依折麦布阿托伐他汀钙片项目信息
介质体积(ml)
900
取样体积(ml)
5
补液体积(ml)
5
对照品批号
DJ333-221017
对照品来源
自制
对照品使用方法
直接使用
对照品含量(%)
99.67
对照品水分(%)
0
对照品稀释倍数
5000
标示量(mg)
10
供试品稀释倍数
5
系数
1
对照品溶液
序号
称样量(mg)
A
1
A
2
A
3
A
4
A
5
A
平均
RSD%
1
10.02
173654
173700
174383
173583
173723
173809
0.19
2
10.03
174892
175161
175026
0.11
单位质量响应值
RSD%
判断
17346.21
17450.25
0.43
数据可信
供试品溶液-2024012021批-依折麦布-pH2.0(内含0.2%Tween80)
时间
(分钟)
样品
A
1
A
2
A
平均
溶出量(%)
平均(%)
RSD%
累计溶
出量(%)
平均(%)
RSD%
5min
1
40350
-
40350
20.804
14.88
32.21
20.80
14.88
32.21
2
28427
-
28427
14.657
14.66
3
30140
-
30140
15.540
15.54
4
15057
-
15057
7.763
7.76
5
36865
-
36865
19.007
19.01
6
22279
-
22279
11.487
11.49
10min
1
84977
-
84977
43.813
49.94
9.17
43.93
50.02
9.14
2
106135
-
106135
54.722
54.80
3
105679
-
105679
54.487
54.57
4
100722
-
100722
51.931
51.97
5
95219
-
95219
49.094
49.20
6
88405
-
88405
45.581
45.64
15min
1
115826
-
115826
59.719
71.30
8.76
60.08
71.66
8.71
2
150965
-
150965
77.836
78.22
3
135263
-
135263
69.740
70.13
4
142181
-
142181
73.307
73.64
5
143942
-
143942
74.215
74.59
6
141563
-
141563
72.989
73.31
20min
1
134180
-
134180
69.182
82.75
8.47
69.87
83.51
8.43
2
167390
-
167390
86.305
87.12
3
157562
-
157562
81.238
82.01
4
166814
-
166814
86.008
86.75
5
170184
-
170184
87.745
88.54
6
166878
-
166878
86.041
86.76
30min
1
160600
-
160600
82.804
88.51
4.36
83.88
89.72
4.38
2
176306
-
176306
90.902
92.20
3
170328
-
170328
87.820
89.05
4
175085
-
175085
90.272
91.49
5
181334
-
181334
93.494
94.77
6
166331
-
166331
85.759
86.96
45min
1
171296
-
171296
88.319
92.02
3.35
89.85
93.73
3.33
2
174492
-
174492
89.967
91.77
3
176888
-
176888
91.202
92.92
4
177044
-
177044
91.282
93.00
5
183838
-
183838
94.785
96.58
6
187306
-
187306
96.573
98.25
60min
1
179517
-
179517
92.557
94.78
1.35
94.58
97.00
1.42
2
186241
-
186241
96.024
98.33
3
184352
-
184352
95.050
97.27
4
182479
-
182479
94.085
96.31
5
185571
-
185571
95.679
98.00
6
184808
-
184808
95.285
97.50
极限
1
182824
-
182824
94.263
95.35
1.03
96.80
98.10
1.07
2
184137
-
184137
94.939
97.78
3
183693
-
183693
94.711
97.46
4
184447
-
184447
95.099
97.85
5
187387
-
187387
96.615
99.47
6
187161
-
187161
96.499
99.24
依折麦布阿托伐他汀钙片项目信息
介质体积(ml)
900
取样体积(ml)
5
补液体积(ml)
5
对照品批号
100590-202005
对照品来源
中检院
对照品使用方法
直接使用
对照品含量(%)
94.9
对照品水分(%)
0
对照品稀释倍数
2500
标示量(mg)
20
供试品稀释倍数
5
系数
0.9671
对照品溶液
序号
称样量(mg)
A
1
A
2
A
3
A
4
A
5
A
平均
RSD%
1
11.17
309279
309713
311230
309225
309177
309725
0.29
2
11.11
310337
312484
311410
0.49
单位质量响应值
RSD%
判断
27728.29
28029.70
0.77
数据可信
供试品溶液-2024012021批-阿托伐他汀钙-pH2.0(内含0.2%Tween80)
时间
(分钟)
样品
A
1
A
2
A
平均
溶出量(%)
平均(%)
RSD%
累计溶
出量(%)
平均(%)
RSD%
5min
1
80248
-
80248
23.777
34.45
56.37
23.78
34.45
56.37
2
192034
-
192034
56.898
56.90
3
205097
-
205097
60.768
60.77
4
81622
-
81622
24.184
24.18
5
91025
-
91025
26.970
26.97
6
47628
-
47628
14.112
14.11
10min
1
168122
-
168122
49.813
65.21
28.39
49.94
65.40
28.46
2
284905
-
284905
84.414
84.73
3
283721
-
283721
84.063
84.40
4
246612
-
246612
73.068
73.20
5
204372
-
204372
60.553
60.70
6
132798
-
132798
39.347
39.42
15min
1
224473
-
224473
66.509
77.05
20.25
66.92
77.60
20.36
2
318067
-
318067
94.240
95.02
3
311762
-
311762
92.372
93.18
4
272138
-
272138
80.632
81.17
5
253591
-
253591
75.136
75.62
6
180271
-
180271
53.412
53.71
20min
1
256571
-
256571
76.019
84.22
14.81
76.80
85.20
14.96
2
322365
-
322365
95.513
96.82
3
324075
-
324075
96.020
97.34
4
305280
-
305280
90.451
91.44
5
280764
-
280764
83.187
84.09
6
216477
-
216477
64.140
64.73
30min
1
289672
-
289672
85.827
