托伐普坦口崩片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101242-202302对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数1000
标示量(mg)15供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.473845183856633850963845523850993849860.13
216.533885533901173893350.29
单位质量响应值RSD%判断
23374.9823553.240.54数据可信
供试品溶液-2025050421批-shui(内含0.22%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1353292-35329290.25189.761.8090.2589.761.80
2351105-35110589.69289.69
3359658-35965891.87791.88
4342231-34223187.42687.43
5355586-35558690.83790.84
6346385-34638588.48788.49
10min1374844-37484495.75794.911.0295.9195.061.01
2366665-36666593.66793.82
3376645-37664596.21796.37
4371659-37165994.94395.09
5370927-37092794.75694.91
6368472-36847294.12994.28
15min1377088-37708896.33096.420.8896.6496.730.88
2375611-37561195.95396.26
3383208-38320897.89398.21
4379251-37925196.88397.19
5374415-37441595.64795.96
6374994-37499495.79596.10
20min1379826-37982697.02996.221.0697.5096.691.05
2373237-37323795.34695.81
3382828-38282897.79698.27
4376631-37663196.21396.68
5374498-37449895.66896.14
6372916-37291695.26495.73
30min1376539-37653996.19096.721.0496.8297.341.04
2377302-37730296.38597.01
3385476-38547698.47399.11
4380708-38070897.25597.88
5374373-37437395.63696.26
6377251-37725196.37296.99
45min1377745-37774596.49896.781.4297.2997.571.41
2371502-37150294.90395.69
3387515-38751598.99499.80
4380094-38009497.09897.89
5375858-37585896.01696.80
6380315-38031597.15497.94
60min1376008-37600896.05496.650.8497.0197.600.84
2374421-37442195.64996.59
3383273-38327397.91098.88
4377374-37737496.40397.35
5380100-38010097.09998.05
6378786-37878696.76497.71
极限1387735-38773599.05098.281.10100.1699.391.10
2383161-38316197.88198.98
3391693-391693100.061101.19
4383349-38334997.92999.04
5382444-38244497.69898.81
6379996-37999697.07398.18
托伐普坦口崩片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101242-202302对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数1000
标示量(mg)15供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.473871633867093872463871513866893869920.07
216.533925963919373922660.12
单位质量响应值RSD%判断
23496.7823730.550.71数据可信
供试品溶液-2025050421批-shui(内含0.22%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1370025-37002593.92895.701.1993.9395.701.19
2381314-38131496.79496.79
3380332-38033296.54496.54
4377977-37797795.94795.95
5379249-37924996.26996.27
6373123-37312394.71494.71
10min1376682-37668295.61897.981.4495.7798.141.44
2392346-39234699.59499.76
3388036-38803698.50098.66
4389299-38929998.82198.98
5386747-38674798.17398.33
6382715-38271597.14997.31
15min1375787-37578795.39197.501.3795.7197.821.37
2389767-38976798.93999.27
3384198-38419897.52697.85
4389653-38965398.91099.24
5382883-38288397.19297.52
6382286-38228697.04097.36
20min1371911-37191194.40796.891.4394.8897.381.43
2385073-38507397.74898.24
3382507-38250797.09697.58
4388007-38800798.49398.98
5381247-38124796.77797.26
6381443-38144396.82697.31
30min1373727-37372794.86897.161.5195.5097.811.51
2388885-38888598.71599.37
3386124-38612498.01598.66
4386714-38671498.16498.82
5382964-38296497.21297.86
6378249-37824996.01696.66
45min1373170-37317094.72696.991.3995.5297.801.39
2386684-38668498.15798.98
3381067-38106796.73197.54
4388120-38812098.52199.34
5380904-38090496.69097.50
6382623-38262397.12697.93
60min1373878-37387894.90696.941.2195.8597.911.21
2383556-38355697.36398.35
3383969-38396997.46898.44
4387572-38757298.38299.36
5381954-38195496.95697.93
6380403-38040396.56297.53
极限1372250-37225094.49396.831.4295.6097.961.41
2389088-38908898.76799.91
3381752-38175296.90598.04
4382710-38271097.14898.29
5381499-38149996.84197.97
6381338-38133896.80097.93
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