辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.242861962865872862442862742864222863450.06
210.222867982868772868380.02
单位质量响应值RSD%判断
27963.3828066.340.26数据可信
供试品溶液-2025071821批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1231684-23168482.53579.792.7682.5479.792.76
2222613-22261379.30479.30
3230992-23099282.28982.29
4222323-22232379.20179.20
5220131-22013178.42078.42
6216106-21610676.98676.99
10min1252597-25259789.98589.372.1290.2389.612.11
2253800-25380090.41490.65
3256261-25626191.29191.54
4250960-25096089.40289.64
5250781-25078189.33889.57
6240895-24089585.81786.05
15min1260297-26029792.72892.812.5993.2593.322.58
2265323-26532394.51995.03
3264477-26447794.21794.74
4263025-26302593.70094.21
5262760-26276093.60694.11
6247252-24725288.08188.57
20min1260542-26054292.81694.052.3493.6194.832.33
2269461-26946195.99396.79
3266773-26677395.03595.84
4266804-26680495.04695.83
5267401-26740195.25996.04
6253027-25302790.13990.89
30min1262759-26275993.60595.192.7994.6896.262.78
2274184-27418497.67698.76
3270122-27012296.22897.32
4270424-27042496.33697.41
5271529-27152996.73097.80
6254151-25415190.53991.56
45min1262609-26260993.55295.142.4594.9196.492.44
2272678-27267897.13998.51
3269652-26965296.06197.44
4270155-27015596.24097.60
5271435-27143596.69698.06
6255817-25581791.13292.43
60min1261619-26161993.19994.632.5994.8496.272.58
2271643-27164396.77098.44
3267673-26767395.35697.02
4268776-26877695.74997.40
5270589-27058996.39598.04
6253580-25358090.33691.90
极限1269158-26915895.88598.761.6397.80100.681.60
2277433-27743398.833100.79
3277698-27769898.927100.88
4282945-282945100.797102.73
5276954-27695498.662100.60
6279146-27914699.443101.28
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.242910432912142909392902582901922907290.17
210.222866572865752866160.03
单位质量响应值RSD%判断
28391.5028044.620.87数据可信
供试品溶液-2025071921批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1216978-21697876.74275.431.6576.7475.431.65
2213975-21397575.68075.68
3207559-20755973.41173.41
4210813-21081374.56274.56
5214319-21431975.80275.80
6215970-21597076.38676.39
10min1239690-23969084.77583.341.2085.0183.571.20
2238234-23823484.26084.49
3234619-23461982.98283.20
4233493-23349382.58482.81
5235453-23545383.27783.50
6232343-23234382.17782.41
15min1248355-24835587.84086.271.6988.3286.741.68
2245530-24553086.84187.32
3246827-24682787.30087.77
4241804-24180485.52385.99
5243983-24398386.29486.77
6236913-23691383.79384.27
20min1252471-25247189.29687.692.2090.0488.422.18
2248082-24808287.74488.48
3252320-25232089.24289.97
4249561-24956188.26788.99
5247412-24741287.50788.24
6237665-23766584.05984.79
30min1255352-25535290.31588.642.4991.3389.642.47
2251281-25128188.87589.88
3255503-25550390.36891.37
4251872-25187289.08490.08
5251063-25106388.79889.80
6238581-23858184.38385.36
45min1257888-25788891.21289.312.6992.5090.572.67
2252671-25267189.36790.64
3257791-25779191.17792.45
4254215-25421589.91391.17
5252968-25296889.47290.74
6239478-23947884.70085.93
60min1256742-25674290.80689.392.3692.3790.932.35
2252763-25276389.39990.94
3257542-25754291.08992.63
4253941-25394189.81691.35
5254370-25437089.96891.50
6241142-24114285.28986.78
极限1270935-27093595.82694.600.7697.6696.400.77
2267775-26777594.70996.52
3267628-26762894.65796.47
4267608-26760894.65096.45
5265235-26523593.81095.61
6265688-26568893.97195.71
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.242838872834722834142831492830382833920.12
210.222781342775852778600.14
单位质量响应值RSD%判断
27675.0027187.871.26数据可信
供试品溶液-2025071821批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1220476-22047680.21979.871.3480.2279.871.34
2218310-21831079.43179.43
3224483-22448381.67781.68
4219048-21904879.69979.70
5215585-21558578.44078.44
6219219-21921979.76279.76
10min1243446-24344688.57788.391.4288.8288.631.43
2243425-24342588.56988.81
3247563-24756390.07590.32
4242257-24225788.14488.38
5236939-23693986.20986.44
6243969-24396988.76789.01
15min1251481-25148191.50090.961.0392.0191.471.03
2249647-24964790.83391.34
3253102-25310292.09092.61
4248766-24876690.51291.02
5245795-24579589.43189.93
6251263-25126391.42191.93
20min1247988-24798890.22991.271.2891.0192.051.28
2250373-25037391.09791.87
3255889-25588993.10493.90
4249470-24947090.76891.54
5247896-24789690.19690.96
6253448-25344892.21693.00
30min1251692-25169291.57792.080.9092.6393.140.90
2253582-25358292.26593.31
3256588-25658893.35894.43
4253128-25312892.09993.15
5249792-24979290.88691.92
6253733-25373392.31993.38
45min1252454-25245491.85492.621.3593.1893.951.34
2254847-25484792.72594.05
3260700-26070094.85496.21
4253113-25311392.09493.42
5250883-25088391.28292.59
6255328-25532892.90094.23
60min1252366-25236691.82292.841.2793.4294.451.27
2255055-25505592.80094.41
3260963-26096394.95096.59
4254066-25406692.44194.04
5252281-25228191.79193.37
6256319-25631993.26094.87
极限1269259-26925997.96998.051.7999.8599.931.78
2267286-26728697.25199.13
3275283-275283100.160102.08
4263840-26384095.99797.87
5265958-26595896.76798.62
6275240-275240100.145102.04
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