89.20
10.34
87.03
90.65
10.53
2
321343
-
321343
95.210
97.05
3
326553
-
326553
96.754
98.61
4
318345
-
318345
94.322
95.81
5
306908
-
306908
90.933
92.30
6
243439
-
243439
72.128
73.08
45min
1
303877
-
303877
90.035
92.59
2.56
91.71
94.54
2.83
2
312680
-
312680
92.644
95.01
3
318783
-
318783
94.452
96.84
4
317867
-
317867
94.181
96.20
5
320187
-
320187
94.868
96.74
6
301667
-
301667
89.381
90.73
60min
1
312030
-
312030
92.451
94.73
2.34
94.63
97.19
2.68
2
327809
-
327809
97.126
100.01
3
325773
-
325773
96.523
99.44
4
320066
-
320066
94.832
97.37
5
323235
-
323235
95.771
98.17
6
309460
-
309460
91.690
93.54
极限
1
314393
-
314393
93.151
95.82
1.82
95.84
98.80
1.68
2
321403
-
321403
95.228
98.65
3
322454
-
322454
95.540
98.99
4
322688
-
322688
95.609
98.67
5
328029
-
328029
97.191
100.12
6
331417
-
331417
98.195
100.55
依折麦布阿托伐他汀钙片项目信息
介质体积(ml)
900
取样体积(ml)
5
补液体积(ml)
5
对照品批号
DJ333-221017
对照品来源
自制
对照品使用方法
直接使用
对照品含量(%)
99.67
对照品水分(%)
0
对照品稀释倍数
5000
标示量(mg)
10
供试品稀释倍数
5
系数
1
对照品溶液
序号
称样量(mg)
A
1
A
2
A
3
A
4
A
5
A
平均
RSD%
1
10.02
175491
176011
176533
176701
176684
176284
0.30
2
10.03
174832
175582
175207
0.31
单位质量响应值
RSD%
判断
17593.21
17468.30
0.51
数据可信
供试品溶液-2024012021批-依折麦布-pH2.0(内含0.2%Tween80)
时间
(分钟)
样品
A
1
A
2
A
平均
溶出量(%)
平均(%)
RSD%
累计溶
出量(%)
平均(%)
RSD%
5min
1
36127
-
36127
18.486
22.62
26.67
18.49
22.62
26.68
2
39034
-
39034
19.974
19.97
3
42523
-
42523
21.759
21.76
4
39636
-
39636
20.282
20.28
5
67902
-
67902
34.745
34.75
6
39998
-
39998
20.467
20.47
10min
1
130463
-
130463
66.757
70.34
5.60
66.86
70.47
5.64
2
134333
-
134333
68.738
68.85
3
140938
-
140938
72.117
72.24
4
132782
-
132782
67.944
68.06
5
151462
-
151462
77.502
77.70
6
134804
-
134804
68.979
69.09
15min
1
164825
-
164825
84.340
85.91
2.05
84.81
86.43
2.10
2
168647
-
168647
86.296
86.79
3
169476
-
169476
86.720
87.24
4
164960
-
164960
84.409
84.90
5
173684
-
173684
88.873
89.50
6
165809
-
165809
84.844
85.34
20min
1
171729
-
171729
87.873
89.84
2.12
88.82
90.83
2.16
2
174746
-
174746
89.417
90.39
3
177636
-
177636
90.896
91.90
4
172396
-
172396
88.214
89.17
5
181810
-
181810
93.031
94.15
6
175091
-
175091
89.593
90.56
30min
1
175623
-
175623
89.866
90.70
0.60
91.30
92.19
0.59
2
177022
-
177022
90.581
92.05
3
177296
-
177296
90.722
92.23
4
178885
-
178885
91.535
92.98
5
177107
-
177107
90.625
92.26
6
177581
-
177581
90.867
92.33
45min
1
164592
-
164592
84.221
90.09
4.43
86.15
92.09
4.38
2
178951
-
178951
91.568
93.54
3
178474
-
178474
91.324
93.34
4
168407
-
168407
86.173
88.13
5
181638
-
181638
92.943
95.08
6
184331
-
184331
94.321
96.29
60min
1
175147
-
175147
89.622
91.64
1.41
92.02
94.14
1.46
2
179756
-
179756
91.980
94.46
3
180135
-
180135
92.174
94.69
4
177573
-
177573
90.863
93.30
5
182589
-
182589
93.430
96.08
6
179328
-
179328
91.761
94.26
极限
1
179844
-
179844
92.025
92.54
0.58
94.92
95.55
0.64
2
180539
-
180539
92.381
95.37
3
182346
-
182346
93.306
96.34
4
180193
-
180193
92.204
95.15
5
181936
-
181936
93.096
96.27
6
180242
-
180242
92.229
95.23
依折麦布阿托伐他汀钙片项目信息
介质体积(ml)
900
取样体积(ml)
5
补液体积(ml)
5
对照品批号
100590-202005
对照品来源
中检院
对照品使用方法
直接使用
对照品含量(%)
94.9
对照品水分(%)
0
对照品稀释倍数
2500
标示量(mg)
20
供试品稀释倍数
5
系数
0.9671
对照品溶液
序号
称样量(mg)
A
1
A
2
A
3
A
4
A
5
A
平均
RSD%
1
11.17
312422
313587
314397
314196
313875
313695
0.25
2
11.11
310344
313110
311727
0.63
单位质量响应值
RSD%
判断
28083.71
28058.24
0.07
数据可信
供试品溶液-2024012021批-阿托伐他汀钙-pH2.0(内含0.2%Tween80)
时间
(分钟)
样品
A
1
A
2
A
平均
溶出量(%)
平均(%)
RSD%
累计溶
出量(%)
平均(%)
RSD%
5min
1
73210
-
73210
21.542
28.33
15.50
21.54
