辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.242871392872002870122868312863232869010.13
210.222895482901392898440.15
单位质量响应值RSD%判断
28017.6828360.470.86数据可信
供试品溶液-2025071821批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1232143-23214382.19079.892.1182.1979.892.11
2218590-21859077.39277.39
3223750-22375079.21979.22
4223612-22361279.17079.17
5226655-22665580.24780.25
6229162-22916281.13581.14
10min1247790-24779087.73086.523.1987.9886.763.18
2243154-24315486.08986.32
3246711-24671187.34887.59
4248424-24842487.95588.19
5229306-22930681.18681.43
6250811-25081188.80089.04
15min1252507-25250789.40089.781.1389.9190.281.13
2249484-24948488.33088.82
3253249-25324989.66390.16
4255804-25580490.56891.07
5252748-25274889.48689.97
6257699-25769991.23991.75
20min1253006-25300689.57790.301.1990.3591.071.19
2250988-25098888.86389.62
3254795-25479590.21090.98
4257235-25723591.07491.85
5254771-25477190.20290.95
6259517-25951791.88292.67
30min1253443-25344389.73290.591.1790.7891.631.17
2252521-25252189.40590.43
3255227-25522790.36391.40
4258473-25847391.51392.56
5255248-25524890.37191.39
6260348-26034892.17693.24
45min1255126-25512690.32890.981.1591.6492.301.15
2253283-25328389.67590.97
3255752-25575290.54991.86
4259287-25928791.80193.12
5257031-25703191.00292.30
6261390-26139092.54593.88
60min1254888-25488890.24391.121.1391.8392.701.13
2254020-25402089.93691.50
3257322-25732291.10592.69
4258497-25849791.52193.12
5257184-25718491.05692.62
6262221-26222192.84094.45
极限1272390-27239096.44096.700.6798.3098.550.68
2271046-27104695.96497.79
3273903-27390396.97698.83
4272425-27242596.45298.32
5272593-27259396.51298.35
6276324-27632497.83399.72
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.242813932810322810142805942809402809950.11
210.222820162806322813240.35
单位质量响应值RSD%判断
27440.9227526.810.23数据可信
供试品溶液-2025071721批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1206900-20690075.13073.371.7475.1373.371.74
2200002-20000272.62572.63
3199287-19928772.36672.37
4202775-20277573.63273.63
5205206-20520674.51574.52
6198068-19806871.92371.92
10min1228347-22834782.91881.822.5383.1482.042.53
2227397-22739782.57382.79
3223748-22374881.24881.47
4229813-22981383.45083.67
5228249-22824982.88283.11
6214469-21446977.87978.09
15min1236487-23648785.87484.832.5686.3585.302.56
2236518-23651885.88586.35
3232809-23280984.53885.00
4237882-23788286.38086.85
5236095-23609585.73286.20
6221916-22191680.58381.03
20min1240267-24026787.24686.552.6287.9887.262.61
2243303-24330388.34989.07
3236890-23689086.02086.73
4242184-24218487.94388.67
5240942-24094287.49288.22
6226438-22643882.22582.92
30min1243619-24361988.46487.662.8289.4688.642.81
2245812-24581289.26090.25
3241203-24120387.58688.56
4247276-24727689.79290.79
5242259-24225987.97088.96
6228338-22833882.91583.85
45min1247241-24724189.77988.952.9591.0490.192.95
2250835-25083591.08492.34
3244376-24437688.73989.97
4249244-24924490.50691.77
5247137-24713789.74191.00
6230903-23090383.84685.03
60min1247071-24707189.71789.383.0491.2590.893.02
2250421-25042190.93492.46
3246336-24633689.45090.95
4253602-25360292.08993.62
5247491-24749189.87091.39
6231924-23192484.21785.66
极限1261102-26110294.81295.301.2596.6197.071.27
2264123-26412395.90997.71
3261374-26137494.91196.68
4265113-26511396.26998.08
5265850-26585096.53698.33
6257050-25705093.34195.03
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