苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%) 96.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 14.058433984312844608447884329843840.10
2 14.038436884470844190.09
单位质量响应值RSD%判断
6005.986017.030.13数据可信
供试品溶液-8145761批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min153032-5303261.37969.577.9661.3869.587.96
258582-5858267.80267.80
363307-6330773.27173.27
456643-5664365.55865.56
564271-6427174.38774.39
664845-6484575.05175.05
10min160683-6068370.23480.658.5270.8581.358.52
268996-6899679.85580.53
371766-7176683.06183.79
465636-6563675.96676.62
573778-7377885.39086.13
677251-7725189.41090.16
15min163984-6398474.05484.258.5075.3785.768.49
272103-7210383.45184.93
373369-7336984.91786.48
468440-6844079.21280.63
577813-7781390.06091.66
681068-8106893.82795.47
20min165315-6531575.59586.158.4977.6588.498.49
274063-7406385.72088.03
374966-7496686.76589.18
470405-7040581.48683.69
578120-7812090.41592.91
683718-8371896.89499.48
30min168514-6851479.29788.447.1882.1191.647.21
276539-7653988.58591.75
376144-7614488.12891.41
473354-7335484.89987.92
579049-7904991.49094.89
684865-8486598.222101.77
45min171947-7194783.27190.645.8386.8894.735.91
279851-7985192.41996.47
379293-7929391.77395.93
474302-7430285.99689.87
579645-7964592.18096.50
684822-8482298.172102.71
60min173148-7314884.66190.734.3089.1095.734.46
279492-7949292.00396.98
379297-7929791.77896.86
476013-7601387.97792.71
579500-7950092.01297.25
682897-8289795.944101.46
极限178889-7888991.30594.852.9396.59100.763.06
282321-8232195.277101.18
385155-8515598.558104.55
480509-8050993.18098.79
580646-8064693.33999.50
684207-8420797.460103.94
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%) 96.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 14.058424384179843088431584225842540.07
2 14.038446384520844920.05
单位质量响应值RSD%判断
5996.736022.240.31数据可信
供试品溶液-8145761批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min151175-5117559.25063.924.9559.2563.924.95
256784-5678465.74465.74
357975-5797567.12367.12
456404-5640465.30465.30
556475-5647565.38665.39
652421-5242160.69260.69
10min167652-6765278.32680.945.6378.9281.585.62
271682-7168282.99283.65
372825-7282584.31684.99
470317-7031781.41282.06
573784-7378485.42686.08
663176-6317673.14473.75
15min175405-7540587.30388.933.8788.6890.383.88
278005-7800590.31391.80
377382-7738289.59291.11
478237-7823790.58292.05
580192-8019292.84594.35
671627-7162782.92984.27
20min180157-8015792.80492.903.6795.0595.233.66
280331-8033193.00695.40
379335-7933591.85394.26
482164-8216495.12897.50
584075-8407597.34199.78
675349-7534987.23889.41
30min185511-8551199.00397.361.24102.18100.621.25
283497-8349796.67199.99
383617-8361796.810100.14
483788-8378897.008100.33
585231-8523198.679102.09
682898-8289895.97899.02
45min183950-8395097.19695.671.35101.3699.911.33
282430-8243095.43699.72
382720-8272095.772100.07
483817-8381797.042101.34
581670-8167094.55698.95
681192-8119294.00398.00
60min184617-8461797.96896.111.44103.11101.311.41
282367-8236795.363100.60
381723-8172394.61899.87
483465-8346596.634101.90
584007-8400797.262102.60
681916-8191694.84199.78
极限183248-8324896.38395.100.89102.50101.260.88
281832-8183294.744100.94
381364-8136494.202100.40
482027-8202794.970101.20
582765-8276595.824102.14
681595-8159594.469100.36
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%) 96.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 14.058451484657845928460684659846060.08
2 14.038443684313843740.11
单位质量响应值RSD%判断
6021.786013.830.10数据可信
供试品溶液-8145761批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125539-2553929.52830.588.0329.5330.588.03
224580-2458028.41928.42
328476-2847632.92332.92
429022-2902233.55533.55
523828-2382827.54927.55
627233-2723331.48631.49
10min135835-3583541.43243.704.8741.7344.004.89
236950-3695042.72143.00
338926-3892645.00545.33
440924-4092447.31547.65
536698-3669842.42942.70
637456-3745643.30643.62
15min140578-4057846.91550.395.4747.6251.135.46
242005-4200548.56549.28
345408-4540852.50053.28
446668-4666853.95754.77
544814-4481451.81352.51
642002-4200248.56249.31
20min146066-4606653.26155.965.5154.4457.215.50
246188-4618853.40254.60
351320-5132059.33560.64
451672-5167259.74261.09
549102-4910256.77157.99
646055-4605553.24854.48
30min152346-5234660.52163.874.5562.2365.674.57
253394-5339461.73363.46
357003-5700365.90667.80
458961-5896168.16970.12
555985-5598564.72966.51
653741-5374162.13463.90
45min160411-6041169.84671.993.7572.1674.433.79
260333-6033369.75672.10
362949-6294972.78075.34
466317-6631776.67479.30
562952-6295272.78475.22
660617-6061770.08472.47
60min164556-6455674.63877.433.6577.6580.593.69
265361-6536175.56978.61
368099-6809978.73582.02
470904-7090481.97885.37
567883-6788378.48581.65
665010-6501075.16378.25
极限182069-8206994.88695.862.6098.6599.802.39
284064-8406497.193100.99
381403-8140394.11698.19
479883-7988392.35996.57
585650-8565099.027102.97
684382-8438297.561101.40
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