辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852621162624232628602630172622032625240.16
210.042640232635462637840.13
单位质量响应值RSD%判断
26652.1826273.311.02数据可信
供试品溶液-236B11S批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1243165-24316591.71095.182.1491.7195.182.14
2250342-25034294.41794.42
3252318-25231895.16395.16
4258756-25875697.59197.59
5256098-25609896.58896.59
6253505-25350595.61095.61
10min1252376-25237695.18497.451.2295.4697.741.23
2257903-25790397.26997.55
3259434-25943497.84698.13
4260406-26040698.21398.51
5261140-26114098.49098.78
6259026-25902697.69397.98
15min1253709-25370995.68797.951.2596.2598.531.25
2258495-25849597.49298.07
3261264-26126498.53799.12
4260816-26081698.36898.96
5262587-26258799.03699.62
6261366-26136698.57599.15
20min1252458-25245895.21597.861.4896.0698.731.48
2258110-25811097.34798.21
3261018-26101898.44499.32
4261591-26159198.66099.54
5263236-26323699.280100.16
6260437-26043798.22599.10
30min1252021-25202195.05197.691.5996.1898.851.58
2257436-25743697.09398.25
3260347-26034798.19199.36
4261340-26134098.56599.74
5264039-26403999.583100.76
6258895-25889597.64398.81
45min1252866-25286695.36997.621.2596.7999.081.25
2257754-25775497.21398.66
3260368-26036898.19999.66
4260394-26039498.20899.68
5261957-26195798.798100.28
6259692-25969297.94499.41
60min1252054-25205495.06397.601.3696.7799.351.36
2258177-25817797.37299.11
3260422-26042298.21999.98
4261578-26157898.655100.42
5261038-26103898.451100.23
6259376-25937697.82599.58
极限1258263-25826397.40599.581.2599.39101.631.25
2262548-26254899.021101.06
3266123-266123100.369102.42
4266900-266900100.662102.73
5266406-266406100.476102.55
6263983-26398399.562101.61
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852631022637492639272637662640902637270.15
210.042675522682612679060.19
单位质量响应值RSD%判断
26774.3126683.860.24数据可信
供试品溶液-236B11S批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1255239-25523995.30093.652.3795.3093.652.36
2245976-24597691.84291.84
3260306-26030697.19297.19
4246506-24650692.04092.04
5245959-24595991.83591.84
6250899-25089993.68093.68
10min1257894-25789496.29295.143.3796.5895.423.37
2241961-24196190.34390.62
3268438-268438100.229100.52
4252711-25271194.35694.63
5254729-25472995.11095.39
6253156-25315694.52394.80
15min1258849-25884996.64896.372.1197.2296.932.11
2257614-25761496.18796.73
3268369-268369100.203100.80
4254988-25498895.20795.77
5255860-25586095.53296.09
6252896-25289694.42694.99
20min1259283-25928396.81096.161.9097.6897.021.91
2257371-25737196.09696.93
3266360-26636099.453100.35
4253018-25301894.47195.32
5255386-25538695.35596.20
6253854-25385494.78395.63
30min1259631-25963196.94096.331.8198.1097.471.81
2257166-25716696.02097.14
3266511-26651199.509100.70
4254918-25491895.18196.31
5256151-25615195.64196.77
6253569-25356994.67795.81
45min1260049-26004997.09696.542.3098.5497.972.29
2258309-25830996.44797.86
3269476-269476100.616102.11
4253500-25350094.65196.06
5256307-25630795.69997.12
6253725-25372594.73596.15
60min1260404-26040497.22996.582.1598.9798.302.15
2257893-25789396.29197.99
3268900-268900100.401102.19
4254015-25401594.84396.54
5256541-25654195.78797.49
6254269-25426994.93896.64
极限1265855-26585599.26498.701.73101.29100.721.74
2264384-26438498.715100.70
3271945-271945101.538103.63
4258038-25803896.34598.33
5263480-26348098.377100.37
6262426-26242697.98499.97
