多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.386770867946679736763267650677820.25
210.406802068383682020.38
单位质量响应值RSD%判断
6530.066557.880.31数据可信
供试品溶液-2025072421批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min151498-5149870.60768.992.4570.6168.992.45
248719-4871966.79666.80
350441-5044169.15769.16
449495-4949567.86067.86
549799-4979968.27768.28
651946-5194671.22171.22
10min162496-6249685.68585.990.7085.8086.100.70
262509-6250985.70385.81
362690-6269085.95186.07
463373-6337386.88887.00
563069-6306986.47186.58
662166-6216685.23385.35
15min166439-6643991.09191.700.5491.3591.960.54
266492-6649291.16491.42
367144-6714492.05892.32
467328-6732892.31092.57
566851-6685191.65691.91
667033-6703391.90692.17
20min167402-6740292.41293.160.7492.8293.580.74
267474-6747492.51192.92
368239-6823993.55993.97
468542-6854293.97594.39
567651-6765192.75393.16
668400-6840093.78094.19
30min168581-6858194.02894.350.5094.5994.910.50
268534-6853493.96494.52
368871-6887194.42694.99
469458-6945895.23195.80
568677-6867794.16094.73
668753-6875394.26494.83
45min169094-6909494.73294.690.6695.4595.410.66
268383-6838393.75794.47
369483-6948395.26595.99
469265-6926594.96695.69
568647-6864794.11994.84
669490-6949095.27596.00
60min168948-6894894.53195.090.5295.4195.970.51
268939-6893994.51995.39
369559-6955995.36996.25
469705-6970595.56996.45
569291-6929195.00295.88
669701-6970195.56496.45
极限169574-6957495.39095.670.3796.4396.710.37
269499-6949995.28796.32
370117-7011796.13497.18
469778-6977895.66996.71
569662-6966295.51096.55
670039-7003996.02797.07
多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.386775767916680686791568628680570.50
210.406831568029681720.30
单位质量响应值RSD%判断
6556.556555.000.02数据可信
供试品溶液-2025072521批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min157188-5718878.26673.198.2978.2773.188.29
254386-5438674.43274.43
353656-5365673.43373.43
452561-5256171.93471.93
545405-4540562.14062.14
657661-5766178.91478.91
10min165932-6593290.23386.803.8490.3686.923.84
263754-6375487.25287.38
364034-6403487.63687.76
462260-6226085.20885.33
559216-5921681.04281.15
665342-6534289.42689.56
15min167512-6751292.39690.631.6092.6890.901.62
266472-6647290.97291.24
366476-6647690.97891.25
465580-6558089.75190.01
564481-6448188.24788.49
666827-6682791.45891.74
20min168985-6898594.41192.421.2994.8592.841.31
267857-6785792.86893.29
367549-6754992.44692.87
467043-6704391.75492.17
566395-6639590.86791.25
667332-6733292.14992.58
30min169733-6973395.43594.090.8596.0394.660.85
268559-6855993.82894.40
368340-6834093.52994.10
469024-6902494.46595.03
568744-6874494.08294.62
668086-6808693.18193.77
45min169691-6969195.37894.650.8696.1395.380.86
268839-6883994.21294.94
368803-6880394.16294.89
470116-7011695.95996.68
568869-6886994.25394.95
668655-6865593.96094.70
60min170016-7001695.82295.060.6896.7395.950.68
269517-6951795.14096.03
369329-6932994.88295.77
469969-6996995.75896.64
569056-6905694.50995.36
668873-6887394.25895.16
极限170656-7065696.69896.250.8897.7797.300.88
269914-6991495.68396.73
371258-7125897.52298.57
470610-7061096.63597.68
569656-6965695.33096.34
669881-6988195.63896.69
多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.386784967713678736783367923678380.12
210.406791067883678960.03
单位质量响应值RSD%判断
6535.456528.460.08数据可信
供试品溶液-2025072522批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min154524-5452474.89373.512.1174.8973.512.11
252573-5257372.21372.21
352973-5297372.76272.76
452088-5208871.54771.55
554075-5407574.27674.28
654855-5485575.34775.35
10min164620-6462088.76088.580.8188.8888.700.81
264098-6409888.04388.16
364851-6485189.07789.20
463649-6364987.42687.55
565046-6504689.34589.47
664659-6465988.81488.94
15min167367-6736792.53392.680.5492.8192.950.55
267656-6765692.93093.20
367831-6783193.17193.44
466809-6680991.76792.03
567467-6746792.67192.94
667694-6769492.98293.26
20min168145-6814593.60294.240.4794.0394.660.47
268610-6861094.24194.66
369119-6911994.94095.36
468610-6861094.24194.66
568445-6844594.01494.44
668718-6871894.38994.82
30min169596-6959695.59595.650.6896.1896.240.67
270400-7040096.69997.28
369628-6962895.63996.22
469866-6986695.96696.54
569058-6905894.85695.44
669282-6928295.16495.75
45min170206-7020696.43396.010.9397.1896.760.92
270965-7096597.47598.22
369851-6985195.94596.69
469838-6983895.92796.66
569089-6908994.89995.64
669448-6944895.39296.14
60min170337-7033796.61396.280.7197.5297.180.70
270832-7083297.29398.20
369988-6998896.13397.04
470123-7012396.31997.21
569337-6933795.23996.14
669950-6995096.08196.98
极限170327-7032796.59996.820.8797.6697.880.86
271658-7165898.42799.49
370335-7033596.61097.67
470304-7030496.56797.62
569854-6985495.94997.01
670454-7045496.77497.84
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