28.33
15.50
2
87308
-
87308
25.691
25.69
3
106053
-
106053
31.207
31.21
4
99421
-
99421
29.255
29.26
5
116118
-
116118
34.168
34.17
6
95491
-
95491
28.099
28.10
10min
1
235959
-
235959
69.432
71.26
2.63
69.55
71.42
2.65
2
232729
-
232729
68.481
68.62
3
245225
-
245225
72.159
72.33
4
244373
-
244373
71.908
72.07
5
245659
-
245659
72.286
72.48
6
249072
-
249072
73.290
73.45
15min
1
277439
-
277439
81.638
81.98
1.50
82.14
82.53
1.48
2
278612
-
278612
81.983
82.51
3
278249
-
278249
81.876
82.45
4
276932
-
276932
81.488
82.05
5
273942
-
273942
80.609
81.20
6
286370
-
286370
84.266
84.83
20min
1
286317
-
286317
84.250
85.47
1.76
85.21
86.48
1.76
2
289793
-
289793
85.273
86.25
3
291244
-
291244
85.700
86.73
4
287179
-
287179
84.504
85.52
5
287941
-
287941
84.728
85.77
6
300202
-
300202
88.336
89.37
30min
1
288361
-
288361
84.851
85.80
2.51
86.28
87.29
2.47
2
292207
-
292207
85.983
87.44
3
292639
-
292639
86.110
87.62
4
293951
-
293951
86.496
87.98
5
280065
-
280065
82.410
83.92
6
302357
-
302357
88.970
90.49
45min
1
271462
-
271462
79.879
85.85
4.43
81.78
87.80
4.35
2
298463
-
298463
87.824
89.75
3
294269
-
294269
86.590
88.57
4
283429
-
283429
83.400
85.36
5
308954
-
308954
90.911
92.88
6
293873
-
293873
86.473
88.49
60min
1
287319
-
287319
84.545
86.81
2.01
86.89
89.25
2.00
2
298885
-
298885
87.948
90.37
3
296867
-
296867
87.354
89.82
4
292634
-
292634
86.109
88.54
5
290734
-
290734
85.550
88.02
6
303619
-
303619
89.341
91.84
极限
1
307522
-
307522
90.490
92.32
1.48
93.30
95.24
1.48
2
312966
-
312966
92.092
95.00
3
316064
-
316064
93.003
95.95
4
317172
-
317172
93.329
96.24
5
309381
-
309381
91.037
93.98
6
319382
-
319382
93.980
96.97
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图1 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转<br>溶剂 图2 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转<br>对照品溶液-1-1 图3 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转<br>对照品溶液-1-2 图4 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转<br>对照品溶液-1-3 图5 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转<br>对照品溶液-1-4 图6 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转<br>对照品溶液-1-5 图7 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-5min-片1<br>供试品溶液-1 图8 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-5min-片2<br>供试品溶液-1 图9 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-5min-片3<br>供试品溶液-1 图10 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-5min-片4<br>供试品溶液-1 图11 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-5min-片5<br>供试品溶液-1 图12 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-5min-片6<br>供试品溶液-1 图13 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-10min-片1<br>供试品溶液-1 图14 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-10min-片2<br>供试品溶液-1 图15 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-10min-片3<br>供试品溶液-1 图16 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-10min-片4<br>供试品溶液-1 图17 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-10min-片5<br>供试品溶液-1 图18 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-10min-片6<br>供试品溶液-1 图19 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-15min-片1<br>供试品溶液-1 图20 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-15min-片2<br>供试品溶液-1 图21 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-15min-片3<br>供试品溶液-1 图22 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-15min-片4<br>供试品溶液-1 图23 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-15min-片5<br>供试品溶液-1 图24 