熊去氧胆酸口服混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号C092A240304对照品来源原料对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数50
标示量(mg)250供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.215630856582561235598855898561800.49
214.185618756190561880.01
单位质量响应值RSD%判断
3953.553962.480.16数据可信
供试品溶液-240003A批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125525-2552546.43246.552.4346.4346.552.42
226537-2653748.27348.27
325646-2564646.65246.65
425904-2590447.12247.12
525212-2521245.86345.86
624709-2470944.94844.95
10min130396-3039655.29352.942.5755.5553.202.57
229481-2948153.62953.90
328963-2896352.68652.95
428862-2886252.50352.76
528623-2862352.06852.32
628284-2828451.45151.70
15min131890-3189058.01155.942.2058.5856.502.20
231182-3118256.72357.29
330564-3056455.59956.15
430499-3049955.48156.03
530009-3000954.58955.13
630372-3037255.25055.79
20min132174-3217458.52857.411.5159.4158.281.51
232054-3205458.30959.19
331493-3149357.28958.15
431517-3151757.33258.19
530994-3099456.38157.23
631142-3114256.65057.49
30min133534-3353461.00259.052.1562.2160.242.14
232915-3291559.87561.08
332274-3227458.70959.89
431494-3149457.29158.47
532136-3213658.45859.62
632425-3242558.98460.14
45min133988-3398861.82760.481.7063.3861.991.70
233729-3372961.35662.89
333136-3313660.27861.78
433209-3320960.41061.91
532373-3237358.89060.37
633065-3306560.14861.63
60min134036-3403661.91561.320.7763.8163.160.78
233651-3365161.21463.09
333798-3379861.48263.32
433798-3379861.48263.32
533705-3370561.31363.13
633251-3325160.48762.31
极限135110-3511063.86863.910.7666.1166.100.75
235231-3523164.08966.31
335040-3504063.74165.92
435429-3542964.44966.62
534674-3467463.07565.23
635328-3532864.26566.42
熊去氧胆酸口服混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号C092A240304对照品来源原料对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数50
标示量(mg)250供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.215625656425561495600055853561370.40
214.185576455896558300.17
单位质量响应值RSD%判断
3950.533937.240.24数据可信
供试品溶液-240003A批-pH4.5(内含0.2%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min146813-4681385.46379.984.8185.4679.984.81
241914-4191476.51976.52
345986-4598683.95383.95
443471-4347179.36179.36
542782-4278278.10478.10
641898-4189876.49076.49
10min147018-4701885.83783.972.4086.3184.422.41
244146-4414680.59481.02
346883-4688385.59086.06
446359-4635984.63485.07
546339-4633984.59785.03
645239-4523982.58983.01
15min147812-4781287.28687.461.8188.2488.371.81
246210-4621084.36285.23
348518-4851888.57589.52
448337-4833788.24589.16
548299-4829988.17689.08
648263-4826388.11088.99
20min149666-4966690.67188.891.8292.1190.281.83
247231-4723186.22687.57
349085-4908589.61091.04
449243-4924389.89991.30
548805-4880589.09990.49
648100-4810087.81289.19
30min151548-5154894.10792.182.2196.0594.082.21
248418-4841888.39390.21
351248-5124893.55995.49
450855-5085592.84294.74
550644-5064492.45794.35
650256-5025691.74893.61
45min152379-5237995.62494.542.1798.0996.942.17
249704-4970490.74193.05
352952-5295296.67099.12
452213-5221395.32197.74
551889-5188994.72997.13
651564-5156494.13696.51
60min152934-5293496.63795.652.7399.6398.582.71
249577-4957790.50993.32
353297-5329797.300100.29
453436-5343697.554100.50
552415-5241595.69098.62
652697-5269796.20599.10
极限153521-5352197.70996.731.78101.24100.191.79
251181-5118193.43796.76
353728-5372898.087101.62
453434-5343497.550101.04
553245-5324597.205100.67
652790-5279096.37499.80
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