339-425033993.70294.06
34163794-416379491.79492.11
44200646-420064692.60792.87
54213239-421323992.88593.25
64265468-426546894.03694.39
20min14247600-424760093.64293.941.0594.1894.481.03
24314609-431460995.11995.68
34220027-422002793.03493.56
44309121-430912194.99895.47
54207798-420779892.76593.33
64267810-426781094.08894.65
30min14217790-421779092.98593.691.2393.7394.441.19
24246837-424683793.62594.40
34263701-426370193.99794.73
44338081-433808195.63796.32
54181831-418183192.19292.97
64250645-425064593.70994.48
45min14214408-421440892.91093.431.0693.8694.391.02
24224428-422442893.13194.11
34280763-428076394.37395.31
44303311-430331194.87095.77
54183062-418306292.21993.20
64222660-422266093.09294.07
极限14191440-419144092.40493.051.0693.5694.221.02
24225131-422513193.14794.34
34235720-423572093.38094.53
44298180-429818094.75795.86
54170580-417058091.94493.13
64204043-420404392.68293.87
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.653858870385572938572013864577385650838585770.10
29.824007623400575240066880.04
单位质量响应值RSD%判断
399852.54408013.031.43数据可信
供试品溶液-20200710批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12851196-285119663.53456.6621.6563.5356.6621.65
22957014-295701465.89265.89
32196095-219609548.93648.94
42998261-299826166.81166.81
52662139-266213959.32159.32
61591005-159100535.45335.45
10min14219758-421975894.03089.837.2394.1789.957.25
24196128-419612893.50393.65
34031638-403163889.83889.95
44177934-417793493.09893.25
54108079-410807991.54191.67
63453221-345322176.94977.03
15min14337212-433721296.64793.752.6397.0094.082.66
24239501-423950194.47094.82
34268424-426842495.11495.42
44226155-422615594.17294.53
54156668-415666892.62492.96
64015950-401595089.48889.74
20min14325946-432594696.39694.201.6496.9694.741.65
24244759-424475994.58795.15
34273582-427358295.22995.75
44216631-421663193.96094.52
54139211-413921192.23592.78
64165579-416557992.82293.27
30min14339250-433925096.69294.541.5797.4795.281.57
24234499-423449994.35895.13
34290854-429085495.61496.35
44208185-420818593.77294.55
54146875-414687592.40693.15
64235112-423511294.37295.03
45min14317187-431718796.20194.391.4597.1995.341.46
24226362-422636294.17795.16
34280975-428097595.39496.34
44247032-424703294.63795.62
54141620-414162092.28993.24
64202871-420287193.65394.52
极限14289585-428958595.58693.881.5296.7995.041.50
24196770-419677093.51894.71
34250626-425062694.71895.87
44199993-419999393.58994.78
54103150-410315091.43192.59
64238543-423854394.44895.52
点击查看处理图标(人工保存)
　
原始图谱(等待粘贴贴图标)
Current page cost:71 ms