辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852605152604062606902603322604802604850.06
210.042612742603222607980.26
单位质量响应值RSD%判断
26445.1825975.901.27数据可信
供试品溶液-236B11S批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1246636-24663693.91793.860.9793.9293.860.97
2242388-24238892.30092.30
3249215-24921594.89994.90
4246296-24629693.78893.79
5245974-24597493.66593.67
6248420-24842094.59794.60
10min1256710-25671097.75397.240.7198.0497.520.71
2254201-25420196.79897.07
3258112-25811298.28798.57
4253083-25308396.37296.65
5255297-25529797.21597.50
6254694-25469496.98697.27
15min1259078-25907898.65598.180.6199.2398.750.61
2255860-25586097.43098.00
3259933-25993398.98199.56
4257431-25743198.02898.60
5256454-25645497.65698.23
6258210-25821098.32598.90
20min1259410-25941098.78298.190.4899.6599.060.48
2256517-25651797.68098.54
3259269-25926998.72899.60
4256885-25688597.82098.68
5257668-25766898.11898.98
6257416-25741698.02298.89
30min1258341-25834198.37598.180.6599.5499.340.65
2255702-25570297.37098.52
3260105-26010599.046100.22
4257832-25783298.18199.34
5258873-25887398.57799.74
6256105-25610597.52398.69
45min1258397-25839798.39697.340.6499.8698.800.64
2254451-25445196.89398.34
3256701-25670197.75099.22
4254131-25413196.77198.22
5255141-25514197.15698.61
6254967-25496797.09098.55
60min1258202-25820298.32297.270.80100.0899.020.80
2253604-25360496.57198.31
3257707-25770798.13399.90
4253861-25386196.66998.41
5253999-25399996.72198.47
6255209-25520997.18298.93
极限1259064-25906498.65097.690.68100.7099.730.68
2254459-25445996.89698.92
3258179-25817998.313100.37
4255970-25597097.47299.50
5256176-25617697.55099.59
6255394-25539497.25299.29
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852587872584322584782576432590192584720.21
210.042597402594592596000.08
单位质量响应值RSD%判断
26240.8125856.571.05数据可信
供试品溶液-243B62S批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1255953-25595398.06895.041.9198.0795.041.91
2243392-24339293.25693.26
3246631-24663194.49794.50
4251217-25121796.25496.25
5246784-24678494.55594.56
6244295-24429593.60193.60
10min1260042-26004299.63597.582.0799.9397.862.07
2252187-25218796.62596.91
3251747-25174796.45796.74
4259625-25962599.47599.76
5257582-25758298.69298.98
6246823-24682394.57094.85
15min1260583-26058399.84298.491.56100.4499.061.56
2254979-25497997.69598.26
3254968-25496897.69198.26
4261391-261391100.152100.74
5259218-25921899.31999.90
6251121-25112196.21796.78
20min1261613-261613100.23798.182.12101.1399.062.11
2252954-25295496.91997.78
3256602-25660298.31799.18
4259014-25901499.241100.13
5260226-26022699.705100.58
6247121-24712194.68495.54
30min1260809-26080999.92997.862.03101.1299.032.03
2254913-25491397.67098.82
3250463-25046395.96597.13
4259746-25974699.522100.71
5258378-25837898.997100.17
6248155-24815595.08096.22
45min1260270-26027099.72297.691.84101.2299.161.84
2254614-25461497.55599.00
3253981-25398197.31398.76
4257728-25772898.748100.23
5256651-25665198.33699.81
6246607-24660794.48795.91
60min1259903-25990399.58297.811.93101.3799.561.93
2255609-25560997.93699.68
3252847-25284796.87898.62
4258604-25860499.084100.86
5258070-25807098.879100.65
6246617-24661794.49196.20
极限1263732-263732101.04999.071.95103.14101.121.94
2260509-26050999.814101.85
3256262-25626298.187100.22
4259319-25931999.358101.44
5261906-261906100.349102.41
6249712-24971295.67797.67
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852572442581022567442576312565492572540.25
210.042675482674942675210.02
单位质量响应值RSD%判断
26117.1626645.521.42数据可信
供试品溶液-249A29S批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1240729-24072991.07691.921.0791.0891.921.07
2243609-24360992.16692.17
3247434-24743493.61393.61
4243592-24359292.16092.16
5240265-24026590.90190.90
6242131-24213191.60791.61
10min1250439-25043994.75095.160.9395.0295.440.93
2251533-25153395.16495.44
3256165-25616596.91697.20
4250055-25005594.60594.88
5250526-25052694.78395.06
6250470-25047094.76295.04
15min1251339-25133995.09195.690.8595.6596.250.85
2252950-25295095.70096.26
3256599-25659997.08197.65
4251509-25150995.15595.72
5251022-25102294.97195.53
6254068-25406896.12396.68
20min1251960-25196095.32595.711.0096.1796.561.00
2252239-25223995.43196.28
3257995-25799597.60998.47
4252344-25234495.47196.32
5250864-25086494.91195.75
6252492-25249295.52796.37
30min1249362-24936294.34395.181.0295.4796.321.02
2250881-25088194.91796.05
3256569-25656997.06998.22
4250765-25076594.87396.01
5250194-25019494.65795.78
6251733-25173395.24096.37
45min1249323-24932394.32895.511.0995.7496.931.09
2252678-25267895.59797.02
3257441-25744197.39998.85
4252455-25245595.51396.93
5251934-25193495.31696.73
6250829-25082994.89896.32
60min1246748-24674893.35496.111.7695.0597.821.75
2254399-25439996.24897.96
3260540-26054098.572100.31
4253615-25361595.95297.65
5253084-25308495.75197.45
6255815-25581596.78498.49
极限1255154-25515496.53496.373.0898.5198.373.03
2261098-26109898.783100.78
3261939-26193999.101101.14
4256776-25677697.14899.14
5240348-24034890.93292.92
6253007-25300795.72297.72
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