非奈利酮片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号D231201对照品来源自制对照品使用方法直接使用
对照品含量(%)99.92对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.023815343817973814053815983815593815790.04
210.883790743775953783340.28
单位质量响应值RSD%判断
34626.0434773.350.31数据可信
供试品溶液-BXK2XG1批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min15685-56857.3677.8710.117.377.8810.12
26538-65388.4728.47
36220-62208.0608.06
46644-66448.6098.61
55026-50266.5136.51
66349-63498.2278.23
10min117692-1769222.92525.1713.2022.9725.2213.19
224000-2400031.09931.15
319309-1930925.02125.07
419780-1978025.63125.68
516462-1646221.33221.37
619309-1930925.02125.07
15min124714-2471432.02534.2911.0632.1934.4811.06
232207-3220741.73441.95
326287-2628734.06334.25
426229-2622933.98834.18
524294-2429431.48031.64
625054-2505432.46532.65
20min128870-2887037.41040.3011.2137.7640.6711.21
237645-3764548.78149.23
330853-3085339.98040.35
431666-3166641.03341.41
527835-2783536.06936.40
629728-2972838.52238.89
30min136109-3610946.79050.319.1347.3450.919.16
245619-4561959.11459.84
338544-3854449.94650.54
439102-3910250.66951.28
536145-3614546.83747.37
637450-3745048.52849.11
45min144546-4454657.72360.967.5158.5461.837.55
253652-5365269.52370.57
346837-4683760.69261.56
447787-4778761.92362.81
544007-4400757.02557.81
645428-4542858.86659.71
60min150979-5097966.05969.555.4167.1970.775.46
257914-5791475.04676.48
352442-5244267.95569.16
454440-5444070.54471.78
550478-5047865.41066.52
655787-5578772.28973.47
极限154998-5499871.26774.835.0672.7776.445.12
262651-6265181.18483.04
358966-5896676.40978.00
458528-5852875.84177.47
556143-5614372.75174.22
655217-5521771.55173.13
非奈利酮片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号D231201对照品来源自制对照品使用方法直接使用
对照品含量(%)99.92对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.023795163793163792353792983791043792940.04
210.883776283774223775250.04
单位质量响应值RSD%判断
34418.6934698.990.58数据可信
供试品溶液-BXK2XG1批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min15846-58467.6067.3613.647.617.3613.63
26447-64478.3888.39
35208-52086.7766.78
45438-54387.0757.08
56501-65018.4588.46
64494-44945.8475.85
10min117637-1763722.94823.599.7822.9923.639.77
218652-1865224.26824.31
316501-1650121.47021.51
421427-2142727.87927.92
517618-1761822.92322.97
616944-1694422.04622.08
15min124477-2447731.84732.879.1132.0233.049.10
225644-2564433.36633.55
322763-2276329.61729.77
429488-2948838.36738.56
525203-2520332.79232.97
624010-2401031.24031.39
20min129655-2965538.58439.117.1738.9339.467.19
230202-3020239.29639.66
327571-2757135.87336.19
434058-3405844.31344.72
529632-2963238.55438.91
629236-2923638.03938.37
30min136377-3637747.33048.706.4447.8949.286.46
236909-3690948.02348.61
335962-3596246.79047.31
442289-4228955.02355.68
536877-3687747.98148.55
636183-3618347.07847.62
45min145480-4548059.17460.564.9460.0061.414.97
246643-4664360.68861.54
344506-4450657.90758.69
450975-5097566.32467.28
546342-4634260.29661.13
645342-4534258.99559.80
60min152115-5211567.80768.584.0068.9669.764.05
252565-5256568.39369.58
351055-5105566.42867.53
456759-5675973.85075.18
552685-5268568.54969.72
651083-5108366.46467.59
极限157391-5739174.67274.982.4976.2076.542.55
257894-5789475.32676.90
356454-5645473.45374.92
460237-6023778.37580.11
556235-5623573.16874.72
657547-5754774.87576.37
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