非奈利酮片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号D231201对照品来源自制对照品使用方法直接使用
对照品含量(%)99.92对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.023797383798373797173800153802193799050.06
210.883780143778033779080.04
单位质量响应值RSD%判断
34474.1434734.190.54数据可信
供试品溶液-BXJUS91批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min16319-63198.2118.5718.098.218.5718.08
26754-67548.7768.78
35924-59247.6987.70
45094-50946.6196.62
56822-68228.8658.86
68658-865811.25011.25
10min119833-1983325.77126.628.9325.8226.678.93
219767-1976725.68525.73
322601-2260129.36829.41
417840-1784023.18123.22
520333-2033326.42126.47
622554-2255429.30729.37
15min127782-2778236.10036.768.5136.2936.968.51
226769-2676934.78434.98
331467-3146740.88841.09
424992-2499232.47532.64
528122-2812236.54236.74
630608-3060839.77240.00
20min133501-3350143.53143.638.1643.9244.038.16
233183-3318343.11843.50
337279-3727948.44048.87
429106-2910637.82038.17
533011-3301142.89443.29
635399-3539945.99746.44
30min141678-4167854.15653.576.2554.7954.226.26
241987-4198754.55855.18
345025-4502558.50559.21
437135-3713548.25348.81
540140-4014052.15852.80
641409-4140953.80754.51
45min151397-5139766.78565.176.2267.7266.116.23
250129-5012965.13866.06
354322-5432270.58671.61
445084-4508458.58259.41
548599-4859963.15064.08
651383-5138366.76767.77
60min155758-5575872.45272.085.7373.7573.395.74
257340-5734074.50875.80
358673-5867376.24077.66
449452-4945264.25865.41
556149-5614972.96074.24
655477-5547772.08773.46
极限160139-6013978.14577.136.4079.8578.836.39
261108-6110879.40481.11
365087-6508784.57486.42
453682-5368269.75471.26
558193-5819375.61677.30
657942-5794275.29077.06
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