苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%) 96.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.058497284674849138495684930848890.15
214.038575985882858200.11
单位质量响应值RSD%判断
6041.926116.890.88数据可信
供试品溶液-8145761批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min156215-5621564.33868.085.6664.3468.085.66
258065-5806566.45666.46
359138-5913867.68467.68
456355-5635564.49964.50
563126-6312672.24872.25
664024-6402473.27673.28
10min169397-6939779.42580.241.6980.0780.921.71
270147-7014780.28480.95
371226-7122681.51982.20
468182-6818278.03578.68
570380-7038080.55081.27
671299-7129981.60282.33
15min174278-7427885.01284.661.9086.4586.141.89
273251-7325183.83685.30
376252-7625287.27188.76
472033-7203382.44283.87
573636-7363684.27785.80
674370-7437085.11786.67
20min175914-7591486.88487.141.9989.1789.481.98
277181-7718188.33490.64
377985-7798589.25491.62
473575-7357584.20786.46
575698-7569886.63789.01
676496-7649687.55089.95
30min176739-7673987.82889.341.7290.9892.541.71
279686-7968691.20194.39
378869-7886990.26693.52
476402-7640287.44390.53
577622-7762288.83992.08
679039-7903990.46193.74
45min178067-7806789.34890.231.9293.3894.331.87
281009-8100992.71596.82
377141-7714188.28892.45
477520-7752088.72292.69
579959-7995991.51495.64
679343-7934390.80894.99
60min177473-7747388.66889.981.5793.6094.981.54
280921-8092192.61597.64
378388-7838889.71594.76
477810-7781089.05493.91
578187-7818789.48594.53
678935-7893590.34295.43
极限179674-7967491.18792.581.7897.0098.481.69
282976-8297694.966100.92
379844-7984491.38297.32
480886-8088692.57498.32
582282-8228294.172100.11
679683-7968391.19897.19
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%) 96.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.058491984769846968486484714847920.12
214.038538385052852180.28
单位质量响应值RSD%判断
6035.026073.980.46数据可信
供试品溶液-8145761批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min153124-5312461.04959.794.4461.0559.794.44
251434-5143459.10759.11
348480-4848055.71255.71
454721-5472162.88462.88
553818-5381861.84761.85
650592-5059258.13958.14
10min168901-6890179.18077.634.9179.7978.234.91
266880-6688076.85777.45
362138-6213871.40871.96
471037-7103781.63482.26
570466-7046680.97881.60
665911-6591175.74476.33
15min175934-7593487.26286.644.6288.6688.014.62
274997-7499786.18587.54
369530-6953079.90381.17
478404-7840490.10091.55
579301-7930191.13192.56
674191-7419185.25986.60
20min181294-8129493.42291.495.6195.7093.745.59
279353-7935391.19193.41
371861-7186182.58184.65
483862-8386296.37398.72
583535-8353595.99798.34
677794-7779489.39991.59
30min182723-8272395.06495.454.4998.2798.614.49
283296-8329695.72298.86
376432-7643287.83490.73
486432-8643299.326102.64
586754-8675499.696103.00
682717-8271795.05798.14
45min179839-7983991.75095.883.1995.9199.983.19
285460-8546098.209102.30
380933-8093393.00796.78
485483-8548398.236102.54
586150-8615099.002103.30
682710-8271095.04999.08
60min178308-7830889.99095.513.6695.07100.583.54
285800-8580098.600103.67
380748-8074892.79497.50
483277-8327795.700100.99
584591-8459197.210102.50
685947-8594798.769103.76
极限181658-8165893.84095.271.2599.82101.291.15
283017-8301795.402101.46
383016-8301695.400101.03
482057-8205794.298100.54
583016-8301695.400101.66
684634-8463497.260103.23
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%) 96.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.058514184890850498498485293850710.19
214.038468084510845950.15
单位质量响应值RSD%判断
6054.886029.580.30数据可信
供试品溶液-8145761批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min124102-2410227.75429.815.8327.7529.805.83
224862-2486228.62928.63
325472-2547229.33129.33
427654-2765431.84431.84
525429-2542929.28229.28
627791-2779132.00232.00
10min133373-3337338.42941.365.5838.7141.665.57
233620-3362038.71439.00
336022-3602241.48041.77
438201-3820143.98944.31
537195-3719542.83043.12
637119-3711942.74343.06
15min139213-3921345.15447.974.7645.8248.684.76
239226-3922645.16945.84
341780-4178048.11048.82
443296-4329649.85650.61
543428-4342850.00850.73
643020-4302049.53850.29
20min145925-4592552.88353.802.4954.0055.002.52
245001-4500151.81952.94
346601-4660153.66154.85
447069-4706954.20055.46
548275-4827555.58956.81
647479-4747954.67355.92
30min151655-5165559.48161.764.0561.1263.494.04
250520-5052058.17459.82
354186-5418662.39664.12
453872-5387262.03463.83
556192-5619264.70666.48
655375-5537563.76565.55
45min159294-5929468.27870.414.7070.5172.764.67
256532-5653265.09767.32
361100-6110070.35772.71
462879-6287972.40674.82
564538-6453874.31676.74
662539-6253972.01474.44
60min163131-6313172.69675.293.6475.6278.343.63
263552-6355273.18176.06
363063-6306372.61875.67
467181-6718177.36080.50
568206-6820678.54081.71
667177-6717777.35580.50
极限178894-7889490.84795.472.8894.4999.282.80
285390-8539098.327101.94
383794-8379496.490100.27
482576-8257695.08799.00
584950-8495097.821101.77
681860-8186094.26398.18
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