辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852629452625212629682631472631142629390.10
210.042644482643632644060.03
单位质量响应值RSD%判断
26694.3126335.260.96数据可信
供试品溶液-249A29S批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1241749-24174990.99790.191.4891.0090.191.48
2235946-23594688.81388.81
3240670-24067090.59190.59
4243983-24398391.83891.84
5234736-23473688.35788.36
6240478-24047890.51990.52
10min1251849-25184994.79993.921.4595.0794.191.45
2246880-24688092.92893.19
3250794-25079494.40294.67
4252794-25279495.15495.43
5243427-24342791.62991.89
6251357-25135794.61494.89
15min1252133-25213394.90694.391.3595.4694.941.35
2248412-24841293.50594.05
3250837-25083794.41894.97
4254868-25486895.93596.50
5245450-24545092.39092.93
6252922-25292295.20395.76
20min1251959-25195994.84094.451.5695.6895.281.56
2247588-24758893.19594.02
3252816-25281695.16396.00
4255074-25507496.01396.86
5244783-24478392.13992.96
6253245-25324595.32496.17
30min1253034-25303495.24594.471.5596.3795.581.55
2248174-24817493.41594.52
3252581-25258195.07496.20
4254730-25473095.88397.02
5244403-24440391.99693.09
6252860-25286095.17996.31
45min1252657-25265795.10394.431.6896.5295.831.67
2246746-24674692.87894.26
3252102-25210294.89496.30
4254646-25464695.85297.28
5244622-24462292.07893.45
6254460-25446095.78297.19
60min1252521-25252195.05294.251.5796.7595.941.57
2246831-24683192.91094.57
3251867-25186794.80696.50
4253924-25392495.58097.29
5244216-24421691.92693.57
6253019-25301995.23996.94
极限1263402-26340299.14797.881.63101.1399.841.63
2257144-25714496.79298.73
3262346-26234698.750100.73
4263374-26337499.137101.14
5252821-25282195.16597.09
6261063-26106398.267100.25
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852648752650752647242643612654262648920.15
210.042672272670342671300.06
单位质量响应值RSD%判断
26892.5926606.570.76数据可信
供试品溶液-249A29S批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1240875-24087589.87189.001.3889.8789.001.38
2242097-24209790.32790.33
3239636-23963689.40889.41
4233356-23335687.06587.07
5235891-23589188.01188.01
6239349-23934989.30189.30
10min1249976-24997693.26692.311.5893.5492.581.58
2252399-25239994.17094.44
3250050-25005093.29493.56
4243211-24321190.74291.00
5245329-24532991.53291.80
6243503-24350390.85191.12
15min1251612-25161293.87793.011.4194.4393.551.41
2253734-25373494.66895.22
3251305-25130593.76294.31
4245047-24504791.42791.96
5248282-24828292.63493.17
6245723-24572391.67992.22
20min1253415-25341594.54993.111.7295.3893.931.71
2254505-25450594.95695.79
3251651-25165193.89194.72
4244147-24414791.09191.90
5247979-24797992.52193.34
6245611-24561191.63892.45
30min1253658-25365894.64093.131.5995.7594.241.59
2253247-25324794.48795.61
3252487-25248794.20395.31
4244673-24467391.28892.37
5247414-24741492.31093.40
6246258-24625891.87992.97
45min1251310-25131093.76492.811.4695.1694.191.46
2253195-25319594.46795.87
3250862-25086293.59794.99
4244025-24402591.04692.40
5247666-24766692.40493.78
6245402-24540291.56092.93
60min1251296-25129693.75992.721.2795.4494.381.28
2251150-25115093.70495.39
3251160-25116093.70895.38
4244613-24461391.26592.89
5247809-24780992.45894.11
6245011-24501191.41493.05
极限1262993-26299398.12396.671.70100.0898.601.70
2264431-26443198.659100.63
3261348-26134897.50999.46
4254229-25422994.85396.75
5256878-25687895.84197.77
6254665-25466595.01696.93
