依折麦布瑞舒伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号DSMF-387-240606对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.75对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.161918021917201919621918431920651918780.08
211.151921351920001920680.05
单位质量响应值RSD%判断
17193.3717225.830.14数据可信
供试品溶液-25090101批-依折麦布-pH7.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min166920-6692034.90918.5796.2034.9118.5796.19
265991-6599134.42534.42
367633-6763335.28135.28
42676-26761.3961.40
55727-57272.9882.99
64662-46622.4322.43
10min1121591-12159163.42934.9394.5063.4934.9694.50
2130025-13002567.82867.89
3122331-12233163.81563.87
48839-88394.6114.61
510368-103685.4095.41
68593-85934.4834.49
15min1156117-15611781.44043.6795.3381.6043.7695.33
2160983-16098383.97884.15
3152494-15249479.55079.71
410156-101565.2985.31
511634-116346.0696.08
610936-109365.7055.72
20min1174171-17417190.85848.0695.1791.1648.2295.17
2170403-17040388.89289.20
3171892-17189289.66989.97
411844-118446.1796.20
512193-121936.3616.38
612267-122676.3996.42
30min1184815-18481596.41051.0795.1596.8651.3195.14
2179526-17952693.65194.11
3184345-18434596.16596.61
412777-127776.6656.69
513113-131136.8406.88
612774-127746.6646.70
45min1185468-18546896.75151.8994.4597.3652.2194.45
2183917-18391795.94296.56
3186263-18626397.16597.77
413417-134176.9997.04
513735-137357.1657.21
613979-139797.2927.34
60min1186438-18643897.25752.2693.5598.0352.6893.56
2183693-18369395.82596.60
3187068-18706897.58598.35
414695-146957.6667.72
514652-146527.6437.70
614560-145607.5957.65
极限1187022-18702297.56152.5394.0498.5053.0394.04
2185968-18596897.01297.95
3188363-18836398.26199.19
413612-136127.1017.17
514583-145837.6077.68
614592-145927.6127.68
依折麦布瑞舒伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100601-201906对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.314376564377894377704382804385174380020.09
211.264383204387374385280.07
单位质量响应值RSD%判断
38726.9738945.650.40数据可信
供试品溶液-25090101批-瑞舒伐他汀钙-pH7.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1179957-17995741.49521.53103.1041.5021.53103.12
2179980-17998041.50141.50
3183675-18367542.35342.35
41061-10610.2450.24
58563-85631.9741.97
66981-69811.6101.61
10min1307965-30796571.01238.5296.4171.0838.5696.42
2326646-32664675.32075.39
3307130-30713070.82070.89
415860-158603.6573.66
524988-249885.7625.77
619727-197274.5494.55
15min11119-11190.2583.14101.960.453.2495.78
21044-10440.2410.44
31067-10670.2460.43
422575-225755.2055.21
528505-285056.5736.59
627482-274826.3376.35
20min11087-10870.2513.80102.350.443.9197.23
21187-11870.2740.47
31151-11510.2650.45
429223-292236.7386.75
532645-326457.5277.55
633630-336307.7557.78
30min11380-13800.3184.56102.600.514.6798.26
21211-12110.2790.47
31196-11960.2760.47
437691-376918.6918.72
539400-394009.0859.12
637678-376788.6888.72
45min11418-14180.3275.69103.680.525.82100.12
21385-13850.3190.52
31284-12840.2960.49
445410-4541010.47110.51
548704-4870411.23011.28
649965-4996511.52111.57
60min11536-15360.3546.49103.990.546.62100.91
21387-13870.3200.52
31380-13800.3180.51
453895-5389512.42712.49
555357-5535712.76412.83
655428-5542812.78112.85
极限11518-15180.3506.77104.280.546.91101.32
21566-15660.3610.56
31422-14220.3280.52
452848-5284812.18612.27
560122-6012213.86313.95
