褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)0
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.066409064116638906400964038640290.14
210.026379664257640260.51
单位质量响应值RSD%判断
6364.716389.820.28数据可信
供试品溶液-2025041021批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min167345-6734594.94795.262.4894.9595.262.48
265365-6536592.15592.16
368424-6842496.46896.47
468848-6884897.06697.07
569523-6952398.01898.02
665877-6587792.87792.88
10min170100-7010098.83197.661.6599.8998.721.65
268926-6892697.17698.20
370590-7059099.522100.59
469893-6989398.53999.62
568613-6861396.73597.82
667499-6749995.16496.20
15min170136-7013698.88298.111.20101.03100.251.20
268907-6890797.14999.25
370176-7017698.938101.12
468974-6897497.24399.42
570659-7065999.619101.78
668683-6868396.83398.92
20min168689-6868996.84296.931.69100.09100.161.68
267758-6775895.52998.71
370413-7041399.272102.55
468444-6844496.49699.75
569797-6979798.404101.67
667412-6741295.04198.21
30min168801-6880197.00096.641.35101.33100.961.35
267973-6797395.832100.08
369621-6962198.156102.54
468328-6832896.333100.66
569399-6939997.843102.21
667165-6716594.69398.91
45min169661-6966198.21296.002.61103.62101.382.54
266954-6695494.39699.70
369887-6988798.531104.00
468942-6894297.198102.59
567858-6785895.670101.12
665261-6526192.00997.28
60min169931-6993198.59397.861.00105.09104.321.03
268947-6894797.205103.56
370385-7038599.233105.80
469341-6934197.761104.24
569434-6943497.892104.41
668441-6844196.492102.79
极限168413-6841396.45396.091.89104.04103.631.85
268183-6818396.128103.57
369910-6991098.563106.23
467531-6753195.209102.77
568822-6882297.029104.63
666083-6608393.168100.54
褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)0
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.066399864233639406404364308641040.25
210.026410364215641590.13
单位质量响应值RSD%判断
6372.176403.090.35数据可信
供试品溶液-2025041021批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min166664-6666493.83491.906.6993.8391.906.69
256599-5659979.66779.67
367677-6767795.26095.26
465903-6590392.76392.76
568566-6856696.51296.51
666328-6632893.36193.36
10min168698-6869896.69796.771.1197.7497.791.06
269673-6967398.07098.95
368658-6865896.64197.70
467389-6738994.85595.89
569000-6900097.12398.19
669063-6906397.21198.25
15min168028-6802895.75496.661.2197.8798.761.15
269963-6996398.478100.45
368209-6820996.00998.14
468010-6801095.72997.81
569438-6943897.73999.89
668382-6838296.25398.37
20min167744-6774495.35594.221.7198.5497.391.67
267191-6719194.57697.65
367083-6708394.42497.62
464656-6465691.00894.16
567382-6738294.84598.08
667561-6756195.09798.28
30min168237-6823796.04995.721.18100.2999.941.12
269211-6921197.419101.54
367352-6735294.80399.05
467014-6701494.32798.49
568470-6847096.376100.67
667741-6774195.35099.59
45min168599-6859996.55895.991.13101.87101.271.11
268671-6867196.659101.86
367791-6779195.421100.72
466877-6687794.13499.34
569017-6901797.146102.51
668228-6822896.036101.34
60min169060-6906097.20796.271.11103.59102.621.08
269006-6900697.131103.41
367790-6779095.419101.78
467159-6715994.531100.78
568692-6869296.689103.13
668673-6867396.662103.03
极限168385-6838596.25795.391.31103.72102.811.29
267294-6729494.721102.08
368180-6818095.968103.39
466196-6619693.176100.48
568570-6857096.517104.03
667993-6799395.705103.15
褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)0
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.066423763781639386435064040640690.36
210.026418063972640760.23
单位质量响应值RSD%判断
6368.696394.810.29数据可信
供试品溶液-2025041021批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min163822-6382289.91790.891.7789.9290.891.77
263775-6377589.85189.85
363691-6369189.73289.73
464323-6432390.62390.62
564820-6482091.32391.32
666664-6666493.92193.92
10min167609-6760995.25294.890.8796.2595.900.85
268294-6829496.21797.22
367444-6744495.02096.02
467079-6707994.50595.51
566579-6657993.80194.82
667124-6712494.56995.61
15min166209-6620993.28094.592.1995.3496.652.15
264627-6462791.05193.12
367536-6753695.14997.20
467768-6776895.47697.53
568656-6865696.72798.78
668020-6802095.83197.93
20min166862-6686294.20095.110.8097.2998.220.79
267564-6756495.18998.27
367890-6789095.64898.76
466830-6683094.15597.27
567893-6789395.65298.78
668014-6801495.82398.98
30min167670-6767095.33895.031.7499.4899.201.68
267971-6797195.76299.90
367314-6731494.83699.01
465197-6519791.85496.02
568493-6849396.498100.69
668043-6804395.864100.09
45min168098-6809895.94195.561.43101.14100.791.35
269454-6945497.851103.05
367534-6753495.146100.37
466678-6667893.94099.13
567147-6714794.60199.87
668067-6806795.897101.19
60min168319-6831996.25295.811.04102.52102.100.99
268613-6861396.667102.95
367321-6732194.846101.13
467286-6728694.797101.03
568929-6892997.112103.43
667578-6757895.208101.56
极限167901-6790195.66395.290.89103.00102.640.86
267296-6729694.811102.17
367924-6792495.696103.03
466581-6658193.804101.09
568226-6822696.121103.52
667890-6789095.648103.06
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