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-15min-片6<br>供试品溶液-1 图25 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-20min-片1<br>供试品溶液-1 图26 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-20min-片2<br>供试品溶液-1 图27 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-20min-片3<br>供试品溶液-1 图28 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-20min-片4<br>供试品溶液-1 图29 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-20min-片5<br>供试品溶液-1 图30 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-20min-片6<br>供试品溶液-1 图31 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-30min-片1<br>供试品溶液-1 图32 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-30min-片2<br>供试品溶液-1 图33 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-30min-片3<br>供试品溶液-1 图34 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-30min-片4<br>供试品溶液-1 图35 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-30min-片5<br>供试品溶液-1 图36 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-30min-片6<br>供试品溶液-1 图37 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-45min-片1<br>供试品溶液-1 图38 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-45min-片2<br>供试品溶液-1 图39 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-45min-片3<br>供试品溶液-1 图40 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-45min-片4<br>供试品溶液-1 图41 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-45min-片5<br>供试品溶液-1 图42 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-45min-片6<br>供试品溶液-1 图43 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-60min-片1<br>供试品溶液-1 图44 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-60min-片2<br>供试品溶液-1 图45 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-60min-片3<br>供试品溶液-1 图46 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-60min-片4<br>供试品溶液-1 图47 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-60min-片5<br>供试品溶液-1 图48 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-60min-片6<br>供试品溶液-1 图49 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-极限转速-片1<br>供试品溶液-1 图50 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-极限转速-片2<br>供试品溶液-1 图51 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-极限转速-片3<br>供试品溶液-1 图52 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-极限转速-片4<br>供试品溶液-1 图53 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-极限转速-片5<br>供试品溶液-1 图54 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转-极限转速-片6<br>供试品溶液-1 图55 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转<br>对照品溶液-2-1 图56 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-桨法-50转<br>对照品溶液-2-2 图57 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转<br>溶剂 图58 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转<br>对照品溶液-1-1 图59 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转<br>对照品溶液-1-2 图60 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转<br>对照品溶液-1-3 图61 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转<br>对照品溶液-1-4 图62 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转<br>对照品溶液-1-5 图63 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-5min-片1<br>供试品溶液-1 图64 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-5min-片2<br>供试品溶液-1 图65 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-5min-片3<br>供试品溶液-1 图66 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-5min-片4<br>供试品溶液-1 图67 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-5min-片5<br>供试品溶液-1 图68 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-5min-片6<br>供试品溶液-1 图69 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-10min-片1<br>供试品溶液-1 