熊去氧胆酸口服混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号C092A240304对照品来源原料对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数50
标示量(mg)250供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.935415254607543255430854218543220.33
214.025499854911549540.12
单位质量响应值RSD%判断
3899.643919.690.37数据可信
供试品溶液-240003A批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min129867-2986755.00353.701.4155.0053.701.41
228778-2877852.99853.00
329324-2932454.00354.00
429206-2920653.78653.79
528994-2899453.39553.40
628786-2878653.01253.01
10min132070-3207059.06057.831.1559.3758.131.15
231263-3126357.57457.87
331543-3154358.09058.39
431146-3114657.35957.66
531264-3126457.57657.87
631122-3112257.31457.61
15min133056-3305660.87660.050.8661.5160.670.87
232257-3225759.40560.02
332740-3274060.29460.92
432665-3266560.15660.77
532516-3251659.88260.50
632410-3241059.68660.30
20min133548-3354861.78261.170.8262.7562.120.82
232935-3293560.65361.60
333389-3338961.48962.45
433383-3338361.47862.43
533153-3315361.05562.00
632871-3287160.53561.48
30min134454-3445463.45162.630.8164.7763.930.81
233677-3367762.02063.30
334142-3414262.87664.18
434041-3404162.69063.98
533939-3393962.50263.79
633805-3380562.25563.54
45min134862-3486264.20263.830.4365.8765.470.44
234447-3444763.43865.06
334716-3471663.93365.58
434641-3464163.79565.44
534743-3474363.98365.62
634547-3454763.62265.25
60min135139-3513964.71264.340.7766.7466.340.77
234603-3460363.72565.70
335344-3534465.09067.09
434894-3489464.26166.26
534924-3492464.31666.31
634734-3473463.96665.95
极限135786-3578665.90465.600.7268.2967.950.72
235379-3537965.15467.49
335880-3588066.07768.44
435864-3586466.04768.40
535517-3551765.40867.76
635299-3529965.00767.34
熊去氧胆酸口服混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号C092A240304对照品来源原料对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数50
标示量(mg)250供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.935443555082544635455854512546100.50
214.025468054638546590.06
单位质量响应值RSD%判断
3920.323898.640.40数据可信
供试品溶液-240003A批-pH4.5(内含0.2%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min142940-4294079.08284.475.3879.0884.475.38
243053-4305379.29079.29
346637-4663785.89185.89
447229-4722986.98186.98
549236-4923690.67890.68
646108-4610884.91784.92
10min147701-4770187.85188.102.7588.2988.572.76
245507-4550783.81084.25
348215-4821588.79789.27
448260-4826088.88089.36
549521-4952191.20291.71
647822-4782288.07388.55
15min148779-4877989.83691.312.7790.7692.262.78
247546-4754687.56588.47
350407-5040792.83493.80
450211-5021192.47393.45
551406-5140694.67495.68
649123-4912390.46991.43
20min149990-4999092.06693.472.6893.4994.942.69
248493-4849389.30990.70
351621-5162195.07096.56
451801-5180195.40196.89
552030-5203095.82397.36
650579-5057993.15194.61
30min151633-5163395.09296.562.3497.0398.542.36
250504-5050493.01394.90
352950-5295097.51899.53
453340-5334098.236100.26
553859-5385999.192101.26
652296-5229696.31398.29
45min153173-5317397.92898.842.58100.39101.362.59
251453-5145394.76197.17
354305-54305100.013102.57
454850-54850101.017103.58
555165-55165101.597104.22
653065-5306597.729100.25
60min153585-5358598.687100.152.77101.70103.222.77
252128-5212896.00498.94
354621-54621100.595103.71
456237-56237103.571106.70
555769-55769102.709105.89
653944-5394499.348102.41
极限154165-5416599.75599.552.37103.31103.172.37
252424-5242496.549100.01
353040-5304097.683101.35
454510-54510100.391104.09
556126-56126103.367107.12
654046-5404699.536103.15
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