辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852604552612522615602615482616742612980.19
210.042635222643252639240.22
单位质量响应值RSD%判断
26527.7226287.250.65数据可信
供试品溶液-236B11S批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1258511-25851197.69994.163.0797.7094.163.08
2239880-23988090.65890.66
3251893-25189395.19895.20
4248931-24893194.07994.08
5240497-24049790.89190.89
6255193-25519396.44596.45
10min1262020-26202099.02597.552.7299.3297.832.72
2249171-24917194.16994.44
3260938-26093898.61798.90
4258236-25823697.59597.88
5250783-25078394.77995.05
6267548-267548101.115101.40
15min1264040-26404099.78998.392.61100.3898.972.61
2252482-25248295.42195.98
3263518-26351899.592100.17
4260341-26034198.39198.97
5252378-25237895.38195.94
6269314-269314101.782102.37
20min1263727-26372799.67198.242.58100.5699.112.58
2250835-25083594.79895.64
3262736-26273699.296100.18
4261721-26172198.91299.78
5252738-25273895.51896.36
6267892-267892101.245102.14
30min1264146-26414699.82998.002.66101.0299.162.66
2251178-25117894.92896.05
3262221-26222199.101100.28
4259832-25983298.19999.37
5250891-25089194.81995.95
6267512-267512101.101102.30
45min1262922-26292299.36697.512.81100.8598.972.80
2249114-24911494.14895.56
3260220-26022098.34599.82
4259653-25965398.13199.59
5249410-24941094.26095.67
6266741-266741100.810102.31
60min1260584-26058498.48397.292.48100.2799.042.48
2249164-24916494.16795.86
3260477-26047798.442100.21
4258036-25803697.52099.28
5250601-25060194.71096.41
6265706-265706100.419102.23
极限1263198-26319899.47198.492.52101.55100.532.52
2252979-25297995.60997.58
3262032-26203299.030101.10
4260336-26033698.389100.44
5254134-25413496.04598.03
6270861-270861102.367104.48
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852616962607322614912618782607902613170.21
210.042624812609802617300.41
单位质量响应值RSD%判断
26529.6426068.731.24数据可信
供试品溶液-243B62S批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1247777-24777794.03393.842.5194.0393.842.51
2244270-24427092.70392.70
3251138-25113895.30995.31
4240036-24003691.09691.10
5257170-25717097.59897.60
6243141-24314192.27492.27
10min1259834-25983498.60997.052.6398.8997.332.63
2255016-25501696.78197.06
3263211-26321199.891100.18
4249101-24910194.53694.81
5260628-26062898.91199.20
6246533-24653393.56193.84
15min1252995-25299596.01497.152.7096.5997.722.70
2257099-25709997.57198.14
3264469-264469100.368100.95
4251424-25142495.41895.97
5263117-26311799.855100.44
6246790-24679093.65994.22
20min1254415-25441596.55397.151.9097.4298.011.91
2256387-25638797.30198.16
3261964-26196499.418100.30
4253739-25373996.29697.14
5260654-26065498.92099.81
6248722-24872294.39295.23
30min1251916-25191695.60496.942.3696.7698.092.36
2256286-25628697.26398.42
3261727-26172799.328100.51
4251267-25126795.35896.49
5263147-26314799.867101.05
6248236-24823694.20895.33
45min1251088-25108895.29096.952.4396.7398.402.43
2257787-25778797.83299.28
3263849-263849100.133101.62
4252764-25276495.92697.34
5260121-26012198.718100.20
6247216-24721693.82195.22
60min1252643-25264395.88097.072.4397.6198.812.42
2256916-25691697.50299.24
3264873-264873100.522102.30
4252425-25242595.79797.50
5260249-26024998.767100.55
6247617-24761793.97395.66
极限1254465-25446596.57298.272.7098.59100.302.69
2259698-25969898.558100.59
3268553-268553101.918104.00
4253932-25393296.36998.36
5265712-265712100.840102.92
6251224-25122495.34297.31
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.852597082592242599712594512596802596070.11
210.042611022625992618500.41
单位质量响应值RSD%判断
26356.0426080.680.75数据可信
供试品溶液-249A29S批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1244765-24476593.17292.241.9193.1792.241.91
2238902-23890290.94090.94
3245728-24572893.53993.54
4247047-24704794.04194.04
5242584-24258492.34292.34
6234909-23490989.42089.42
10min1254422-25442296.84895.981.8697.1396.261.86
2247417-24741794.18294.45
3252933-25293396.28196.56
4259269-25926998.69398.98
5252143-25214395.98196.26
6246636-24663693.88494.15
15min1254057-25405796.70996.661.6597.2897.221.65
2250678-25067895.42395.98
3256685-25668597.71098.28
4260030-26003098.98399.56
5253755-25375596.59497.16
6248283-24828394.51195.06
20min1254890-25489097.02696.161.5997.8997.021.59
2249643-24964395.02995.87
3255223-25522397.15398.02
4257239-25723997.92198.80
5252185-25218595.99796.85
6246476-24647693.82494.66
30min1254314-25431496.80796.231.7397.9697.381.73
2249111-24911194.82795.95
3254811-25481196.99698.15
4258924-25892498.56299.73
5253014-25301496.31297.46
6246647-24664793.88995.00
45min1254621-25462196.92496.291.9398.3797.721.93
2249467-24946794.96296.37
3254406-25440696.84298.29
4260815-26081599.282100.75
5251693-25169395.80997.24
6246776-24677693.93895.33
60min1253540-25354096.51296.001.9498.2497.721.94
2247320-24732094.14595.84
3255694-25569497.33299.07
4258939-25893998.568100.33
5251407-25140795.70197.42
6246231-24623193.73095.41
极限1256084-25608497.48196.991.5699.5099.001.56
2253071-25307196.33498.31
3257736-25773698.110100.14
4259850-25985098.914100.97
5253423-25342396.46898.47
6248661-24866194.65596.61
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