玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.289903098757991129934299156990790.22
211.189876298687987240.06
单位质量响应值RSD%判断
8783.608830.410.38数据可信
供试品溶液-2025062821批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min140696-4069641.49250.2213.0141.4950.2213.01
247084-4708448.00548.01
354282-5428255.34455.34
454769-5476955.84155.84
555323-5532356.40656.41
643372-4337244.22144.22
10min157179-5717958.29867.339.9658.5367.619.97
263801-6380165.05065.32
371962-7196273.37073.68
471161-7116172.55472.86
572034-7203473.44473.76
660087-6008761.26361.51
15min169535-6953570.89679.126.6771.4579.786.71
277274-7727478.78679.41
381939-8193983.54384.26
480641-8064182.21982.93
582598-8259884.21484.94
673639-7363975.08075.67
20min176892-7689278.39787.286.0279.3588.376.05
285132-8513286.79887.86
388876-8887690.61591.79
486795-8679588.49489.66
592036-9203693.83795.03
683880-8388085.52286.52
30min186255-8625587.94392.462.9389.3394.043.00
289722-8972291.47893.03
392863-9286394.68096.36
490446-9044692.21693.88
593798-9379895.63497.34
691017-9101792.79894.28
45min193796-9379695.63295.981.0797.5098.081.14
292863-9286394.68096.74
395305-9530597.17099.38
493673-9367395.50697.68
595387-9538797.25499.50
693824-9382495.66097.65
60min192863-9286394.68095.860.9997.0898.481.09
293070-9307094.89197.47
395300-9530097.16599.91
494530-9453096.38099.08
594425-9442596.27399.06
693937-9393795.77598.30
极限192354-9235494.16195.431.8697.0998.581.91
293306-9330695.13298.24
395170-9517097.033100.32
491873-9187393.67196.91
596258-9625898.142101.46
692603-9260394.41597.47
玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.289920898899992209924999211991570.15
211.189927698851990640.31
单位质量响应值RSD%判断
8790.518860.820.57数据可信
供试品溶液-2025062821批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min146464-4646447.27452.7512.6947.2752.7512.69
249283-4928350.14250.14
344196-4419644.96644.97
458558-5855859.57859.58
551921-5192152.82652.83
660634-6063461.69061.69
10min165425-6542566.56571.527.9766.8371.817.99
268302-6830269.49269.77
364290-6429065.41065.66
476482-7648277.81578.15
569600-6960070.81371.11
677651-7765179.00479.35
15min179173-7917380.55281.275.6981.1881.965.72
277676-7767679.02979.69
373789-7378975.07575.69
484688-8468886.16486.93
578164-7816479.52680.21
685768-8576887.26288.04
20min185069-8506986.55188.233.0287.6389.373.09
286116-8611687.61688.72
383418-8341884.87185.90
490473-9047392.04993.29
586106-8610687.60688.73
689131-8913190.68491.95
30min184975-8497586.45692.773.6688.0294.403.62
290389-9038991.96493.55
393682-9368295.31496.82
491920-9192093.52295.27
594206-9420695.84797.46
691902-9190293.50395.27
45min192279-9227993.88794.540.9495.9396.690.87
292683-9268394.29896.40
393902-9390295.53897.57
492262-9226293.87096.14
594137-9413795.77797.93
692291-9229193.89996.19
60min192278-9227893.88695.101.9096.4597.771.92
290754-9075492.33594.96
393338-9333894.96497.53
495525-9552597.18999.98
595067-9506796.72399.40
693844-9384495.47998.29
极限191386-9138692.97895.461.6196.0698.661.60
293220-9322094.84497.98
395039-9503996.69599.78
494766-9476696.41799.75
595351-9535197.012100.23
693203-9320394.82798.17
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