658781-5878113.55413.64
依折麦布瑞舒伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号DSMF-387-240606对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.75对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.161947371951481952641947221945521948850.16
211.151954481957901956190.13
单位质量响应值RSD%判断
17462.8117544.300.33数据可信
供试品溶液-25090101批-依折麦布-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min14256-42562.1832.7416.322.182.7416.32
26365-63653.2653.26
35656-56562.9012.90
44348-43482.2302.23
56039-60393.0973.10
65430-54302.7852.79
10min18979-89794.6054.8710.264.614.8710.26
210810-108105.5445.55
310584-105845.4295.43
48704-87044.4644.47
59355-93554.7984.80
68539-85394.3804.38
15min112005-120056.1575.8212.566.175.8412.54
212868-128686.6006.61
312920-129206.6276.64
49704-97044.9774.99
510544-105445.4085.42
610083-100835.1725.18
20min112558-125586.4416.308.176.466.328.17
213241-132416.7916.82
313572-135726.9616.99
411106-111065.6965.72
511400-114005.8475.87
611825-118256.0656.09
30min114066-140667.2146.6810.377.256.7210.38
214895-148957.6407.68
313666-136667.0097.05
411778-117786.0416.07
511936-119366.1226.15
611848-118486.0776.11
45min113580-135806.9656.788.877.016.828.90
214247-142477.3077.36
314758-147587.5697.62
411919-119196.1136.15
512764-127646.5476.59
612027-120276.1696.21
60min114853-148537.6187.078.547.677.128.53
214747-147477.5647.63
314876-148767.6307.69
412469-124696.3956.44
512543-125436.4336.49
613176-131766.7586.81
极限114858-148587.6217.105.607.697.175.61
214166-141667.2667.34
314291-142917.3307.40
412613-126136.4696.53
513532-135326.9417.00
613612-136126.9827.04
依折麦布瑞舒伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100601-201906对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.314443764454754459784446224445374449980.16
211.264452304451794452040.01
单位质量响应值RSD%判断
39345.5339538.540.35数据可信
供试品溶液-25090101批-瑞舒伐他汀钙-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min17494-74941.7011.8673.271.701.8673.37
216270-162703.6943.69
313380-133803.0383.04
48951-89512.0322.03
51736-17360.3940.39
61420-14200.3220.32
10min131843-318437.2304.5191.617.234.5191.52
237332-373328.4768.48
339725-397259.0199.02
43322-33220.7540.76
53603-36030.8180.82
63330-33300.7560.76
15min151564-5156411.7076.7193.7511.726.7293.74
254311-5431112.33112.35
358322-5832213.24213.26
43919-39190.8900.89
54891-48911.1101.11
64200-42000.9540.96
20min148642-4864211.0446.6891.0211.086.7091.03
253986-5398612.25712.30
358384-5838413.25613.30
44562-45621.0361.04
55087-50871.1551.16
65772-57721.3101.31
30min158121-5812113.1967.2790.7913.257.3090.78
262250-6225014.13314.19
355077-5507712.50512.57
45276-52761.1981.21
55875-58751.3341.34
65543-55431.2591.26
45min153203-5320312.0797.0388.3212.157.0788.33
252616-5261611.94612.03
361380-6138013.93614.02
45740-57401.3031.31
56866-68661.5591.57
65879-58791.3351.34
60min159756-5975613.5677.5586.8013.667.6186.82
262278-6227814.14014.24
356652-5665212.86212.97
46653-66531.5111.52
56777-67771.5391.55
67440-74401.6891.70
极限155735-5573512.6547.2682.3412.777.3382.38
255370-5537012.57112.70
356998-5699812.94113.07
47555-75551.7151.73
58362-83621.8991.91
67941-79411.8031.82
点击查看处理图标(人工保存)
　
原始图谱下载图谱(谢鑫慧 于 2025-09-06 15:29:00 完成)
生成报告数据部分(等待生成报告)
Current page cost:106 ms