图70 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-10min-片2<br>供试品溶液-1 图71 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-10min-片3<br>供试品溶液-1 图72 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-10min-片4<br>供试品溶液-1 图73 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-10min-片5<br>供试品溶液-1 图74 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-10min-片6<br>供试品溶液-1 图75 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-15min-片1<br>供试品溶液-1 图76 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-15min-片2<br>供试品溶液-1 图77 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-15min-片3<br>供试品溶液-1 图78 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-15min-片4<br>供试品溶液-1 图79 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-15min-片5<br>供试品溶液-1 图80 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-15min-片6<br>供试品溶液-1 图81 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-20min-片1<br>供试品溶液-1 图82 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-20min-片2<br>供试品溶液-1 图83 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-20min-片3<br>供试品溶液-1 图84 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-20min-片4<br>供试品溶液-1 图85 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-20min-片5<br>供试品溶液-1 图86 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-20min-片6<br>供试品溶液-1 图87 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-30min-片1<br>供试品溶液-1 图88 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-30min-片2<br>供试品溶液-1 图89 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-30min-片3<br>供试品溶液-1 图90 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-30min-片4<br>供试品溶液-1 图91 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-30min-片5<br>供试品溶液-1 图92 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-30min-片6<br>供试品溶液-1 图93 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-45min-片1<br>供试品溶液-1 图94 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-45min-片2<br>供试品溶液-1 图95 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-45min-片3<br>供试品溶液-1 图96 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-45min-片4<br>供试品溶液-1 图97 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-45min-片5<br>供试品溶液-1 图98 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-45min-片6<br>供试品溶液-1 图99 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-60min-片1<br>供试品溶液-1 图100 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-60min-片2<br>供试品溶液-1 图101 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-60min-片3<br>供试品溶液-1 图102 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-60min-片4<br>供试品溶液-1 图103 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-60min-片5<br>供试品溶液-1 图104 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-60min-片6<br>供试品溶液-1 图105 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-极限转速-片1<br>供试品溶液-1 图106 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-极限转速-片2<br>供试品溶液-1 图107 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-极限转速-片3<br>供试品溶液-1 图108 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-极限转速-片4<br>供试品溶液-1 图109 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-极限转速-片5<br>供试品溶液-1 图110 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转-极限转速-片6<br>供试品溶液-1 图111 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转<br>对照品溶液-2-1 图112 依折麦布阿托伐他汀钙片溶出曲线测定HPLC图谱<br>自制品-2024012021批(10mg/20mg规格)-pH2.0(内含0.2%Tween80)介质-篮法-100转<br>对照品溶液-2-2
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