褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)0
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.066483465001647776489564773648560.15
210.026509965023650610.09
单位质量响应值RSD%判断
6446.926493.110.51数据可信
供试品溶液-2025041021批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min168907-6890795.75796.831.0895.7696.831.08
269545-6954596.64496.64
369115-6911596.04696.05
469512-6951296.59896.60
569968-6996897.23297.23
671014-7101498.68598.69
10min169575-6957596.68697.691.1797.7598.761.17
270190-7019097.54098.61
369745-6974596.92297.99
470169-7016997.51198.58
570212-7021297.57198.65
671882-7188299.891100.99
15min169533-6953396.62797.691.1298.7799.851.12
270259-7025997.63699.79
369878-6987897.10799.25
470059-7005997.35899.51
570258-7025897.63599.80
671799-7179999.776101.98
20min169562-6956296.66797.082.1899.88100.332.13
270567-7056798.064101.31
369607-6960796.73099.95
467273-6727393.48796.73
570278-7027897.662100.91
671860-7186099.861103.18
30min168648-6864895.39796.291.1699.68100.611.17
269252-6925296.237100.57
368633-6863395.37699.67
469027-6902795.924100.20
569372-6937296.403100.74
670807-7080798.398102.82
45min168748-6874895.53696.611.32100.88102.001.32
269642-6964296.779102.18
368954-6895495.823101.18
468927-6892795.785101.13
569631-6963196.763102.17
671219-7121998.970104.49
60min169524-6952496.61597.281.23103.02103.751.22
269916-6991697.159103.64
369185-6918596.144102.57
469983-6998397.252103.66
569754-6975496.934103.41
671643-7164399.559106.18
极限169347-6934796.36996.820.96103.85104.370.98
269890-6989097.123104.68
368986-6898695.867103.36
469378-6937896.412103.90
569550-6955096.651104.21
670892-7089298.516106.24
褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)0
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.066461664920647256479364667647440.19
210.026519464867650300.36
单位质量响应值RSD%判断
6435.796490.020.60数据可信
供试品溶液-2025041021批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min168951-6895195.92496.921.0895.9296.921.08
269851-6985197.17697.18
370565-7056598.17098.17
468815-6881595.73595.74
570456-7045698.01898.02
669359-6935996.49296.49
10min169577-6957796.79598.281.0297.8699.361.02
271313-7131399.210100.29
370703-7070398.36299.45
470275-7027597.76698.83
571554-7155499.546100.63
670459-7045998.02299.09
15min167001-6700193.21194.071.1295.3596.241.11
268344-6834495.08097.26
368001-6800194.60396.79
466674-6667492.75794.91
568460-6846095.24197.44
667212-6721293.50595.67
20min167382-6738293.74294.281.3496.9297.501.32
268073-6807394.70397.94
368202-6820294.88298.12
466611-6661192.66995.85
569170-6917096.22999.48
667184-6718493.46696.67
30min166870-6687093.02993.810.9197.2598.070.91
267884-6788494.44098.73
367887-6788794.44498.73
466467-6646792.46996.68
567657-6765794.12498.45
667827-6782794.36198.60
45min166776-6677692.89894.151.1798.1599.461.16
267722-6772294.21599.55
368449-6844995.226100.56
466796-6679692.92698.16
568640-6864095.492100.86
667685-6768594.16399.45
60min168540-6854095.35394.930.89101.64101.280.87
268247-6824794.945101.33
368849-6884995.782102.18
467098-6709893.34699.62
568449-6844995.226101.66
668251-6825194.950101.28
极限166595-6659592.64794.601.2099.99102.011.17
268715-6871595.596103.04
368346-6834695.083102.54
467574-6757494.009101.32
568731-6873195.618103.11
668034-6803494.649102.04
褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)0
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.066468564637648676483364720647480.16
210.026490064828648640.08
单位质量响应值RSD%判断
6436.186473.450.41数据可信
供试品溶液-2025041021批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min164593-6459389.97390.281.5489.9790.281.54
264650-6465090.05390.05
364769-6476990.21890.22
466696-6669692.90392.90
563743-6374388.78988.79
664420-6442089.73289.73
10min165653-6565391.45092.281.2092.4593.281.20
266122-6612292.10393.10
366328-6632892.39093.39
467749-6774994.36995.40
565576-6557691.34292.33
666048-6604892.00093.00
15min166199-6619992.21092.631.5494.2394.661.54
266316-6631692.37394.40
366275-6627592.31694.35
468530-6853095.45797.54
566001-6600191.93493.94
665667-6566791.46993.49
20min167041-6704193.38392.981.5196.4296.041.50
266215-6621592.23395.28
367029-6702993.36696.42
468490-6849095.40198.54
565747-6574791.58194.60
665997-6599791.92994.96
30min166282-6628292.32692.621.1796.4096.711.18
266227-6622792.24996.32
366502-6650292.63296.72
468012-6801294.73698.94
566091-6609192.06096.10
665833-6583391.70095.76
45min167108-6710893.47693.940.7798.5899.060.68
267932-6793294.62499.72
368002-6800294.72299.84
466712-6671292.92598.18
567693-6769394.29199.35
667211-6721193.62098.70
60min168327-6832795.17494.760.67101.32100.920.58
268171-6817194.957101.11
368215-6821595.018101.19
467112-6711293.48299.77
568246-6824695.062101.17
668110-6811094.872100.99
极限168323-6832395.16994.900.48102.37102.120.47
267670-6767094.259101.47
367864-6786494.529101.76
468563-6856395.503102.83
568101-6810194.860102.03
668267-6826795.091102.26
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