熊去氧胆酸口服混悬液项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号C092A240304对照品来源原料对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数50
标示量(mg)250供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.145554855564554275536055433554660.16
214.135595555792558740.21
单位质量响应值RSD%判断
3922.633954.280.57数据可信
供试品溶液-25071801批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min133761-3376161.72063.121.5161.7263.121.51
234341-3434162.78162.78
334558-3455863.17763.18
435318-3531864.56764.57
534817-3481763.65163.65
634373-3437362.83962.84
10min138361-3836170.13069.331.5270.8270.041.50
237812-3781269.12669.82
337594-3759468.72869.43
438523-3852370.42671.14
538262-3826269.94970.66
636998-3699867.63868.34
15min139486-3948672.18771.640.9373.6573.120.92
239215-3921571.69173.16
338722-3872270.79072.26
439467-3946772.15273.65
539483-3948372.18173.67
638759-3875970.85872.31
20min139848-3984872.84872.031.6675.1274.301.63
238504-3850470.39172.65
338937-3893771.18373.44
440039-4003973.19875.50
540021-4002173.16575.45
639059-3905971.40673.64
30min140206-4020673.50373.471.0576.5876.541.05
240292-4029273.66076.70
339785-3978572.73375.78
440651-4065174.31677.43
540583-4058374.19277.29
639602-3960272.39975.43
45min141259-4125975.42874.381.1779.3278.261.15
240851-4085174.68278.54
340204-4020473.49977.35
440656-4065674.32678.27
541070-4107075.08279.01
640060-4006073.23677.07
极限141221-4122175.35875.930.6780.0980.640.65
241805-4180576.42681.12
341596-4159676.04480.71
441801-4180176.41981.19
541594-4159476.04080.80
641178-4117875.28079.93
熊去氧胆酸口服混悬液项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号C092A240304对照品来源原料对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数50
标示量(mg)250供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.145579055638556955578255781557370.13
214.135550555430554680.10
单位质量响应值RSD%判断
3941.803925.550.30数据可信
供试品溶液-25071802批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min133516-3351661.34662.061.1861.3562.061.18
233446-3344661.21861.22
333714-3371461.70961.71
434089-3408962.39562.40
534320-3432062.81862.82
634337-3433762.84962.85
10min137191-3719168.07368.720.7968.7569.410.79
237237-3723768.15768.84
337681-3768168.97069.66
437862-3786269.30169.99
537471-3747168.58569.28
637839-3783969.25969.96
15min139555-3955572.40071.900.5173.8473.360.49
239346-3934672.01773.45
339059-3905971.49272.94
439123-3912371.60973.07
539455-3945572.21773.68
639168-3916871.69173.16
20min140325-4032573.80973.471.0876.0575.721.04
240447-4044774.03376.27
339680-3968072.62974.87
440380-4038073.91076.17
539510-3951072.31774.58
640500-4050074.13076.39
30min141152-4115275.32375.560.8378.3978.630.79
241931-4193176.74979.81
341268-4126875.53578.59
441231-4123175.46878.55
541165-4116575.34778.41
640932-4093274.92078.01
45min142583-4258377.94277.210.7181.8481.120.67
242385-4238577.58081.49
341842-4184276.58680.48
442036-4203676.94180.86
542336-4233677.49081.39
641911-4191176.71280.63
极限142349-4234977.51477.970.5882.2882.730.55
243044-4304478.78683.56
342513-4251377.81482.56
442436-4243677.67382.45
542565-4256577.90982.67
642670-4267078.10182.87
熊去氧胆酸口服混悬液项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号C092A240304对照品来源原料对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数50
标示量(mg)250供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.145536655491554075544555162553740.23
214.135547855453554660.04
单位质量响应值RSD%判断
3916.123925.410.17数据可信
供试品溶液-25071803批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min126850-2685049.30748.141.7349.3148.141.73
226237-2623748.18148.18
326074-2607447.88247.88
426362-2636248.41148.41
526314-2631448.32248.32
625461-2546146.75646.76
10min132226-3222659.17957.822.2859.7358.352.27
231134-3113457.17457.71
332026-3202658.81259.34
431568-3156857.97158.51
531710-3171058.23258.77
630243-3024355.53856.06
15min135184-3518464.61163.252.7065.8264.422.68
234631-3463163.59664.77
334873-3487364.04065.23
434384-3438463.14264.32
534941-3494164.16565.35
632633-3263359.92761.06
20min136751-3675167.48966.121.9469.4168.001.95
235969-3596966.05367.93
336352-3635266.75668.65
435984-3598466.08067.96
536285-3628566.63368.53
634708-3470863.73765.54
30min138730-3873071.12368.972.4173.8071.582.39
237240-3724068.38771.00
338024-3802469.82672.47
436845-3684567.66170.28
538165-3816570.08572.72
636335-3633566.72569.24
45min139551-3955172.63170.832.6976.0974.212.64
238342-3834270.41073.78
339492-3949272.52275.94
437173-3717368.26471.63
539309-3930972.18675.60
637567-3756768.98772.24
极限139950-3995073.36373.300.5577.6377.460.61
239827-3982773.13777.29
340220-4022073.85978.08
439750-3975072.99677.12
540090-4009073.62077.84
639643-3964372.80076.82
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