玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.209886499436991999937699088991930.24
211.169970899829997680.09
单位质量响应值RSD%判断
8856.528939.780.67数据可信
供试品溶液-2025062821批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min174359-7435975.03977.752.5075.0477.752.50
279732-7973280.46180.46
376578-7657877.27877.28
478172-7817278.88778.89
577807-7780778.51878.52
675623-7562376.31476.31
10min188289-8828989.09688.211.9889.5188.651.97
287956-8795688.76089.21
385535-8553586.31786.75
489804-8980490.62591.06
587629-8762988.43088.87
685281-8528186.06186.48
15min192034-9203492.87591.631.8193.7992.551.81
292885-9288593.73494.67
388523-8852389.33290.24
490614-9061491.44292.38
591381-9138192.21693.14
689361-8936190.17891.08
20min189854-8985490.67592.711.5292.1094.141.51
292293-9229393.13794.60
392043-9204392.88494.29
494049-9404994.90996.36
591942-9194292.78394.22
691062-9106291.89493.30
30min191970-9197092.81192.501.0194.7494.441.00
293082-9308293.93395.91
390481-9048191.30893.23
491458-9145892.29494.27
590906-9090691.73793.69
692050-9205092.89294.81
45min190011-9001190.83493.101.4693.2895.561.43
294141-9414195.00297.50
392780-9278093.62896.06
492358-9235893.20295.69
591946-9194692.78795.25
692318-9231893.16295.59
60min192551-9255193.39792.831.8296.3595.811.79
292980-9298093.83096.86
389685-8968590.50593.45
494406-9440695.26998.28
590999-9099991.83194.81
691320-9132092.15595.10
极限189099-8909989.91492.451.8993.3895.951.85
291781-9178192.62096.17
390652-9065291.48194.93
492788-9278893.63697.17
594106-9410694.96698.46
691276-9127692.11095.57
玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.209868198922995559945798446990120.49
211.161002741003141002940.03
单位质量响应值RSD%判断
8840.368986.921.17数据可信
供试品溶液-2025062821批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min175417-7541775.97876.861.7475.9876.861.74
274328-7432874.88174.88
376999-7699977.57177.57
478077-7807778.65778.66
576918-7691877.49077.49
676027-7602776.59276.59
10min185618-8561886.25586.140.5786.6886.560.57
285437-8543786.07286.49
386127-8612786.76787.20
485897-8589786.53686.97
584873-8487385.50485.93
685059-8505985.69186.12
15min191102-9110291.77990.812.7492.6891.722.72
288298-8829888.95489.85
393529-9352994.22495.14
489724-8972490.39191.31
586607-8660787.25188.16
691564-9156492.24593.15
20min190518-9051891.19191.912.0692.6093.322.02
291705-9170592.38793.78
391408-9140892.08893.52
491496-9149692.17693.60
594019-9401994.71896.11
688244-8824488.90090.31
30min190419-9041991.09192.031.1693.0193.951.15
292432-9243293.11995.02
392298-9229892.98494.93
492169-9216992.85494.79
590689-9068991.36393.28
690103-9010390.77392.68
45min187609-8760988.26091.481.7990.6893.911.75
291375-9137592.05494.47
390741-9074191.41693.88
491595-9159592.27694.72
591483-9148392.16394.59
692029-9202992.71395.13
60min191941-9194192.62590.491.4595.5493.431.40
289439-8943990.10493.03
388896-8889689.55792.53
490577-9057791.25094.21
589808-8980890.47693.41
688282-8828288.93891.87
极限189654-8965490.32189.351.7193.7592.801.65
287623-8762388.27491.71
388095-8809588.75092.22
491052-9105291.72995.20
588873-8887389.53492.97
686861-8686187.50790.93
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