玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.291003781006161004801004601004151004700.10
211.381005381006521005950.09
单位质量响应值RSD%判断
8899.038839.630.48数据可信
供试品溶液-2025062821批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min157756-5775658.47355.279.0358.4755.279.04
254119-5411954.79154.79
356922-5692257.62857.63
459642-5964260.38260.38
553422-5342254.08554.08
645705-4570546.27246.27
10min174648-7464875.57472.056.6175.9072.366.62
271885-7188572.77773.08
373434-7343474.34574.67
474864-7486475.79376.13
569773-6977370.63970.94
662388-6238863.16263.42
15min183421-8342184.45681.723.4385.2082.433.46
280158-8015881.15381.86
381253-8125382.26182.99
483792-8379284.83285.59
579299-7929980.28380.98
676384-7638477.33277.94
20min187095-8709588.17686.712.7389.3987.862.77
286547-8654787.62188.78
385292-8529286.35187.54
488010-8801089.10290.33
585573-8557386.63587.77
681337-8133782.34683.38
30min186587-8658787.66291.242.3189.3792.892.26
292741-9274193.89295.54
390198-9019891.31792.99
490697-9069791.82393.55
591223-9122392.35593.98
689308-8930890.41691.91
45min189719-8971990.83292.422.3593.0294.572.33
293249-9324994.40696.57
391060-9106092.19094.37
490572-9057291.69693.93
594384-9438495.55597.69
688734-8873489.83591.83
60min191161-9116192.29293.221.2494.9995.881.22
293802-9380294.96697.66
391003-9100392.13294.82
491912-9191293.05395.80
593104-9310494.25996.92
691468-9146892.60395.10
极限192657-9265793.80792.961.4797.0296.141.46
292970-9297094.12497.34
389598-8959890.71093.91
492076-9207693.21996.48
592804-9280493.95697.14
690807-9080791.93494.94
玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.291004191013461012331014241014261011700.43
211.381024021021341022680.19
单位质量响应值RSD%判断
8961.038986.640.21数据可信
供试品溶液-2025062821批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min132609-3260932.62944.4118.9332.6344.4118.93
240620-4062040.64540.64
338353-3835338.37638.38
449828-4982849.85849.86
553818-5381853.85153.85
651091-5109151.12251.12
10min150304-5030450.33560.1613.5550.5260.4013.57
256710-5671056.74556.97
352462-5246252.49452.71
463888-6388863.92764.20
570157-7015770.20070.50
667205-6720567.24667.53
15min163924-6392463.96372.969.2564.4273.549.30
270359-7035970.40270.94
367480-6748067.52168.03
475534-7553475.58076.21
579673-7967379.72280.41
680505-8050580.55481.21
20min176487-7648776.53480.804.9177.3581.795.00
278718-7871878.76679.70
376440-7644076.48777.37
484185-8418584.23685.29
584313-8431384.36585.50
684360-8436084.41285.52
30min186368-8636886.42188.842.1687.6690.272.28
289323-8932389.37890.75
386376-8637686.42987.73
490404-9040490.45991.98
590384-9038490.43992.04
689851-8985189.90691.48
45min187305-8730587.35890.281.8789.0892.201.89
292270-9227092.32694.19
390487-9048790.54292.33
491298-9129891.35493.38
589801-8980189.85691.96
690160-9016090.21592.29
60min190859-9085990.91590.340.8993.1292.760.80
290778-9077890.83393.21
390005-9000590.06092.35
491055-9105591.11193.64
588908-8890888.96291.56
690074-9007490.12992.70
极限193457-9345793.51490.632.2996.2393.562.22
289628-8962889.68392.57
387499-8749987.55290.34
491720-9172091.77694.81
591411-9141191.46794.56
689710-8971089.76592.84
玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.291018641023501022791024941028481023670.35
211.381014601014251014420.03
单位质量响应值RSD%判断
9067.058914.061.21数据可信
供试品溶液-2025062821批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min134356-3435634.31541.0520.8634.3241.0620.86
234837-3483734.79634.80
333838-3383833.79833.80
440373-4037340.32540.33
549477-4947749.41949.42
653719-5371953.65653.66
10min166832-6683266.75363.5216.8466.9463.7516.83
250146-5014650.08750.28
359942-5994259.87160.06
458090-5809058.02158.25
564605-6460564.52964.80
681952-8195281.85582.15
15min165964-6596465.88673.0310.6466.4573.6110.60
271263-7126371.17971.65
363521-6352163.44663.97
484397-8439784.29784.84
575881-7588175.79176.42
677644-7764477.55278.31
20min185270-8527085.16982.025.0886.1083.005.10
274464-7446474.37675.24
381286-8128681.19082.06
486058-8605885.95686.97
581991-8199181.89482.95
683613-8361383.51484.70
30min186142-8614286.04087.651.2787.4489.091.32
287103-8710387.00088.28
387615-8761587.51288.84
489195-8919589.09090.58
588792-8879288.68790.20
687655-8765587.55289.20
45min186665-8666586.56390.252.2888.4492.182.22
291090-9109090.98392.75
392172-9217292.06393.87
490116-9011690.01092.00
592185-9218592.07694.08
689896-8989689.79091.92
60min190780-9078090.67390.931.8293.0393.361.72
289903-8990389.79792.07
393862-9386293.75196.07
491536-9153691.42893.92
591113-9111391.00693.52
689005-8900588.90091.53
极限190269-9026990.16390.751.8793.0393.691.70
292228-9222892.11994.89
392898-9289892.78895.63
490670-9067090.56393.56
591045-9104590.93893.96
688056-8805687.95291.08
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