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852663602668772668562669032661382666270.14
210.042665462665282665370.01
单位质量响应值RSD%判断
27068.7326547.511.38数据可信
供试品溶液-249A29S批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1250380-25038093.21993.801.0293.2293.801.01
2252590-25259094.04294.04
3250374-25037493.21793.22
4250558-25055893.28593.29
5256866-25686695.63495.63
6250928-25092893.42393.42
10min1255719-25571995.20795.610.7695.4995.900.76
2260392-26039296.94797.23
3254749-25474994.84695.13
4256145-25614595.36595.65
5256579-25657995.52795.81
6257288-25728895.79196.07
15min1256646-25664695.55296.160.4796.1296.730.47
2260007-26000796.80397.38
3259247-25924796.52097.08
4257833-25783395.99496.56
5257529-25752995.88196.45
6258414-25841496.21096.78
20min1255908-25590895.27796.220.9296.1397.070.91
2261764-26176497.45798.32
3256002-25600295.31296.17
4259098-25909896.46597.32
5260227-26022796.88597.75
6257570-25757095.89696.75
30min1257349-25734995.81496.220.5596.9597.370.55
2260652-26065297.04398.20
3256757-25675795.59396.73
4258974-25897496.41997.56
5259068-25906896.45497.61
6257880-25788096.01197.16
45min1257204-25720495.76096.460.5897.1897.890.58
2261511-26151197.36398.81
3259616-25961696.65898.08
4259524-25952496.62398.06
5258234-25823496.14397.58
6258425-25842596.21497.65
60min1257093-25709395.71896.280.7597.4398.010.75
2262390-26239097.69199.43
3257480-25748095.86297.58
4257796-25779695.98097.70
5258151-25815196.11297.84
6258752-25875296.33698.06
极限1261526-26152697.36997.780.9999.3799.800.97
2264070-26407098.316100.35
3263627-26362798.151100.16
4258139-25813996.10898.12
5262932-26293297.89299.91
6265564-26556498.872100.88
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852661702661412661352653792656112658870.14
210.042671242673932672580.08
单位质量响应值RSD%判断
26993.6026619.320.99数据可信
供试品溶液-249A29S批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1249387-24938792.85193.931.2592.8593.931.25
2257663-25766395.93295.93
3250714-25071493.34593.34
4254412-25441294.72294.72
5250374-25037493.21893.22
6251216-25121693.53293.53
10min1253577-25357794.41195.541.1194.6995.821.11
2261015-26101597.18097.47
3255567-25556795.15295.43
4259109-25910996.47196.75
5254901-25490194.90495.18
6255434-25543495.10295.38
15min1255709-25570995.20595.731.0295.7796.301.02
2259509-25950996.61997.20
3254910-25491094.90795.47
4261247-26124797.26797.84
5255752-25575295.22195.79
6255515-25551595.13295.70
20min1256621-25662195.54496.060.7696.3996.920.76
2260074-26007496.83097.70
3256853-25685395.63196.48
4260450-26045096.97097.84
5258395-25839596.20597.05
6255714-25571495.20796.06
30min1256021-25602195.32195.850.9696.4597.000.96
2259695-25969596.68997.85
3256007-25600795.31696.45
4261368-26136897.31298.47
5256039-25603995.32896.47
6255578-25557895.15696.29
45min1256358-25635895.44695.991.0896.8797.421.07
2260121-26012196.84798.30
3254933-25493394.91696.34
4262221-26222197.62999.08
5256398-25639895.46196.89
6256843-25684395.62797.05
60min1255946-25594695.29396.141.0397.0097.861.02
2261180-26118097.24298.98
3256418-25641895.46997.18
4261962-26196297.53399.27
5257062-25706295.70897.42
6256699-25669995.57397.28
极限1260711-26071197.06797.890.9999.0699.890.99
2266166-26616699.098101.13
3259966-25996696.79098.78
4265863-26586398.985101.02
5262245-26224597.63899.64
6262512-26251297.73899.73
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