苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 14.679202592028920649207891899920190.08
2 14.649188091896918880.02
单位质量响应值RSD%判断
6272.606276.500.05数据可信
供试品溶液-25061701批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min155489-5548962.04069.6112.8662.0469.6112.85
267235-6723575.17375.17
358788-5878865.72965.73
455138-5513861.64861.65
575866-7586684.82384.82
661023-6102368.22768.23
10min176233-7623385.23388.144.0185.8588.844.04
277264-7726486.38687.14
382357-8235792.08092.74
475189-7518984.06684.68
582663-8266392.42293.27
679318-7931888.68289.36
15min175708-7570884.64687.964.4486.1289.544.44
276780-7678085.84587.46
384145-8414594.07995.66
475675-7567584.60986.07
581684-8168491.32893.10
678053-7805387.26888.84
20min176033-7603385.01087.641.9787.3390.101.97
278086-7808687.30589.78
380268-8026889.74592.26
478072-7807287.28989.59
577917-7791787.11689.80
679932-7993289.36991.81
30min176761-7676185.82388.493.0488.9991.822.96
279831-7983189.25692.60
382479-8247992.21795.63
481020-8102090.58593.76
578389-7838987.64491.20
676392-7639285.41188.75
45min174638-7463883.45085.672.3587.4889.892.31
279021-7902188.35092.59
378429-7842987.68892.03
476711-7671185.76889.85
576015-7601584.98989.42
674948-7494883.79687.99
60min175099-7509983.96586.091.6888.8391.161.70
277090-7709086.19191.31
377888-7788887.08492.30
475943-7594384.90989.85
577348-7734886.48091.76
678619-7861987.90192.93
极限177171-7717186.28286.682.8891.9892.622.75
277513-7751386.66492.65
381747-8174791.39897.48
475785-7578584.73290.52
575573-7557384.49590.64
677381-7738186.51792.42
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 14.679194491997919049195391866919330.06
2 14.649192991973919510.04
单位质量响应值RSD%判断
6266.736280.810.16数据可信
供试品溶液-25061701批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min174397-7439783.19179.506.6083.1979.506.60
274314-7431483.09883.10
362322-6232269.68969.69
474042-7404282.79482.79
569588-6958877.81377.81
671907-7190780.40780.41
10min184059-8405993.99591.723.3894.8392.523.41
284878-8487894.91195.74
377080-7708086.19186.89
482244-8224491.96592.79
581072-8107290.65591.43
682837-8283792.62893.43
15min184117-8411794.06090.373.0595.8392.083.07
282555-8255592.31394.09
376971-7697186.06987.63
479568-7956888.97390.72
580830-8083090.38492.07
680856-8085690.41392.14
20min182589-8258992.35191.352.9495.0693.972.96
283833-8383393.74296.45
377127-7712786.24488.66
481163-8116390.75793.39
582632-8263292.39994.99
682822-8282292.61295.25
30min183092-8309292.91489.613.5396.5593.143.54
282149-8214991.85995.50
375286-7528684.18587.47
480212-8021289.69393.24
578691-7869187.99291.50
681393-8139391.01494.57
45min182585-8258592.34790.112.5796.9194.542.61
283108-8310892.93197.49
377461-7746186.61790.74
480321-8032189.81594.26
580559-8055990.08194.47
679486-7948688.88193.35
60min182226-8222691.94590.381.6097.4395.711.68
282016-8201691.71097.20
378982-7898288.31893.31
479757-7975789.18494.52
580588-8058890.11495.41
681396-8139691.01796.38
极限183104-8310492.92790.831.4399.3497.071.42
281695-8169591.35197.76
381306-8130690.91696.79
479616-7961689.02795.26
581010-8101090.58596.78
680668-8066890.20396.47
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 14.679237992396924449248392456924320.05
2 14.649260692724926650.10
单位质量响应值RSD%判断
6300.756329.580.33数据可信
供试品溶液-25061701批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min147031-4703152.24643.1527.0252.2543.1527.03
244463-4446349.39349.39
327978-2797831.08031.08
436442-3644240.48340.48
551373-5137357.06957.07
625758-2575828.61428.61
10min174158-7415882.38076.927.8882.9077.357.99
272585-7258580.63381.13
364375-6437571.51371.82
466602-6660273.98774.39
575284-7528483.63184.20
662437-6243769.36069.65
15min174493-7449382.75380.055.5884.1081.255.71
275703-7570384.09785.40
368302-6830275.87576.90
468674-6867476.28877.43
576810-7681085.32686.73
668393-6839375.97676.96
20min174312-7431282.55180.406.2684.7382.406.35
276458-7645884.93587.08
370511-7051178.32980.11
467417-6741774.89276.80
577959-7795986.60388.86
667598-6759875.09376.83
30min174876-7487683.17881.793.5886.1884.603.75
275486-7548683.85686.85
370928-7092878.79281.36
470881-7088178.74081.40
577241-7724185.80588.93
672340-7234080.36182.85
45min175954-7595484.37682.564.5288.2186.194.65
278307-7830786.98990.82
371268-7126879.17082.53
470979-7097978.84982.29
577632-7763286.24090.22
671805-7180579.76683.06
60min175448-7544883.81382.294.0788.4986.744.21
277785-7778586.41091.11
372761-7276180.82884.98
471154-7115479.04383.28
576754-7675485.26490.11
670576-7057678.40182.49
极限179210-7921087.99387.541.0193.5192.821.16
277930-7793086.57192.13
379092-7909287.86192.82
477998-7799886.64691.67
580008-8000888.87994.58
678596-7859687.31092.19
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