培哚普利氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号DJ468-220103对照品来源中检院对照品使用方法直接使用
对照品含量(%)94.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)10供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.213914539093390593924539209391500.20
29.123959839243394200.64
单位质量响应值RSD%判断
4250.814322.371.19数据可信
供试品溶液-697902批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min148094-4809495.73397.881.6595.7397.881.65
249031-4903197.59897.60
350248-50248100.020100.02
449231-4923197.99698.00
548538-4853896.61696.62
649889-4988999.30699.31
10min148402-4840296.34697.991.2697.4199.081.27
248926-4892697.38998.47
350147-5014799.819100.93
449352-4935298.23799.33
548895-4889597.32798.40
649647-4964798.82499.93
15min147700-4770094.94896.371.2897.0898.541.28
248507-4850796.55598.72
349254-4925498.042100.26
448672-4867296.88399.06
547667-4766794.88397.04
648671-4867196.88199.08
20min147035-4703593.62595.691.8996.8198.941.87
248006-4800695.55798.80
349072-4907297.679100.99
447883-4788395.31398.57
547242-4724294.03797.25
649206-4920697.946101.22
30min146257-4625792.07693.891.2096.3198.201.19
247286-4728694.12498.43
347520-4752094.59098.99
447880-4788095.30799.62
546846-4684693.24897.50
647210-4721093.97398.34
45min146280-4628092.12292.961.1597.3798.321.16
246403-4640392.36797.71
347460-4746094.47199.92
446973-4697393.50198.88
546064-4606491.69296.98
647037-4703793.62999.04
极限145590-4559090.74892.171.4397.0298.561.42
246169-4616991.90198.27
347083-4708393.720100.22
446692-4669292.94299.36
545496-4549690.56196.87
646792-4679293.14199.59
培哚普利氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号DJ468-220103对照品来源中检院对照品使用方法直接使用
对照品含量(%)94.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)10供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.213915339089393013914439224391820.21
29.123971539315395150.72
单位质量响应值RSD%判断
4254.294332.791.30数据可信
供试品溶液-697902批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min148106-4810695.60394.741.4895.6094.741.48
247200-4720093.80293.80
347237-4723793.87693.88
448700-4870096.78396.78
546816-4681693.03993.04
647967-4796795.32795.33
10min148854-4885497.08996.221.4698.1597.281.45
247824-4782495.04296.08
347362-4736294.12495.17
449012-4901297.40398.48
548358-4835896.10497.14
649095-4909597.56898.63
15min148154-4815495.69895.181.3997.8497.301.39
247142-4714293.68795.79
347415-4741594.23096.32
449036-4903697.45199.61
547677-4767794.75096.85
647930-4793095.25397.40
20min147603-4760394.60394.171.4197.8197.361.40
247298-4729893.99797.14
346535-4653592.48195.62
448472-4847296.33099.57
546904-4690493.21496.37
647512-4751294.42297.62
30min147187-4718793.77793.161.3498.0397.391.33
246085-4608591.58795.77
346723-4672392.85497.02
447823-4782395.04199.35
546361-4636192.13596.33
647082-4708293.56897.82
45min147222-4722293.84692.101.5599.1497.361.53
245700-4570090.82196.02
345454-4545490.33395.53
447112-4711293.62898.99
546316-4631692.04697.26
646269-4626991.95297.24
极限146338-4633892.08991.371.3998.4397.661.38
245796-4579691.01297.22
345085-4508589.59995.80
446739-4673992.88699.29
545457-4545790.33896.57
646452-4645292.31698.63
培哚普利氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号DJ468-220103对照品来源中检院对照品使用方法直接使用
对照品含量(%)94.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)10供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.213915239139392603929139145391970.19
29.123970939415395620.53
单位质量响应值RSD%判断
4255.924337.941.35数据可信
供试品溶液-697902批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min146996-4699693.32494.432.4693.3294.432.46
246864-4686493.06293.06
347328-4732893.98393.98
446235-4623591.81391.81
548539-4853996.38896.39
649365-4936598.02898.03
10min147045-4704593.42194.832.2994.4695.882.29
247417-4741794.16095.19
347485-4748594.29595.34
446446-4644692.23293.25
548840-4884096.98698.06
649290-4929097.87998.97
15min147550-4755094.42494.552.3796.5096.662.36
246888-4688893.11095.19
347436-4743694.19896.29
446112-4611291.56993.61
548393-4839396.09898.25
649314-4931497.927100.10
20min146153-4615391.65077.8948.4394.7781.0546.51
247329-4732993.98597.10
347156-4715693.64296.78
446305-4630591.95295.01
5479-4790.9514.17
647934-4793495.18798.45
30min146080-4608091.50592.382.4195.6596.402.28
246281-4628191.90496.06
346702-4670292.74096.92
444745-4474588.85492.94
547332-4733293.99197.22
647999-4799995.31699.64
45min145705-4570590.76091.722.0795.9296.771.90
246055-4605591.45596.64
345868-4586891.08496.29
444899-4489989.16094.23
547154-4715493.63897.91
647451-4745194.22899.61
极限145324-4532490.00490.301.3196.1796.361.25
245470-4547090.29496.49
345587-4558790.52696.75
444412-4441288.19394.25
545956-4595691.25996.57
646080-4608091.50597.93
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