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852682392684522691932686012690882687150.16
210.042787842795112791480.19
单位质量响应值RSD%判断
27280.7127803.591.35数据可信
供试品溶液-243B62S批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1246210-24621089.22388.651.7689.2288.651.76
2237957-23795786.23286.23
3248900-24890090.19890.20
4241442-24144287.49587.50
5248694-24869490.12390.12
6244619-24461988.64788.65
10min1253255-25325591.77691.681.1492.0491.941.15
2248694-24869490.12390.38
3256789-25678993.05793.33
4250788-25078890.88291.14
5254839-25483992.35092.62
6253577-25357791.89392.16
15min1254511-25451192.23192.211.0992.7792.741.10
2249988-24998890.59291.12
3258073-25807393.52294.07
4253003-25300391.68592.22
5256202-25620292.84493.39
6254874-25487492.36392.90
20min1256524-25652492.96193.061.3693.7893.881.37
2251367-25136791.09291.89
3260956-26095694.56795.40
4254433-25443392.20393.01
5258146-25814693.54994.37
6259384-25938493.99794.82
30min1256579-25657992.98193.381.2394.0894.481.23
2252832-25283291.62392.70
3261259-26125994.67795.79
4256612-25661292.99394.08
5261037-26103794.59695.70
6257804-25780493.42594.53
45min1259942-25994294.19993.951.1695.5895.331.16
2254771-25477192.32693.67
3262076-26207694.97396.37
4256494-25649492.95094.32
5262005-26200594.94796.34
6260313-26031394.33495.71
60min1262593-26259395.16094.961.2596.8296.621.25
2257180-25718093.19994.82
3265870-26587096.34898.03
4259642-25964294.09195.74
5264965-26496596.02097.69
6262066-26206694.96996.63
极限1266736-26673696.66196.661.4798.6198.601.47
2260750-26075094.49296.40
3272957-27295798.916100.89
4265714-26571496.29198.22
5267801-26780197.04799.01
6266392-26639296.53798.49
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852638122644772638542646032653722644240.25
210.042735182734172734680.03
单位质量响应值RSD%判断
26845.0827237.851.03数据可信
供试品溶液-243B62S批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1251662-25166292.88491.121.3992.8891.121.39
2244534-24453490.25390.25
3249164-24916491.96291.96
4242035-24203589.33189.33
5246168-24616890.85690.86
6247779-24777991.45191.45
10min1261101-26110196.36894.331.4396.6594.601.43
2252585-25258593.22593.50
3258002-25800295.22495.50
4251402-25140292.78893.06
5256511-25651194.67494.95
6253849-25384993.69193.97
15min1263365-26336597.20394.881.5097.7795.441.50
2254468-25446893.92094.47
3258609-25860995.44896.01
4252247-25224793.10093.65
5257833-25783395.16295.72
6255941-25594194.46395.02
20min1264265-26426597.53695.011.5598.3995.851.55
2255232-25523294.20295.03
3259476-25947695.76896.62
4252828-25282893.31494.14
5256629-25662994.71795.56
6256100-25610094.52295.36
30min1264933-26493397.78295.291.6598.9396.411.65
2256087-25608794.51795.63
3261187-26118796.40097.53
4254627-25462793.97895.08
5258425-25842595.38096.51
6253825-25382593.68294.80
45min1265523-26552398.00095.331.7099.4596.741.69
2254795-25479594.04095.44
3261051-26105196.34997.77
4255491-25549194.29795.68
5258487-25848795.40396.82
6254350-25435093.87695.28
60min1269201-26920199.35796.421.77101.1098.121.76
2258146-25814695.27796.96
3263662-26366297.31399.03
4256489-25648994.66696.34
5260833-26083396.26997.97
6259121-25912195.63797.32
极限1274149-274149101.18497.931.71103.2299.921.70
2263446-26344697.23399.20
3265034-26503497.81999.82
4261783-26178396.61998.57
5262465-26246596.87198.86
6265184-26518497.87599.85
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