多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.386797367617681376783268155679430.34
210.406784868450681490.63
单位质量响应值RSD%判断
6545.576552.790.08数据可信
供试品溶液-2025072421批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min148223-4822366.06468.325.5766.0668.325.57
246470-4647063.66263.66
351130-5113070.04670.05
453511-5351173.30873.31
547772-4777265.44665.45
652093-5209371.36571.37
10min160001-6000182.19984.672.7982.3184.782.79
260263-6026382.55882.66
361608-6160884.40084.52
463915-6391587.56187.68
561157-6115783.78383.89
663864-6386487.49187.61
15min164941-6494188.96690.511.2189.2190.761.21
265639-6563989.92390.17
365801-6580190.14590.40
466726-6672691.41291.68
566135-6613590.60290.85
667161-6716192.00892.27
20min167583-6758392.58693.010.7892.9893.410.79
267046-6704691.85092.24
368494-6849493.83494.24
468126-6812693.33093.75
567808-6780892.89493.29
668299-6829993.56793.98
30min168499-6849993.84194.260.4494.3994.820.45
268752-6875294.18794.73
368890-6889094.37694.94
469302-6930294.94195.52
568505-6850593.84994.40
668870-6887094.34994.92
45min169003-6900394.53195.230.5495.2495.950.55
269184-6918494.77995.48
369752-6975295.55796.28
469997-6999795.89396.63
569488-6948895.19695.91
669676-6967695.45396.18
60min169107-6910794.67495.360.5995.5496.240.60
269359-6935995.01995.88
369779-6977995.59496.47
470251-7025196.24197.14
569793-6979395.61496.48
669378-6937895.04595.94
极限170100-7010096.03495.950.3197.0696.990.31
269698-6969895.48396.50
370185-7018596.15197.19
470295-7029596.30197.36
570046-7004695.96096.99
669920-6992095.78796.84
多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.386746767396677816738767320674700.27
210.406803867809679240.24
单位质量响应值RSD%判断
6500.006531.150.34数据可信
供试品溶液-2025072521批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min157440-5744079.09775.405.7279.1075.405.72
252547-5254772.35972.36
356991-5699178.47878.48
449469-4946968.12068.12
556570-5657077.89977.90
655528-5552876.46476.46
10min166499-6649991.57189.222.6091.7089.342.60
264440-6444088.73688.86
364869-6486989.32789.46
461736-6173685.01285.13
566057-6605790.96391.09
665143-6514389.70489.83
15min169065-6906595.10592.941.5695.3993.211.56
267483-6748392.92693.19
367544-6754493.01093.29
465886-6588690.72790.98
567939-6793993.55493.84
667027-6702792.29892.58
20min169681-6968195.95394.461.0896.4094.891.08
268599-6859994.46394.89
367581-6758193.06193.50
468113-6811393.79494.20
569097-6909795.14995.59
668512-6851294.34394.77
30min169731-6973196.02295.150.9496.6295.740.94
269092-6909295.14295.72
368393-6839394.17994.77
468529-6852994.36794.93
569989-6998996.37796.97
668866-6886694.83195.42
45min170393-7039396.93395.670.8697.7096.420.86
269134-6913495.20095.94
368661-6866194.54895.30
469646-6964695.90596.62
569751-6975196.04996.81
669281-6928195.40296.15
60min170560-7056097.16395.770.8698.0996.680.86
269292-6929295.41796.32
368876-6887694.84495.75
469380-6938095.53896.42
569897-6989796.25097.17
669281-6928195.40296.31
极限171081-7108197.88196.340.9298.9797.410.92
269693-6969395.96997.03
369422-6942295.59696.66
469363-6936395.51596.55
570193-7019396.65897.74
670028-7002896.43197.49
多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.386760967228674786748167771675130.30
210.406884869059689540.22
单位质量响应值RSD%判断
6504.146630.191.36数据可信
供试品溶液-2025072522批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min150239-5023968.64370.355.8568.6470.355.86
255167-5516775.37675.38
350843-5084369.46869.47
447816-4781665.33265.33
549728-4972867.94567.94
655130-5513075.32675.33
10min162885-6288585.92286.203.0386.0486.313.03
264598-6459888.26288.39
362778-6277885.77685.89
459817-5981781.73081.84
563098-6309886.21386.33
665334-6533489.26889.39
15min165374-6537489.32390.581.8489.5890.841.85
267802-6780292.64092.91
366443-6644390.78391.04
464492-6449288.11788.36
566353-6635390.66090.92
667306-6730691.96292.24
20min167920-6792092.80192.891.2493.2193.301.25
268905-6890594.14794.57
368101-6810193.04993.46
466532-6653290.90591.30
567751-6775192.57092.98
668703-6870393.87194.30
30min168920-6892094.16894.320.5794.7394.880.57
269784-6978495.34895.93
369002-6900294.28094.84
468957-6895794.21894.76
568638-6863893.78294.34
668886-6888694.12194.71
45min169294-6929494.67994.920.7695.4095.640.76
270514-7051496.34597.09
369051-6905194.34795.07
469328-6932894.72595.43
569384-6938494.80295.52
669233-6923394.59595.34
60min168949-6894994.20795.240.9795.0896.120.97
270964-7096496.96097.86
369378-6937894.79395.67
469651-6965195.16696.02
569642-6964295.15496.03
669668-6966895.19096.09
极限169277-6927794.65596.090.9995.6997.130.98
271436-7143697.60598.67
370375-7037596.15697.19
470285-7028596.03397.05
570438-7043896.24297.28
670163-7016395.86696.92
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