奥美沙坦酯左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数4000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.791666316717166601672916640166820.24
215.861661516636166260.09
单位质量响应值RSD%判断
1056.491048.300.56数据可信
供试品溶液-8170102批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min113324-1332439.96938.962.7439.9738.962.74
212665-1266537.99237.99
312910-1291038.72738.73
412884-1288438.64938.65
513506-1350640.51540.51
612630-1263037.88737.89
10min117044-1704451.12850.301.4051.1950.371.40
216508-1650849.52049.58
316853-1685350.55550.62
416575-1657549.72149.79
517018-1701851.05051.12
616617-1661749.84749.91
15min119600-1960058.79658.002.6258.9558.152.61
218795-1879556.38156.53
319719-1971959.15359.30
418714-1871456.13856.29
519945-1994559.83159.98
619237-1923757.70757.85
20min121247-2124763.73662.813.1963.9963.063.18
220467-2046761.39661.64
321660-2166064.97565.22
420012-2001260.03160.27
521601-2160164.79865.05
620652-2065261.95162.19
30min123842-2384271.52170.252.8871.8870.602.87
222850-2285068.54568.89
324273-2427372.81473.17
422454-2245467.35767.70
523354-2335470.05770.42
623729-2372971.18271.53
45min125805-2580577.40975.883.0977.8876.343.08
224552-2455273.65074.11
325834-2583477.49677.97
424092-2409272.27172.72
525958-2595877.86878.35
625522-2552276.56077.02
60min127378-2737882.12880.483.2482.7381.073.24
226097-2609778.28578.86
327752-2775283.25083.86
425457-2545776.36576.94
527094-2709481.27681.88
627194-2719481.57682.17
极限132476-3247697.42197.342.8098.1698.072.80
232013-3201396.03296.74
333177-3317799.524100.27
430860-3086092.57393.27
532908-3290898.71799.46
633268-3326899.797100.52
奥美沙坦酯左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数4000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.791657316480165281654716546165350.21
215.861658116530165560.22
单位质量响应值RSD%判断
1047.181043.880.23数据可信
供试品溶液-8170102批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min113239-1323939.97437.287.0939.9737.287.08
211183-1118333.76633.77
312344-1234437.27237.27
412395-1239537.42637.43
513370-1337040.37040.37
611557-1155734.89534.90
10min117970-1797054.25950.155.7254.3350.225.73
216035-1603548.41648.47
316467-1646749.72149.78
416071-1607148.52548.59
517563-1756353.03053.10
615557-1555746.97347.03
15min120413-2041361.63557.695.3661.7957.845.36
218541-1854155.98356.12
318898-1889857.06157.21
418389-1838955.52455.67
520350-2035061.44561.60
618054-1805454.51354.65
20min122470-2247067.84663.945.0868.1164.185.09
220760-2076062.68362.91
321204-2120464.02464.26
420615-2061562.24562.48
522336-2233667.44267.70
619667-1966759.38359.61
30min124523-2452374.04570.994.6374.4271.344.64
223408-2340870.67971.01
323537-2353771.06871.41
422982-2298269.39269.73
524808-2480874.90675.28
621804-2180465.83666.16
45min126001-2600178.50876.403.6179.0076.863.62
225420-2542076.75477.21
325334-2533476.49476.96
424858-2485875.05775.51
526401-2640179.71680.21
623798-2379871.85672.29
60min127628-2762883.42180.933.6384.0581.533.64
227091-2709181.79982.38
326781-2678180.86381.46
426911-2691181.25681.84
527478-2747882.96883.60
624933-2493375.28375.84
极限132144-3214497.05697.412.3297.8298.142.33
232212-3221297.26297.98
331994-3199496.60397.33
432826-3282699.11699.83
533286-33286100.505101.27
631106-3110693.92294.60
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