苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%) 96.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 14.058587886095858978592485998859580.11
2 14.038591085930859200.02
单位质量响应值RSD%判断
6118.016124.020.07数据可信
供试品溶液-FX3469批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min163451-6345172.12473.082.0072.1273.082.00
265962-6596274.97874.98
364336-6433673.13073.13
462786-6278671.36871.37
565668-6566874.64474.64
663533-6353372.21772.22
10min178294-7829488.99588.991.3689.7289.721.36
277857-7785788.49989.25
378043-7804388.71089.44
476757-7675787.24887.96
579944-7994490.87191.62
678862-7886289.64190.36
15min179772-7977290.67591.481.4292.2993.101.40
279073-7907389.88191.52
380489-8048991.49093.11
480557-8055791.56893.15
582475-8247593.74895.40
680532-8053291.53993.16
20min181766-8176692.94293.610.8695.4696.140.87
281978-8197893.18395.72
382426-8242693.69296.23
481606-8160692.76095.26
583412-8341294.81397.41
682922-8292294.25696.79
30min183221-8322194.59695.200.6898.0498.670.68
282922-8292294.25697.72
383900-8390095.36898.84
483882-8388295.34798.78
584236-8423695.75099.29
684353-8435395.88399.36
45min184077-8407795.56996.691.1099.96101.111.08
284895-8489596.499100.91
386220-8622098.005102.43
483902-8390295.37099.75
585653-8565397.360101.86
685627-8562797.331101.77
60min184508-8450896.05996.631.07101.41102.021.05
285152-8515296.791102.16
385933-8593397.679103.08
483439-8343994.844100.18
585400-8540097.073102.54
685617-8561797.319102.73
极限183929-8392995.40195.780.97101.71102.130.95
284713-8471396.292102.63
385046-8504696.670103.05
482775-8277594.089100.37
584642-8464296.211102.65
684459-8445996.003102.38
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%) 96.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 14.058616986085860358587285875860070.16
2 14.038571686368860420.54
单位质量响应值RSD%判断
6121.496132.720.13数据可信
供试品溶液-FX3469批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min163694-6369472.32876.429.0172.3376.429.01
262901-6290171.42771.43
371331-7133181.00081.00
463670-6367072.30172.30
577924-7792488.48788.49
664287-6428773.00173.00
10min175881-7588186.16793.156.2186.8993.926.22
276791-7679187.20087.91
386090-8609097.76098.57
480424-8042491.32692.05
588120-88120100.065100.95
684891-8489196.39897.13
15min178727-7872789.39994.945.3290.9896.645.35
279604-7960490.39591.98
387854-8785499.763101.55
481083-8108392.07493.71
589272-89272101.373103.26
685123-8512396.66298.36
20min180773-8077391.72296.303.6794.2098.953.74
282473-8247393.65396.14
388015-8801599.946102.73
483166-8316694.43997.00
588240-88240100.201103.10
686174-8617497.855100.52
30min182543-8254393.73296.922.7997.13100.532.79
283316-8331694.61098.04
387883-8788399.796103.58
485823-8582397.457100.96
584269-8426995.69299.59
688269-88269100.234103.87
45min183291-8329194.58197.082.0298.91101.652.04
284137-8413795.54299.91
385876-8587697.517102.30
486430-8643098.146102.62
585062-8506296.592101.45
688136-88136100.083104.72
60min180613-8061391.54095.442.6096.82100.982.61
282333-8233393.49498.82
385164-8516496.708102.47
485691-8569197.307102.76
584143-8414395.549101.37
686312-8631298.012103.65
极限181875-8187592.97395.422.5399.17101.932.52
281700-8170092.77599.04
386028-8602897.689104.41
485074-8507496.606103.04
583002-8300294.253101.03
686523-8652398.251104.87
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%) 96.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 14.058595785795861748606586107860200.18
2 14.038555785748856520.16
单位质量响应值RSD%判断
6122.426104.920.21数据可信
供试品溶液-8145761批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min171739-7173981.64383.634.6681.6483.634.66
274139-7413984.37484.37
370754-7075480.52280.52
473547-7354783.70083.70
579863-7986390.88890.89
670855-7085580.63780.64
10min180355-8035591.44894.483.6992.2695.313.70
281892-8189293.19794.04
382238-8223893.59194.40
481726-8172693.00893.85
589036-89036101.327102.24
682844-8284494.28195.09
15min183213-8321394.70196.212.4296.4398.002.45
284357-8435796.00397.78
382813-8281394.24595.99
483688-8368895.24197.01
588460-88460100.672102.59
684728-8472896.42598.17
20min183002-8300294.46096.171.9297.1498.921.93
285238-8523897.00599.74
383702-8370295.25797.94
482624-8262494.03096.75
586441-8644198.374101.30
686032-8603297.909100.62
30min184338-8433895.98196.151.8899.6099.861.86
284080-8408095.68799.39
384144-8414495.76099.40
482042-8204293.36897.03
585565-8556597.377101.29
686748-8674898.724102.42
45min183379-8337994.89095.692.4599.47100.362.39
283613-8361395.15699.82
384663-8466396.351100.94
480739-8073991.88596.48
585269-8526997.040101.93
686820-8682098.806103.49
60min182861-8286194.30094.222.1699.8399.842.09
281001-8100192.18397.80
383338-8333894.843100.40
480711-8071191.85397.37
583198-8319894.684100.54
685611-8561197.430103.10
极限182882-8288294.32493.782.46100.80100.352.37
282025-8202593.34999.88
382003-8200393.32499.83
479344-7934490.29796.73
582529-8252993.922100.73
685649-8564997.473104.12
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%) 96.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 14.058568585663856768586086038857840.20
2 14.038613086175861520.04
单位质量响应值RSD%判断
6105.626140.560.41数据可信
供试品溶液-8145761批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min167911-6791177.16880.213.1877.1780.213.17
273834-7383483.89883.90
370050-7005079.59879.60
468457-6845777.78877.79
572026-7202681.84481.84
671258-7125880.97180.97
10min180320-8032091.26892.592.6692.0493.392.66
285527-8552797.18598.02
380928-8092891.95992.75
479801-7980190.67891.46
580057-8005790.96991.79
682256-8225693.46894.28
15min181936-8193693.10493.962.1994.7995.682.19
286303-8630398.06799.88
381516-8151692.62794.34
482345-8234593.56995.25
581681-8168192.81594.54
682332-8233293.55495.30
20min183488-8348894.86894.492.4797.4897.162.45
287125-8712599.001101.79
381905-8190593.06995.71
481758-8175892.90295.52
582605-8260593.86596.52
682043-8204393.22695.91
30min183349-8334994.71095.811.9198.2799.421.92
287304-8730499.204102.99
382794-8279494.07997.65
484750-8475096.30299.85
583577-8357794.96998.56
684106-8410695.57099.18
45min182270-8227093.48495.181.9298.0099.751.93
286733-8673398.555103.33
382643-8264393.90898.42
483605-8360595.00199.51
583185-8318594.52499.07
684155-8415595.626100.19
60min179855-7985590.74093.701.9496.1999.221.90
284053-8405395.510101.27
381503-8150392.61298.06
483696-8369695.104100.57
582252-8225293.46398.95
683397-8339794.765100.29
极限178080-7808088.72392.592.8495.0899.052.72
283079-8307994.403101.12
379533-7953390.37496.75
484356-8435695.854102.27
582120-8212093.31399.74
681714-8171492.85299.32
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