他克莫司颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号130550-202401对照品来源中检所对照品使用方法直接使用
对照品含量(%)97.9对照品水分(%)0对照品稀释倍数17500
标示量(mg)1供试品稀释倍数1.4系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.881511661515391511571513481509271512270.16
213.891511541505481508510.29
单位质量响应值RSD%判断
10895.3210860.400.23数据可信
供试品溶液-2025051921批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min164901-6490142.05641.083.6542.0641.083.65
262413-6241340.44340.44
359640-5964038.64738.65
463687-6368741.26941.27
566443-6644343.05543.05
663248-6324840.98440.98
10min192368-9236859.85460.192.9260.3260.642.92
293228-9322860.41160.86
388953-8895357.64158.07
495579-9557961.93562.39
596085-9608562.26362.74
691075-9107559.01659.47
15min1105286-10528668.22568.392.0969.3669.522.07
2109033-10903370.65371.77
3104655-10465567.81668.89
4103100-10310066.80867.96
5107232-10723269.48670.66
6103977-10397767.37768.49
20min1114777-11477774.37576.343.2376.2778.223.18
2121215-12121578.54780.45
3111594-11159472.31374.14
4120603-12060378.15080.04
5118804-11880476.98578.93
6119835-11983577.65379.51
30min1129843-12984384.13885.612.1686.8588.342.13
2133799-13379986.70189.48
3128650-12865083.36585.99
4135396-13539687.73690.49
5130344-13034484.46287.26
6134683-13468387.27490.00
45min1140088-14008890.77792.573.0794.4396.253.00
2141771-14177191.86795.61
3137646-13764689.19492.75
4150522-15052297.538101.27
5143451-14345192.95696.69
6143634-14363493.07496.77
60min1144632-14463293.72194.272.0798.3898.992.04
2143730-14373093.13797.90
3142493-14249392.33596.88
4151041-15104197.874102.69
5144652-14465293.73498.50
6146358-14635894.84099.57
90min1149103-14910396.61896.372.51102.32102.132.46
2149134-14913496.638102.44
3144404-14440493.57399.14
4155387-155387100.690106.59
5146411-14641194.874100.68
6147868-14786895.818101.60
极限1146445-14644594.89694.702.20101.67101.532.16
2144921-14492193.908100.78
3142237-14223792.16998.78
4151617-15161798.247105.27
5144320-14432093.519100.38
6147273-14727395.432102.28
他克莫司颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号130550-202401对照品来源中检所对照品使用方法直接使用
对照品含量(%)97.9对照品水分(%)0对照品稀释倍数17500
标示量(mg)1供试品稀释倍数1.4系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.881514491511361510171507651509111510560.18
213.891515751507121511440.41
单位质量响应值RSD%判断
10883.0010881.500.01数据可信
供试品溶液-2025051921批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min165241-6524142.25942.625.4642.2642.625.46
270237-7023745.49545.49
363863-6386341.36641.37
469644-6964445.11145.11
565047-6504742.13342.13
660773-6077339.36539.36
10min1101479-10147965.73161.265.8766.2061.735.85
298045-9804563.50764.01
392230-9223059.74060.20
497370-9737063.07063.57
592480-9248059.90260.37
685836-8583655.59956.04
15min1116925-11692575.73672.454.6776.9473.604.64
2109265-10926570.77571.99
3116128-11612875.22076.34
4112099-11209972.61073.81
5113843-11384373.74074.87
6102844-10284466.61667.67
20min1123120-12312079.74979.252.3081.7981.212.34
2123147-12314779.76681.76
3121713-12171378.83880.80
4126477-12647781.92383.93
5121837-12183778.91880.87
6117811-11781176.31078.11
30min1129342-12934283.77987.243.7986.7190.093.72
2141515-14151591.66494.55
3135942-13594288.05490.89
4139426-13942690.31193.23
5132135-13213585.58888.42
6129794-12979484.07286.72
45min1142667-14266792.41093.482.9596.2797.282.94
2150964-15096497.784101.69
3144086-14408693.32997.14
4146370-14637094.80998.73
5143673-14367393.06296.84
6138106-13810689.45693.03
60min1145833-14583394.46195.783.1599.35100.633.11
2155561-155561100.762105.75
3145643-14564394.33899.19
4148332-14833296.080101.06
5149925-14992597.111101.93
6141943-14194391.94196.51
90min1149471-14947196.81798.323.12102.75104.233.09
2156677-156677101.485107.59
3155434-155434100.680106.58
4154121-15412199.829105.87
5151200-15120097.937103.83
6143839-14383993.16998.76
极限1147287-14728795.40396.432.90102.41103.442.89
2152693-15269398.904106.14
3149508-14950896.841103.86
4152709-15270998.915106.07
5149867-14986797.074104.06
6141168-14116891.43998.07
点击查看处理图标(人工保存)
　
原始图谱下载图谱(姜进硙 于 2025-07-23 16:21:55 完成)
生成报告数据部分(等待生成报告)
Current page cost:45 ms